BT

Typical G.C. analysis

cananga odorata flower oil CO2 extract
#%LeftshiftComponents
451.46alpha- amorphene
280.17(E)- anethole
620.02(Z)- asarone
40.59  benzaldehyde
186.15  benzyl acetate
120.04  benzyl alcohol
6411.97  benzyl benzoate
710.04  benzyl cinnamate
673.66  benzyl salicylate
520.02  bisabolene
590.61alpha- bisabolol
470.133- buten-2-yl benzoate
530.19delta- cadinene
540.01gamma- cadinene
423.96beta- caryophyllene
430.21alpha- cedrene
600.02  cedrol
92.731,8- cineole
300.02  cinnamic alcohol
260.21  cinnamic aldehyde
412.28  cinnamyl acetate
370.93alpha- copaene
140.53para- cresol
82.00para- cresyl methyl ether
400.60beta- cubebene
230.101,4- dimethoxybenzene
210.043,4- dimethoxytoluene
690.02  eicosane
380.02delta- elemene
550.02  elemol
190.02  ethyl benzoate
340.03  eugenol
440.54iso eugenol
5114.63(E,E)-alpha- farnesene
631.39(E,E)- farnesol
662.00  farnesyl acetate
351.00  geranyl acetate
4920.03  germacrene D
720.04  hexacosane
700.23  hexadecanoic acid
10.113- hexen-1-ol
70.013- hexen-1-yl acetate
570.01(Z)-3- hexen-1-yl benzoate
460.99alpha- humulene
310.13  indole
110.04  limonene
1616.47  linalool
200.012- methoxy-4-methyl phenol
290.04  methyl 2-methoxybenzoate
330.02  methyl anthranilate
250.074- methyl benzaldoxime
152.42  methyl benzoate
480.14  methyl eugenol
220.04  methyl salicylate
20.182- methyl-3-butenol
560.03alpha- muurolene
500.02gamma- muurolene
610.06alpha- muurolol
60.05  myrcene
580.02  nerolidol
130.02(E)-beta- ocimene
240.162- phenethyl acetate
680.022- phenethyl benzoate
100.03  phenyl acetaldehyde
270.102- phenyl-1-nitroethane
30.19alpha- pinene
50.07beta- pinene
320.024-(2- propenyl) phenol
650.01  tetradecanal
390.53  tetradecane
360.02alpha- ylangene

E. E. Stashenko, W. Torres and J. R. Martinez Morales, A study of the compositional variation of the essential oil of ylang ylang (Cananga odorata Hook. fil. et Thomson, forma genuina) during flower development. J. High Resol. Chromatogr., 18, 101-104 (1995).

P&F 24, No. 4, 31, (1999)

hyacinthus orientalis absolute
#%LeftshiftComponents
340.21-0.27  benzaldehyde
4736..84-44.24  benzyl acetate
521.78-1.95  benzyl alcohol
732.94-3.06  benzyl benzoate
630.80-0.13  benzyl tiglate
33trace2-sec- butyl-3-methoxypyrazine
35trace2-iso butyl-3-methoxypyrazine
20.01-0.05  camphene
390.02beta- caryophyllene
110.011,8- cineole
59trace  cinnamaldehyde
650.21-0.32  cinnamyl acetate
703.46-4.04(E)- cinnamyl alcohol
67trace(Z)- cinnamyl alcohol
560.02-0.04  creosol
170.05-0.56para- cymene
320.01-0.02  decanal
680.29-0.32  elemicin
440.05-0.09  ethyl benzoate
661.57-1.68  eugenol
420.00-trace(E)-beta- farnesene
46trace-0.03(Z,E)-alpha- farnesene
30.02  hexanal
230.03-0.04  hexanol
250.76-2.66(Z)-3- hexen-1-ol
280.02(E)-2- hexen-1-ol
240.03-0.08(E)-3- hexen-1-ol
210.02-0.05(Z)-3- hexen-1-yl acetate
64trace(Z)-3- hexen-1-yl benzoate
310.00-0.01(Z)-3- hexen-1-yl butyrate
150.04-0.19(Z)-3- hexen-1-yl formate
430.32-0.48(Z)-3- hexen-1-yl tiglate
16trace-0.01  hexyl acetate
483.80-3.94 hydroquinone dimethyl ether + (E,E)-alpha-farnesene
720.05-0.08  indole
90.53-1.00  limonene
360.03  linalool
710.00-trace2-(4- methoxyphenyl) ethyl alcohol
40.012- methyl (E)-2-butenal
600.01-0.10  methyl 2-methoxybenzoate
270.01-0.024- methyl anisole
690.02-0.03  methyl anthranilate
400.09-0.10  methyl benzoate
571.12-1.40  methyl eugenol
62trace  methyl N-methyl anthranilate
490.04-0.07  methyl salicylate
220.01-0.036- methyl-5-hepten-2-one
71.80-2.05  myrcene
260.01-0.03  nonanal
1313.72-14.93(E)-beta- ocimene
120.75-1.01(Z)-beta- ocimene
190.02-0.05  octanal
370.04  octanol
140.02-0.033- octanone
300.66-1.301- octen-3-ol
200.011- octen-3-one
60.01-0.021- penten-3-ol
8trace-0.01alpha- phellandrene
100.01beta- phellandrene
511.62-2.482- phenethyl acetate
538.96-16.392- phenethyl alcohol
740.40-0.532- phenethyl benzoate
50trace2- phenethyl formate
410.02-0.05  phenyl acetaldehyde
550.05-0.063- phenyl propyl acetate
580.81-0.863- phenyl propyl alcohol
10.08-0.16alpha- picoline
50.05-0.06gamma-picoline
29trace2-iso propyl-3-methoxypyrazine
450.00-0.04alpha- terpineol
180.01  terpinolene
611.12-1.261,2,4- trimethoxybenzene
380.16-0.172- undecanone
E. J. Brunke, F. J. Hammerschmidt and G. Schmaus, Head-space analysis of hyacinth flowers Fla.. Fragr J., 9, 56-69 (1994). P&F 20, No. 6, 35, (1995)
michelia champaca concrete
#%LeftshiftComponents
520.05iso amyl benzoate
360.035-amyl-3,4-dimethyl isoxazole
370.023-amyl-4,5-dimethyl isoxazole
244trace(E)- anethole
1400.03  benzaldehyde
730.10(E+Z)- benzaldoxime
1590.20  benzoic acid
2160.01 benzyl (Z)-3-hexenoate
212trace  benzyl 2-methyl butyrate
250.60  benzyl acetate
382.00  benzyl alcohol
901.00  benzyl benzoate
211trace  benzyl butyrate
210.10  benzyl formate
2130.03  benzyl isovalerate
240trace  benzyl methyl ether
2170.20  benzyl phenyl acetate
2180.10 benzyl phenyl propionate
209trace  benzyl propionate
2150.02  benzyl tiglate
2140.04  benzyl valerate
1220.10  borneol
2030.03  bornyl acetate
1680.01  bovolide
210trace  butyl benzoate
1010.03beta- caryophyllene
640.20  caryophyllene oxide
40.031,8- cineole
750.30  cinnamic alcohol
1430.02  cinnamic aldehyde
2510.01  cinnamic aldehyde oxime
256trace  cinnamonitrile
710.10(E)- cinnamyl acetate
2310.05  cinnamyl benzoate
2280.01  cinnamyl formate
2290.01  cinnamyl isovalerate
2300.05  cinnamyl tiglate
1720.01  coumarin
1340.02  creosol
133tracepara- cresol
570.04  cubenol
530.02epi- cubenol
139tracebeta- cyclocitral
169trace  decan-5-olide
1180.05  decanol
170trace(Z)-7- decen-5-olide
1540.10  dehydro-beta-ionone
155trace dehydro-beta-ionone 5,6-epoxide
910.053-oxo- dihydro-alpha-ionol
450.01  dihydro-alpha-ionone
870.103-oxo- dihydro-alpha-ionone
820.20(E+Z)-dihydro-alpha-ionone oxime
600.40  dihydro-beta-ionol
930.203-oxo- dihydro-beta-ionol
1290.01 dihydro-beta-ionol 5,6-epoxide
460.30  dihydro-beta-ionone
1570.054-oxo-dihydro-beta-ionone
830.40(E+Z)-dihydro-beta-ionone oxime
500.02 dihydro-beta-ionyl formate
1710.03  dihydroactinidiolide
740.02  dihydrobovolide
610.037-oxo-dihydrotheaspirane a1
670.037-oxo-dihydrotheaspirane a2
620.027-oxo-dihydrotheaspirane b1
680.027-oxo-dihydrotheaspirane b2
1670.022,3-dimethyl-2-nonen-4-olide
120trace(E)-6,10- dimethyl-5,9-undecadien-2-ol
130trace5,8-epidioxy-6-megastigmen-9-ol
153trace2,3- epoxy-2,6,6-trimethyl cyclohexan-1,4-dione
1840.01  ethyl 2-hydroxy-3-methyl valerate
178trace  ethyl 2-methyl butyrate
179trace  ethyl 3-methyl butyrate
220.50  ethyl benzoate
1770.01  ethyl butyrate
181trace  ethyl caproate
196trace  ethyl caprylate
233trace  ethyl cinnamate
2380.03  ethyl nicotinate
183trace  ethyl tiglate
690.30  eugenol
770.10iso eugenol
430.80(E,E)-alpha- farnesene
1250.20(E,E)- farnesol
1380.01  geranial
1580.10  geranic acid
1240.02  geraniol
207trace  geranyl acetate
480.04(E)- geranyl acetone
206trace  geranyl formate
1270.30  geranyl linalool
1030.10  germacrene D
1490.012- heptadecanone
1070.01  heptanol
252trace  heptanonitrile
255trace  hexadecanonitrile
90.02  hexanol
106trace(E)-2- hexenal
100.01(Z)-3- hexen-1-ol
70.01(Z)-3- hexen-1-yl acetate
192trace(Z)-3- hexen-1-yl acetate
1910.05(Z)-3- hexen-1-yl benzoate
189trace(Z)-3- hexen-1-yl butyrate
188trace(Z)-3- hexen-1-yl formate
1900.02(Z)-3- hexen-1-yl tiglate
186trace  hexyl acetate
1870.05  hexyl benzoate
185trace  hexyl formate
102tracealpha- humulene
136tracepara- hydroxyanisole
784.00  indole
550.03(E)-beta- ionol
1560.054-oxo-beta- ionol
510.10alpha- ionol
128tracebeta- ionol 5,6-epoxide
470.03(E)-alpha- ionone
540.20(E)-beta- ionone
560.10beta-ionone 5,7-epoxide
860.50(E)-alpha-ionone oxime
890.90(E)-beta-ionone oxime
850.20(Z)-alpha-ionone oxime
880.30(Z)-beta-ionone oxime
208tracebeta-ionyl formate
490.05(Z)- jasmone
2490.02 jasmone oxime
3trace  limonene
160.80  linalool
120.20(Z)- linalool oxide furanoid
350.20(E)- linalool oxide pyranoid
312.50(Z)- linalool oxide pyranoid
1631.00  linoleic acid
1640.50  linolenic acid
193trace  methyl (E)-2-hexenoate
260.02 methyl (E)-3-methyl-4-decenoate
800.14 methyl (E)-jasmonate
194trace  methyl (Z)-3-hexenoate
2010.01 methyl (Z)-3-methyl-4-decenoate
2000.02  methyl (Z)-4-decenoate
790.06  methyl (Z)-jasmonate
110.01  methyl 2-hydroxy-3-methyl butyrate
130.02 methyl 2-hydroxy-3-methyl valerate
1750.01  methyl 2-methyl butyrate
1760.01  methyl 3-methyl butyrate
2340.02  methyl 5-phenyl valerate
239trace4- methyl anisole
729.00  methyl anthranilate
175.00  methyl benzoate
1040.012- methyl butanol
105trace3- methyl butanol
140.02(E+Z)-2- methyl butyraldoxime
150.02(E+Z)-3- methyl butyraldoxime
174trace  methyl butyrate
1trace2- methyl butyronitrile
199trace  methyl caprinate
180trace  methyl caproate
1950.02  methyl caprylate
2320.05  methyl cinnamate
2420.10  methyl eugenol
2040.05  methyl geranate
173trace  methyl isobutyrate
2430.20  methyl isoeugenol
2500.02(Z)-methyl jasmonate oxime
2020.15  methyl laurate
942.01  methyl linoleate
960.50  methyl linolenate
2360.10  methyl N-acetyl anthranilate
650.02  methyl N-ethyl anthranilate
2370.10  methyl N-formyl anthranilate
630.05  methyl N-methyl anthranilate
280.15  methyl nicotinate
810.20  methyl palmitate
320.10  methyl phenyl acetate
340.15  methyl salicylate
920.20  methyl stearate
182trace  methyl tiglate
2350.01  methyl vanillate
5trace2- methyl-1-nitrobutane
146trace(E)-3- methyl-2-nonen-4-one
1190.02(E)-3- methyl-4-decen-1-ol
410.02(E)-3- methyl-4-decen-1-ol
580.043- methyl-5-(2,6,6-trimethyl cyclohex-1-en-1-yl) isoxazole
80.026- methyl-5-hepten-2-one
440.03(E+Z)-6- methyl-5-hepten-2-one oxime
99trace  myrcene
137trace  neral
1230.01  nerol
700.40(E)- nerolidol
205trace  neryl formate
590.101- nitro-2-phenethane
165trace  nonan-4-olide
1140.03  nonanol
1450.022- nonanone
2470.012- nonanone oxime
1170.02(Z,Z)-3,6- nonen-1-ol
115trace(Z)-3- nonen-1-ol
116trace(Z)-6- nonen-1-ol
1980.01(Z)-6- nonen-1-yl acetate
166trace2- nonen-4-olide
60.20(E)-beta- ocimene
1000.02(Z)-beta- ocimene
113trace(E,E)-2,4- octadien-1-ol
1120.01(Z,Z)-2,5-octadien-1-ol
1080.05  octanol
1440.013- octanone
246trace3- octanone oxime
253trace  octanonitrile
110trace(E)-2- octen-1-ol
109trace(Z)-2- octen-1-ol
1110.01(Z)-5- octen-1-ol
1970.05(Z)-5- octen-1-yl acetate
1610.20  palmitic acid
1480.012- pentadecanone
390.302- phenethyl acetate
4230.002- phenethyl alcohol
950.502- phenethyl benzoate
2200.012- phenethyl butyrate
2230.052- phenethyl caproate
2240.052- phenethyl caprylate
330.302- phenethyl formate
219trace2- phenethyl isobutyrate
2210.022- phenethyl isovalerate
241trace2- phenethyl methyl ether
2250.202- phenethyl phenyl acetate
2220.022- phenethyl tiglate
132trace  phenol
1410.02  phenyl acetaldehyde
761.00(E+Z)- phenyl acetaldoxime
230.01(E+Z)-phenyl acetaldoxime-O-methyl ether
1600.20  phenyl acetic acid
142trace  phenyl propionaldehyde
2270.053- phenyl propyl acetate
1310.023- phenyl propyl alcohol
2260.053- phenyl propyl formate
1260.30  phytol
97tracealpha- pinene
20.01beta- pinene
98trace  sabinene
245trace  safrole
1620.50  stearic acid
1210.03  terpinen-4-ol
270.10alpha- terpineol
254trace  tetradecanonitrile
840.054,4a,5,6-tetrahydro-4,4,7-trimethyl-2(3H)-naphthalenone
190.021,2,5,5-tetramethyl octahydroquinoline
660.031,3,7,7-tetramethyl-2-oxabicyclo(4.4.0)decan-9-one
290.202,5,5,8a- tetramethyl-6,7,8,8a-tetrahydro-1(5H)-1-benzopyran
180.02  theaspirane A
200.02  theaspirane B
1470.022- tridecanone
1520.012,6,6- trimethyl cyclohexan-1,4-dione
1500.206,10,14- trimethyl pentadecan-2-one
2480.056,10,14-trimethyl pentadecan-2-one oxime
1510.052,6,6- trimethyl-2-cyclohexen-1,4-dione
300.012,5,5-trimethyl-5,6,7,8-tetrahydroquinoline
240.012- undecanone
135tracepara- vinyl phenol

R. Kaiser, New volatile constituents of the flower concrete of Michelia champaca L. In: Proceedings of 11th International Congress of Essential Oils, Fragrances and Flavours. Edits., S. C. Bhattacharyya, N. Sen and K. L. Sethi, p. 1-13, Oxford & IBH Publishing Co., Pvt. Ltd, New Delhi (1989).

P&F 25, No. 4, 55, (2000)

ylang ylang flower oil
#%LeftshiftComponents
510.13alpha- amorphene
290.35(E)- anethole
50.94  benzaldehyde
2011.63  benzyl acetate
112.20  benzyl alcohol
636.19  benzyl benzoate
330.04  benzyl butyrate
651.37  benzyl salicylate
580.07alpha- bisabolol
470.713- buten-2-yl benzoate
360.08  butyl benzoate
530.16delta- cadinene
540.12gamma- cadinene
600.12 cadinol
610.12alpha- cadinol
421.69beta- caryophyllene
570.07  caryophyllene oxide
120.091,8- cineole
432.09(E)- cinnamyl acetate
300.26(E)- cinnamyl alcohol
380.13alpha- copaene
170.09para- cresol
100.34para- cresyl methyl ether
450.58beta- cubebene
260.131,4- dimethoxybenzene
250.173,4- dimethoxytoluene
211.46  ethyl benzoate
440.37(Z)-iso eugenol
522.34(E,E)-alpha- farnesene
620.84(E,E)- farnesol
640.61(E,E)- farnesyl acetate
371.96  geranyl acetate
495.55  germacrene D
30.28(E)-2- hexen-1-ol
90.16(Z)-3- hexen-1-yl acetate
550.19(Z)-3- hexen-1-yl benzoate
460.74alpha- humulene
130.07  limonene
1835.49  linalool
220.072- methoxy-4-methyl phenol
150.172- methoxyphenol
390.114-methoxyphenyl methyl acetate
310.05  methyl 2-methoxybenzoate
350.06  methyl 4-methoxybenzoate
320.08  methyl anthranilate
166.50  methyl benzoate
480.86  methyl eugenol
230.29  methyl salicylate
20.063- methyl-2-butenol
40.333- methyl-2-butenyl acetate
10.072- methyl-3-butenol
500.14gamma- muurolene
590.11alpha- muurolol
80.16  myrcene
270.27  nerol
560.13(E)- nerolidol
140.14(E)-beta- ocimene
280.202- phenyl-1-nitroethane
61.87alpha- pinene
70.66beta- pinene
340.084-(2- propenyl) phenol
240.14alpha- terpineol
415.51  tetradecane
400.16alpha- ylangene

E. E. Stashenko, W. Torres and J. R. Martinez Morales, A study of the compositional variation of the essential oil of ylang ylang (Cananga odorata Hook. fil. et Thomson, forma genuina) during flower development. J. High Resol. Chromatogr., 18, 101-104 (1995).

P&F 24, No. 4, 31, (1999)

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