BT

Typical G.C. analysis

croton flavens l. (welensali) leaf oil curacao
#%LeftshiftComponents
470.30allo- aromadendrene
241.20  borneol
320.20  bornyl acetate
280.50  bornyl formate
390.30beta- bourbonene
511.20delta- cadinene
41.70  camphene
220.30  camphene hydrate
19tracealpha- campholenal
20trace  camphor
449.30iso caryophyllene
110.101,8- cineole
380.60alpha- copaene
360.20alpha- cubebene
487.90ar- curcumene
101.70para- cymene
420.50  cyperene
270.102- decanone
430.202,6- dimethoxy-para-cymene
40trace2- dodecanone
410.80beta- elemene
350.30delta- elemene
490.30  germacrene D
450.80alpha- gurjunene
461.50alpha- humulene
121.30  limonene
180.40  linalool
16trace(E)- linalool oxide furanoid
15trace(Z)- linalool oxide furanoid
370.20  longicyclene
8trace4- methyl anisole
300.10  methyl carvacrol
29trace  methyl thymol
70.60  myrcene
520.40(E)- nerolidol
130.20(Z)-beta- ocimene
91.50alpha- phellandrene
316.00alpha- pinene
60.70beta- pinene
21.020trans- pinocarveol
230.10  pinocarvone
50.20  sabinene
534.50  spathulenol
250.10  terpinen-4-ol
140.20gamma- terpinene
260.10alpha- terpineol
17trace  terpinolene
20.30alpha- thujene
34trace  thymol
10.20  tricyclene
500.302- tridecanone
330.502- undecanone
310.60trans- verbenyl acetate
J. of Ess. Oil Res. 12, No. 6, 667, (2000)
glycosmis pentaphylla (cor.) bark oil india
#%LeftshiftComponents
140.50alpha- cadinol
50.20alpha- copaene
120.201-epi- cubenol
60.202- dodecanone
160.60  ethenyl dodecanoate
210.30  ethyl hexadecanoate
90.20  globulol
204.70  hexadecanoic acid
130.20T- muurolol
220.50  oleic acid
190.20  pentadecanoic acid
170.202- pentadecanone
10.20  terpinen-4-ol
110.20  tetradecanal
180.70  tetradecanoic acid
80.502- tridecanol
728.102- tridecanone
40.30  undecanol
32.302- undecanol
252.102- undecanone
100.20  viridiflorol
150.50oxo-alpha-ylangene
J. of Ess. Oil Res. 12, No. 4, 471, (2000)
laurus nobilis leaf oil turkey
#%LeftshiftComponents
840.10(E)- anethole
1390.20  anhydrooplopanone
16trace  benzaldehyde
1230.10  bicyclogermacrene
1290.20alpha- bisabolene
550.30  borneol
830.70  bornyl acetate
1010.10 bourbonene
23<0.10iso butyl 2-methyl butyrate
9traceiso butyl isobutyrate
1520.10  cadalene
128trace  cadina-1,4-diene
1250.30gamma- cadinene
1260.40delta- cadinene
146traceT- cadinol
1500.10alpha- cadinol
1300.10alpha- calacorene
1330.10beta- calacorene
1270.10  calamenene
150.70  camphene
47<0.10alpha- campholenic aldehyde
25<0.10delta-3- carene
890.10  carvacrol
710.20trans- carveol
740.10cis- carveol
780.10  carvone
950.10cis- carvyl acetate
1450.603(15),7(14)- caryophylladien-6-ol
1060.40beta- caryophyllene
1360.90  caryophyllene oxide
2921.801,8- cineole
920.401,8-cineole-2-yl acetate
1080.70  cinnamyl acetate
100<0.10alpha- copaene
770.10  cuminaldehyde
105<0.10  cuminyl acetate
870.10  cuminyl alcohol
600.20para- cymen-8-ol
271.50para- cymene
38<0.10para- cymenene
1140.30(E)-3-decen-1-yl acetate
1540.20  dehydrocostus lactone
75<0.102,3- dimethoxytoluene
96trace2- dodecanone
1020.60beta- elemene
1310.30  elemicin
1470.30(E)-iso elemicin
210.201,8-epoxy-2-para-menthene
1550.10  eremanthin
2trace  ethyl 2-methyl butyrate
3trace  ethyl isovalerate
1490.30alpha- eudesmol
1481.10beta- eudesmol
142<0.1010-epi-gamma- eudesmol
144tracegamma- eudesmol
942.90  eugenol
1110.20(E)-iso eugenol
118<0.10(Z,E)-alpha- farnesene
153<0.10  farnesyl acetone
14<0.10alpha- fenchene
110trace  geranyl acetone
1150.10  germacrene D
109<0.10  guaia-6,9-diene
1070.10alpha- guaiene
104<0.10alpha- gurjunene
22trace2,4- heptadienal
1<0.10  hexanal
7<0.10  hexanol
4<0.10(E)-2- hexenal
6trace(E)-2- hexen-1-ol
50.10(E)-3- hexen-1-ol
410.10  hotrienol
1130.10alpha- humulene
1400.10  humulene oxide
1510.30  intermedeol
510.10  ipsdienol
1410.20laevo-junenol
1380.30  ledol
281.50  limonene
392.00  linalool
36<0.10(E)- linalool oxide furanoid
35<0.10(Z)- linalool oxide furanoid
490.20(Z)-para- menth-2-en-1-ol
460.20(E)-para- menth-2-en-1-ol
910.10para- mentha-1,4-dien-7-ol
570.20para- mentha-1,5-dien-8-ol
640.20para- mentha-1(7),2-dien-8-ol
610.30(E)-para- mentha-1(7),8-dien-2-ol
730.30(Z)-para- mentha-1(7),8-dien-2-ol
480.10(Z)-para-mentha-2,8-dien-1-ol
450.10(E)-para- mentha-2,8-dien-1-ol
42<0.10para- menthatriene
67<0.10  methyl chavicol
1033.50  methyl eugenol
1200.40(E)- methyl isoeugenol
65trace  methyl salicylate
19<0.106- methyl-5-hepten-2-one
1210.10gamma- muurolene
124tracealpha- muurolene
200.60  myrcene
680.40  myrtenal
720.10  nerol
520.10  nerol oxide
1320.10(E)- nerolidol
99<0.10  neryl acetate
31trace2- nonanone
30<0.10(E)-beta- ocimene
134trace  palustrol
810.10  phellandral
240.20alpha- phellandrene
970.103- phenyl propyl acetate
124.60alpha- pinene
184.00beta- pinene
500.10trans- pinocarveol
540.20  pinocarvone
880.10  pinocarvyl acetate
34<0.10  pinol
430.10isopinol
66<0.10(Z)- piperitol
690.10(E)- piperitol
79trace  piperitone
8traceiso propyl 2-methyl butyrate
62trace4-iso propyl-2-cyclohexenone
530.10  sabinaketone
175.30  sabinene
33<0.10(E)- sabinene hydrate
40trace(Z)- sabinene hydrate
76trace  sabinol
860.10  sabinyl acetate
112trace  selina-4(15),5-diene
1190.30beta- selinene
1220.30alpha- selinene
116tracegamma- selinene
1350.80  spathulenol
594.30  terpinen-4-ol
261.30alpha- terpinene
321.80gamma- terpinene
633.10alpha- terpineol
560.60delta- terpineol
370.70  terpinolene
900.90delta- terpinyl acetate
939.80alpha- terpinyl acetate
130.102,4(10)- thujadiene
800.504- thujen-2-alpha-yl acetate
110.60alpha- thujene
44tracebeta- thujone
82trace  thymol
10<0.10  tricyclene
1170.102- tridecanone
58trace  umbellulone
850.202- undecanone
1430.20  valerianol
70<0.10  verbenone
1370.30  viridiflorol
980.10alpha- ylangene
J. of Ess. Oil Res. 13, No. 2, 95, (2001)
petitgrain sweet oil
#%LeftshiftComponents
61.66delta-3- carene
470.20trans- carveol
490.21cis- carveol
500.10  caryophyllene oxide
221.52  citronellal
421.30  citronellol
300.70  citronellyl acetate
440.60  cuminaldehyde
480.50para- cymen-8-ol
80.09ortho- cymene
143.17para- cymene
170.082,6- dimethyl-5-heptenal
390.312- dodecanone
260.03beta- elemene
310.17(E)-beta- farnesene
381.72  geranial
410.32  geranyl acetate
360.31  geranyl formate
109.76  limonene
2412.09  linalool
210.89(E)- linalool oxide furanoid
201.07(Z)- linalool oxide furanoid
250.30  linalyl acetate
510.29para- mentha-1,4-dien-7-ol
120.12ortho- mentha-1(7),5,8-triene
430.09para- methyl acetophenone
340.20  methyl geranate
160.476- methyl-5-hepten-2-one
70.40  myrcene
290.50  myrtenal
450.07  myrtenol
321.01  neral
460.66  nerol
370.08  neryl acetate
180.753- octanol
190.16  perillene
110.01beta- phellandrene
10.95alpha- pinene
41.76beta- pinene
520.46para-iso propyl anisole
280.51iso pulegol
522.32  sabinene
230.61  sabinene hydrate
273.33  terpinen-4-ol
130.11gamma- terpinene
90.08alpha-terpinene + heptanal + 2-methyl-2-butenal
331.09alpha- terpineol
150.02  terpinolene
350.12alpha- terpinyl acetate
20.58alpha- thujene
30.08  toluene
400.392,6,6- trimethyl-2-vinyl-5-hydroxytetrahydropyran

A. Baaliouamer, B. Y. Meklati, D. Fraisse and C. Scharff, Analysis of leaf oils from four varieties of sweet orange by combined gas chromatography mass spectrometry. Flav. Fragr. J., 3, 47-52 ( 1988).

P&F 18, No. 5, 43, (1993)

ruta graveolens flower oil colombia
#%LeftshiftComponents
333.09  chalepensin (xylotenin)
50.051,8- cineole
121.252- decanone
230.087,8- dihydroxy-6-methoxycoumarin
190.682- dodecanone
180.912-dodecanone branched
200.05  dodecyl acetate
240.25  elemol
101.31  geijerene
20.092- heptanone
10.04(Z)-3- hexen-1-ol
60.10  limonene
280.19  methyl 4-(3,4-methylene dioxyphenyl) butyrate
250.164-(3,4- methylene dioxyphenyl)-2-butanone
300.066-(3,4-methylene dioxyphenyl)-2-hexanone
320.778-(3,4- methylene dioxyphenyl)-2-octanone
310.371-(3,4-methylene dioxyphenyl)-4-hexene-3-one
4trace  myrcene
110.04  naphthalene
80.06  nonanal
90.072- nonanol
716.822- nonanone
170.16  nonyl acetate
30.182- octanone
130.16  octyl acetate
140.082- octyl acetate
270.692-(3- phenyl-1-propyl) furan
290.24  psoralen
260.072- tetradecanone
221.392- tridecanone
210.122-tridecanone branched
1568.052- undecanone
160.062-undecanone branched

E. E. Stashenko, H. S. Villa and M. Y. Combariza, Comparitive study of Colombian rue oils by high resolution gas chromatography using different detection systems. J. Microcol. Sep., 7, 117-122 (1995), 35th Internat. Symosium Chromatogr. Proceedings, 475-483, Japan (1995).

P&F 23, No. 6, 53, (1998)

ruta graveolens oil
#%LeftshiftComponents
340.36  angelicin
110.161,8- cineole
90.02para- cymene
191.312- decanone
260.332-decyl acetate
320.052,6- di-tert-butyl-4-methyl phenol
350.25  dibutyl phthalate
280.542- dodecanone
330.18  elemol
20.02  ethyl benzene
30.012- heptanone
10.073- hexen-1-ol
70.043- hexen-1-yl acetate
160.022-hydroxy-4-methoxyphenyl methyl ketone
100.09  limonene
80.022- methoxytoluene
200.10  methyl chavicol
230.129- methyl-2-decanone
300.0711-methyl-2-dodecanone
170.069-methyl-2-nonanone
271.2810- methyl-2-undecanone
150.251-methyl-5,6-diethyl cyclohexene
180.07  nonanol
130.732- nonanol
1224.122- nonanone
250.57  nonyl acetate
2216.712- nonyl acetate
60.022- octanol
50.242- octanone
210.21  octyl acetate
140.482- octyl acetate
360.86  phytol
40.02alpha- pinene
310.802- tridecanone
2436.822- undecanone
293.042- undecyl acetate

H-H. Xu, S-F. Chiug, J. Zhou, J-K. Ding and X-J. Yu, Preliminary studies on insecticidal activity of the rue oil and analysis of its components. Natural Product Res. Dev.,6(4), 56-61 (1994).

P&F 23, No. 6, 35, (1998)

ruta graveolens oil cuba
#%LeftshiftComponents
260.61(E)- amyl cinnamic alcohol
170.77(Z)-gamma- bisabolene
180.07delta- cadinene
60.37  camphor
140.22beta- caryophyllene
298.18  curcuphenol
20.01para- cymene
90.722- decanone
132.432- dodecanone
191.44  elemol
250.42alpha- eudesmol
240.56beta- eudesmol
230.33gamma- eudesmol
71.64  geijerene
315.68  hexadecanoic acid
300.362- hexadecanone
150.03alpha- humulene
30.16  limonene
10.01  myrcene
200.26(E)- nerolidol
50.622- nonanone
40.02(E)-beta- ocimene
322.38iso phytol
110.52 pregeijerene
100.10  pulegone
80.08  terpinen-4-ol
280.29  tetradecanoic acid
270.06  tetradecanol
210.202- tetradecanone
220.07  tridecanoic acid
163.722- tridecanone
1248.672- undecanone

J. A. Pino, A. Rosado and V. Fuentes, Leaf oils of Ruta graveolens L. grown in Cuba. J. Essent. Oil Res., 9, 365-366 (1997).

P&F 23, No. 6, 53, (1998)

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