BT

Typical G.C. analysis

carum petroselinum herb oil
This same year, a sample of Egyptian parsley herb oil was subjected to analysis by CC and CC/MS (El-Nikeety et al. 1998). This oil was found to contain:
#%LeftshiftComponents
210.20 apiole
170.21beta- bisabolene
20.06  camphene
150.05beta- caryophyllene
130.82para- cymene
145.35alpha-para- dimethyl styrene
190.15  elemicin
160.53alpha- humulene
65.36  limonene
106.20para- mentha-1,3,8-triene
220.404- methyl pyridine amine
1123.75  myrcene
208.79  myristicin
51.46alpha- phellandrene
719.47beta- phellandrene
16.94alpha- pinene
34.57beta- pinene
40.63  sabinene
80.17alpha- terpinene
180.13alpha- terpineol
92.78  terpinolene
120.065- undec-5-yne

M. M. A. El-Nikeety, A. T. M. El-Alek, M. M. I. A. El-Hady and A. Z. M. Badei, Changes in physical properties and chemical constituents of parsley herb volatile oil during storage, Egypt. J. Food Sci., 26-28 (1998).

P&F 26, No. 2, 22, (2001)

citrus aurantifolia swingle oil distilled peru
#%LeftshiftComponents
770.72(E)-alpha- bergamotene
730.06(Z)-alpha- bergamotene
900.04(E)-gamma- bisabolene
860.11(Z)-alpha- bisabolene
880.01(Z)-gamma- bisabolene
1000.06alpha- bisabolol
1010.06epi-alpha-bisabolol
450.82  borneol
430.06iso borneol
610.02  bornyl acetate
890.08delta- cadinene
980.03alpha- cadinol
990.03  campherenol
140.03delta-3- carene
54trace  carvone
750.42beta- caryophyllene
71traceiso caryophyllene
940.06  caryophyllene alcohol
950.02  caryophyllene oxide
153.521,4- cineole
204.351,8- cineole
66trace  citronellyl acetate
820.11gamma- curcumene
480.11para- cymen-8-ol
172.30para- cymene
270.16para- cymenene
510.11  decanal
59trace  decanol
74trace  decyl acetate
110.212,3- dihydro-1,8-cineole
180.022,2- dimethyl-5-(1-methyl propenyl) tetrahydrofuran
720.06  dodecanal
81trace  dodecanol
700.06beta- elemene
650.05delta- elemene
76tracegamma- elemene
92trace  elemol
400.034,8-epoxy-para-menth-1-ene
970.06gamma- eudesmol
872.07(E,E)-alpha- farnesene
780.09(Z)-beta- farnesene
50.79alpha- fenchene
320.82alpha- fenchol
330.01beta- fenchol
570.02  geranial
560.01  geraniol
690.07  geranyl acetate
930.05  germacrene B
830.09(Z)-beta- guaiene
790.08alpha- humulene
1939.19  limonene
38trace(E)- limonene oxide
36trace(Z)- limonene oxide
280.16  linalool
31tracepara- mentha-1,3,8-triene
250.02para- mentha-3,8-diene
90.016- methyl-5-hepten-2-one
101.00  myrcene
340.01  myrcenol
530.03  neral
520.02  nerol
670.06  neryl acetate
300.01  nonanal
10.03  nonane
220.45(E)-beta- ocimene
210.20(Z)-beta- ocimene
35traceallo- ocimene
120.05  octanal
240.02  octanol
580.05  perillaldehyde
130.44alpha- phellandrene
40.99alpha- pinene
80.77beta- pinene
390.03trans- pinene hydrate
460.05  pinocamphone
440.05iso pinocamphone
620.01trans- pinocarvyl acetate
55trace  piperitone
420.08iso pulegol
7trace  sabinene
800.04beta- santalene
910.10  selina-3,7(11)-diene
850.09alpha- selinene
371.27  terpinen-1-ol
470.71  terpinen-4-ol
600.02alpha- terpinen-7-al
162.35alpha- terpinene
2313.35gamma- terpinene
410.80(Z)-beta- terpineol
497.00alpha- terpineol
501.24gamma- terpineol
269.70  terpinolene
960.04  tetradecanal
840.181,1,3a,7-tetramethyl-1H-1a,2,2,3a,4,5,6,7b-octahydrocyclopropa(a)naphthalene
30.01alpha- thujene
20.03  tricyclene
63trace  tridecane
60.242,6,6-trimethyl-2-ethenyl tetrahydropyran
640.01  undecanal
290.02  undecane
680.01  undecanol

P. Dugo, A. Cotroneo, I. Bonarcorsi and L. Mondello, On the genuineness of citrus essential oils Part LVII. The composition of distilled lime oil. Flav. Fragr. J., 13, 93-97 (1998).

P&F 24, No. 2, 35, (1999)

cymbopogon laniger extract
#%LeftshiftComponents
9trace-0.40iso amyl hexanoate
232.60-3.70trans- carveol
240.40-0.70cis- carveol
170.10-2.90  carvone
20.10-1.101,8- cineole
16trace-1.20  cuminyl alcohol
50.10-0.20para- cymene
120.20-2.00(Z)- dihydrocarvone
110.10-0.50(E)- dihydrocarvone
10.50-13.20  limonene
80.70-1.20(E)- limonene oxide
6trace-0.40(Z)- limonene oxide
40.40-1.60para- mentha-1,3,8-triene
3trace-0.10para- mentha-1,5,8-triene
2124.00-35.20(E)-para- mentha-1(7),8-dien-2-ol
2516.00-24.00(Z)-para- mentha-1(7),8-dien-2-ol
148.20-10.20(Z)-para-mentha-2,8-dien-1-ol
1313.30-16.20(E)-para- mentha-2,8-dien-1-ol
193.20-6.00para- methyl acetophenone
150.10-1.60  myrtenol
200.30-0.80  perillaldehyde
26trace-0.80  perillyl alcohol
7trace-0.10(Z)-2- phenyl but-2-ene
181.30-3.80 piperitenol
220.10-0.20iso piperitenone
100.10-0.50iso pulegone
cymbopogon martini var. sofia oil
#%LeftshiftComponents
10.08iso amyl alcohol
90.08iso amyl butyrate
280.47iso amyl hexanoate
360.45iso amyl octanoate
30.06  camphene
170.07  camphor
253.05trans- carveol
230.68cis- carveol
293.20  carvone
380.04  caryophyllene oxide
110.13para- cresol
40.05 dehydro-1,8-cineole
210.28(E)- dihydrocarvone
340.10  eucarvone
300.04  geraniol
350.03  geranyl acetate
390.04  humulene oxide
830.09  limonene
160.16(Z)- limonene oxide
130.03  linalool
240.04para- menth-1-en-9-al
330.55para- menth-8-ene-1,2-diol
120.58para- mentha-1,3,8-triene
51.14para- mentha-1,5,8-triene
71.64para-mentha-1(7),2,8-triene
2712.14(E)-para- mentha-1(7),8-dien-2-ol
1913.01(Z)-para- mentha-1(7),8-dien-2-ol
156.84(E)-para- mentha-2,8-dien-1-ol
1411.09(Z)-para-mentha-2,8-dien-1-ol
262.63para- menthadienol
225.34para- menthadienol
201.70para-menthatrienol
180.076-methyl bicyclo(3.3.0)oct-2-en-7-one
400.03alpha- muurolol
370.09  nerolidol
100.02  octanol
320.21  perillaldehyde
20.02alpha- pinene
310.11iso piperitenone
60.02alpha- terpinene

M. H. Boelens, Sensory and chemical evaluation of tropical grass oils. Perfum. Flavor, 19(2), 29-45 (1994).

P&F 25, No. 3, 54, (2000)

hyptis suaveolens (l.) poit. oil mali
#%LeftshiftComponents
482.20-4.00ar- abietatriene
39trace-0.20  aromadendrene oxide
2612.00-18.80(E)-alpha-bergamotene + beta-caryophyllene
461.60-2.50(Z)-alpha-bergamotol
471.80-3.00(E)-alpha- bergamotol
34trace-0.60delta- cadinene
450.30-0.70alpha- cadinol
50.10-0.30delta-3- carene
370.10-0.30iso caryophyllene oxide
380.90-1.90  caryophyllene oxide
90.50-0.801,8- cineole
21trace-0.10alpha- cubebene
22trace-0.20beta- cubebene
350.20-0.40para- cymen-8-ol
140.30-1.30para- cymene
180.10-0.40para- cymenene
40trace-0.10  elemol
25trace-0.20beta- fenchol
330.10-0.90  geranial
360.10-0.30  geraniol
16trace-0.10  hexanol
170.10-0.20(Z)-3- hexen-1-ol
280.70-1.80alpha- humulene
82.00-4.90  limonene
240.10-0.20  linalool
10trace-0.10para- mentha-1,3,8-triene
320.20-0.50alpha- muurolene
43trace-0.10T- muurolol
420.10-0.30alpha- muurolol
60.20-0.50  myrcene
290.20-1.00  neral
13trace-0.10(Z)-beta- ocimene
11trace-0.10(E)-beta- ocimene
190.30-0.901- octen-3-ol
11.80-2.60alpha- pinene
33.70-6.00beta- pinene
430.40-37.10  sabinene
20trace-0.10(E)- sabinene hydrate
23trace-0.20(Z)- sabinene hydrate
410.30-0.70  spathulenol
440.10-0.30epi-spathulenol
272.10-5.30  terpinen-4-ol
70.60-0.90alpha- terpinene
121.00-2.10gamma- terpinene
300.10-0.30alpha- terpineol
154.00-7.20  terpinolene
2trace-0.10alpha- thujene
310.60-1.00  valencene
J. of Ess. Oil Res. 13, No. 1, 55, (2001)
laurus nobilis leaf oil turkey
#%LeftshiftComponents
840.10(E)- anethole
1390.20  anhydrooplopanone
16trace  benzaldehyde
1230.10  bicyclogermacrene
1290.20alpha- bisabolene
550.30  borneol
830.70  bornyl acetate
1010.10 bourbonene
23<0.10iso butyl 2-methyl butyrate
9traceiso butyl isobutyrate
1520.10  cadalene
128trace  cadina-1,4-diene
1250.30gamma- cadinene
1260.40delta- cadinene
146traceT- cadinol
1500.10alpha- cadinol
1300.10alpha- calacorene
1330.10beta- calacorene
1270.10  calamenene
150.70  camphene
47<0.10alpha- campholenic aldehyde
25<0.10delta-3- carene
890.10  carvacrol
710.20trans- carveol
740.10cis- carveol
780.10  carvone
950.10cis- carvyl acetate
1450.603(15),7(14)- caryophylladien-6-ol
1060.40beta- caryophyllene
1360.90  caryophyllene oxide
2921.801,8- cineole
920.401,8-cineole-2-yl acetate
1080.70  cinnamyl acetate
100<0.10alpha- copaene
770.10  cuminaldehyde
105<0.10  cuminyl acetate
870.10  cuminyl alcohol
600.20para- cymen-8-ol
271.50para- cymene
38<0.10para- cymenene
1140.30(E)-3-decen-1-yl acetate
1540.20  dehydrocostus lactone
75<0.102,3- dimethoxytoluene
96trace2- dodecanone
1020.60beta- elemene
1310.30  elemicin
1470.30(E)-iso elemicin
210.201,8-epoxy-2-para-menthene
1550.10  eremanthin
2trace  ethyl 2-methyl butyrate
3trace  ethyl isovalerate
1490.30alpha- eudesmol
1481.10beta- eudesmol
142<0.1010-epi-gamma- eudesmol
144tracegamma- eudesmol
942.90  eugenol
1110.20(E)-iso eugenol
118<0.10(Z,E)-alpha- farnesene
153<0.10  farnesyl acetone
14<0.10alpha- fenchene
110trace  geranyl acetone
1150.10  germacrene D
109<0.10  guaia-6,9-diene
1070.10alpha- guaiene
104<0.10alpha- gurjunene
22trace2,4- heptadienal
1<0.10  hexanal
7<0.10  hexanol
4<0.10(E)-2- hexenal
6trace(E)-2- hexen-1-ol
50.10(E)-3- hexen-1-ol
410.10  hotrienol
1130.10alpha- humulene
1400.10  humulene oxide
1510.30  intermedeol
510.10  ipsdienol
1410.20laevo-junenol
1380.30  ledol
281.50  limonene
392.00  linalool
36<0.10(E)- linalool oxide furanoid
35<0.10(Z)- linalool oxide furanoid
490.20(Z)-para- menth-2-en-1-ol
460.20(E)-para- menth-2-en-1-ol
910.10para- mentha-1,4-dien-7-ol
570.20para- mentha-1,5-dien-8-ol
640.20para- mentha-1(7),2-dien-8-ol
610.30(E)-para- mentha-1(7),8-dien-2-ol
730.30(Z)-para- mentha-1(7),8-dien-2-ol
480.10(Z)-para-mentha-2,8-dien-1-ol
450.10(E)-para- mentha-2,8-dien-1-ol
42<0.10para- menthatriene
67<0.10  methyl chavicol
1033.50  methyl eugenol
1200.40(E)- methyl isoeugenol
65trace  methyl salicylate
19<0.106- methyl-5-hepten-2-one
1210.10gamma- muurolene
124tracealpha- muurolene
200.60  myrcene
680.40  myrtenal
720.10  nerol
520.10  nerol oxide
1320.10(E)- nerolidol
99<0.10  neryl acetate
31trace2- nonanone
30<0.10(E)-beta- ocimene
134trace  palustrol
810.10  phellandral
240.20alpha- phellandrene
970.103- phenyl propyl acetate
124.60alpha- pinene
184.00beta- pinene
500.10trans- pinocarveol
540.20  pinocarvone
880.10  pinocarvyl acetate
34<0.10  pinol
430.10isopinol
66<0.10(Z)- piperitol
690.10(E)- piperitol
79trace  piperitone
8traceiso propyl 2-methyl butyrate
62trace4-iso propyl-2-cyclohexenone
530.10  sabinaketone
175.30  sabinene
33<0.10(E)- sabinene hydrate
40trace(Z)- sabinene hydrate
76trace  sabinol
860.10  sabinyl acetate
112trace  selina-4(15),5-diene
1190.30beta- selinene
1220.30alpha- selinene
116tracegamma- selinene
1350.80  spathulenol
594.30  terpinen-4-ol
261.30alpha- terpinene
321.80gamma- terpinene
633.10alpha- terpineol
560.60delta- terpineol
370.70  terpinolene
900.90delta- terpinyl acetate
939.80alpha- terpinyl acetate
130.102,4(10)- thujadiene
800.504- thujen-2-alpha-yl acetate
110.60alpha- thujene
44tracebeta- thujone
82trace  thymol
10<0.10  tricyclene
1170.102- tridecanone
58trace  umbellulone
850.202- undecanone
1430.20  valerianol
70<0.10  verbenone
1370.30  viridiflorol
980.10alpha- ylangene
J. of Ess. Oil Res. 13, No. 2, 95, (2001)
mandarin oil
#%LeftshiftComponents
10.91alpha- thujene
22.29alpha- pinene
30.05  camphene
41.88beta- pinene
51.73  myrcene
60.02delta-2- carene
70.48alpha- phellandrene
84.25para- cymene
966.41  limonene
100.03(E)-beta- ocimene
110.01(Z)-beta- ocimene
1219.17gamma- terpinene
131.38  terpinolene
14tracepara- mentha-1,3,8-triene
150.01gamma- terpineol
16trace(Z)-para- menth-2-en-1-ol
170.13  linalool
18trace(Z)- sabinene hydrate
19trace(Z)-beta- terpineol
20traceiso pulegol
21trace(E)-beta- terpineol
220.04  terpinen-4-ol
230.12alpha- terpineol
24trace  citronellol
250.02  hexanol
260.123- octanol
270.03  decanol
280.02  benzaldehyde
29trace3- methyl benzaldehyde
30trace  nonanal
31trace  geranial
32trace  perillaldehyde
330.10  terpinen-4-yl acetate
340.50  methyl N-methyl anthranilate
35trace  thymol
360.08beta- caryophyllene
37tracealpha- humulene
38tracebeta- selinene
390.30alpha- farnesene
40tracedelta- cadinene

G. Della Porta, E. Reverchon, D. Chouchi and D. Barth, Mandarin and lime peel oil processing by supercritical CO2 desorption:deterpenation and high molecular weight compounds elimination. J. Essent. Oil Res., 9, 519-522 (1997).

P&F 26, No. 1, 36, (2001)

mandarin oil italy
#%LeftshiftComponents
280.02  benzaldehyde
40tracedelta- cadinene
30.05  camphene
60.02delta-2- carene
360.08beta- caryophyllene
24trace  citronellol
84.25para- cymene
270.03  decanol
390.30alpha- farnesene
31trace  geranial
250.02  hexanol
37tracealpha- humulene
966.41  limonene
170.13  linalool
16trace(Z)-para- menth-2-en-1-ol
14tracepara- mentha-1,3,8-triene
29trace3- methyl benzaldehyde
340.50  methyl N-methyl anthranilate
51.73  myrcene
30trace  nonanal
100.03(E)-beta- ocimene
110.01(Z)-beta- ocimene
260.123- octanol
32trace  perillaldehyde
70.48alpha- phellandrene
22.29alpha- pinene
41.88beta- pinene
20traceiso pulegol
18trace(Z)- sabinene hydrate
38tracebeta- selinene
220.04  terpinen-4-ol
330.10  terpinen-4-yl acetate
1219.17gamma- terpinene
21trace(E)-beta- terpineol
19trace(Z)-beta- terpineol
230.12alpha- terpineol
150.01gamma- terpineol
131.38  terpinolene
10.91alpha- thujene
35trace  thymol

G. Della Porta, E. Reverchon, D. Chouchi and D. Barth, Mandarin and lime peel oil processing by supercritical CO2 desorption:deterpenation and high molecular weight compounds elimination. J. Essent. Oil Res., 9, 519-522 (1997).

P&F 26, No. 1, 36, (2001)

petroselinum crispum leaf oil
#%LeftshiftComponents
3927.96 apiole
250.02alpha- bergamotene
480.04  bergapten
300.41beta- bisabolene
190.02  bornyl acetate
370.783- butyl phthalide
380.63(E)- butylidene phthalide
40trace(Z)- butylidene phthalide
350.01  carotol
240.02beta- caryophyllene
220.02alpha- copaene
71.46para- cymene
120.04para- cymenene
18trace(E)-2- decenal
170.77(Z)-2- decenal
291.672,6- dimethoxy-4-(2-propenyl) phenol
231.59beta- elemene
330.71  elemicin
521.79  falcarindiol
4915.00  falcarinol
260.01(E)-beta- farnesene
270.17  germacrene D
550.37  heraclenol
460.37  hexadecanoic acid
540.04  imperatorin
422.79(E)- ligustilide
440.01(Z)- ligustilide
130.15  linalool
510.01  linoleic acid
140.49para- menthatriene
500.06  methyl linoleate
51.94  myrcene
318.70  myristicin
360.06iso myristicin
150.05  myrtenal
340.02  nerolidol
90.02(E)-beta- ocimene
60.39alpha- phellandrene
81.72beta- phellandrene
328.51beta-sesqui phellandrene
531.06iso pimpinellin
20.25alpha- pinene
42.00beta- pinene
451.24  psoralen
30.01  sabinene
412.29  sedanenolide
430.05(E)-sedanolide
100.09gamma- terpinene
112.50  terpinolene
21tracealpha- terpinyl acetate
10.14alpha- thujene
160.20  undecatriene
200.424- vinyl guaiacol
470.24  xanthotoxin
280.05  zingiberene

M. Spraul, Strukteraufklarung Wertgebender Inhaltsstoffe aus Petersilienblatten, - Wurzeln and -samen sowie aus Dillbluten. Ph.D. thesis Technische Universtat, Munchen (1991).

P&F 21, No. 4, 57, (1996)

petroselinum crispum leaf oil cuba
In 1997, Pino et al. analyLed a parsley leaf oil that was produced from plants grown in Cuba. Using CC/MS as the method of analysis the oil was determined to contain the following constituents:
#%LeftshiftComponents
240.02alpha- amorphene
3414.40 apiole
110.02  benzyl alcohol
210.02(E)-beta- bergamotene
321.42  carotol
190.24beta- caryophyllene
140.03  citronellal
160.09para- cymen-8-ol
50.03para- cymene
90.28alpha-para- dimethyl styrene
180.61beta- elemene
200.21gamma- elemene
281.70  elemicin
290.02iso elemicin
300.02  elemol
230.11(Z)-beta- farnesene
251.09  germacrene D
330.28  guaiol
220.03alpha- humulene
70.06  limonene
123.90para- mentha-1,3,8-triene
130.05para- mentha-1,4,8-triene
150.03para- menthatriene
30.84  myrcene
2663.90  myristicin
310.03  nerolidol
40.09alpha- phellandrene
61.60beta- phellandrene
271.04beta-sesqui phellandrene
10.03alpha- pinene
20.01beta- pinene
80.03gamma- terpinene
100.72  terpinolene
170.02  thymol

J. A. Pino, A. Rosado and V. Fuentes, Herb oil of parsley (Petroselinum crispum Mill.) from Cuba. J. Essent. Oil Res., 9, 241-242 (1997).

P&F 26, No. 2, 22, (2001)

petroselinum crispum leaf oil cuba
In 1997, Pino et al. analyLed a parsley leaf oil that was produced from plants grown in Cuba. Using CC/MS as the method of analysis the oil was determined to contain the following constituents:
#%LeftshiftComponents
240.02alpha- amorphene
3414.40 apiole
110.02  benzyl alcohol
210.02(E)-beta- bergamotene
321.42  carotol
190.24beta- caryophyllene
140.03  citronellal
160.09para- cymen-8-ol
50.03para- cymene
90.28alpha-para- dimethyl styrene
180.61beta- elemene
200.21gamma- elemene
281.70  elemicin
290.02iso elemicin
300.02  elemol
230.11(Z)-beta- farnesene
251.09  germacrene D
330.28  guaiol
220.03alpha- humulene
70.06  limonene
123.90para- mentha-1,3,8-triene
130.05para- mentha-1,4,8-triene
150.03para- menthatriene
30.84  myrcene
2663.90  myristicin
310.03  nerolidol
40.09alpha- phellandrene
61.60beta- phellandrene
271.04beta-sesqui phellandrene
10.03alpha- pinene
20.01beta- pinene
80.03gamma- terpinene
100.72  terpinolene
170.02  thymol

J. A. Pino, A. Rosado and V. Fuentes, Herb oil of parsley (Petroselinum crispum Mill.) from Cuba. J. Essent. Oil Res., 9, 241-242 (1997).

P&F 26, No. 2, 22, (2001)

petroselinum crispum seed oil
#%LeftshiftComponents
230.07 apiole
200.07beta- bisabolene
220.35delta- cadinene
30.13  camphene
160.09para- cymen-8-ol
80.11para- cymene
130.28alpha-para- dimethyl styrene
212.64  elemicin
180.08beta- farnesene
100.10  limonene
140.28para- mentha-1,3,8-triene
150.10para- methyl acetophenone
60.54  myrcene
1947.54  myristicin
70.28alpha- phellandrene
97.52beta- phellandrene
222.28alpha- pinene
516.20beta- pinene
40.87  sabinene
110.10gamma- terpinene
170.07alpha- terpineol
120.14  terpinolene
10.19alpha- thujene

Y.H. Kim, K. S. Kim and C. K. Hong, Volatile Components of Parsley Leaf and Seed (Petrselinum crispum). J. Korean Agric. Chem. Soc., 33, 62-67 (1990).

P&F 16, No. 5, 75, (1991)

piper cernum vell. var. cernum yuncker leaf oil brazil
#%LeftshiftComponents
191.60alpha- agarofuran
260.20  bulnesol
181.30delta- cadinene
242.40alpha- cadinol
25.30  camphene
60.40delta-3- carene
142.30beta- caryophyllene
120.20alpha- copaene
100.30alpha- cubebene
1732.30(Z)-dihydroagarofuran
130.60beta- elemene
90.20delta- elemene
206.70beta- elemol
217.1010-epi-gamma- eudesmol
231.60beta- eudesmol
221.00gamma- eudesmol
150.90alpha- humulene
70.70  limonene
80.30para- mentha-1,3,8-triene
162.90gamma- muurolene
50.50  myrcene
110.20alpha- pinene
47.40beta- pinene
33.50  sabinene
252.10  valerianol
110.90alpha- ylangene
J. of Ess. Oil Res. 12, No. 4, 443, (2000)
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