BT

Typical G.C. analysis

alpinia galanga oil
#%LeftshiftComponents
2410.70alpha- bergamotene
3016.20beta- bisabolene
12trace  borneol
172.50  bornyl acetate
20.50  camphene
230.90  caryophyllene
332.50  caryophyllene oxide
160.20  chavicol
191.00  chavicyl acetate
75.501,8- cineole
201.60  citronellyl acetate
220.70  copaene
281.90ar- curcumene
14tracepara- cymen-8-ol
60.80para- cymene
291.50  eugenyl acetate
2618.20(E)-beta- farnesene
215.10  geranyl acetate
250.60alpha- humulene
81.60  limonene
11trace  linalool
50.70  myrcene
311.90  pentadecane
321.60beta-sesqui phellandrene
110.20alpha- pinene
41.60beta- pinene
3trace  sabinene
270.80 santalene
130.30  terpinen-4-ol
9tracealpha- terpinene
150.20alpha- terpineol
10trace  terpinolene
18trace  tridecane

H. L. De Pooter, M. Nor Omar, B. A. Coolsaet and N. M. Schamp, The Essential Oil of Greater Galanga (Alpinia galanga) from Malaysia, Phytochem.,24, 93-96 (1985).

P&F 11, No. 1, 29, (1986)

boronia megastigma nees absolute
#%LeftshiftComponents
380.102-acetoxylinalool A + tridecane + methyl 2-methoxybenzoate
580.02 acetvanillone + (E)-beta-farnesene
320.45(E)-anethole + safrol + nonanoic acid
87trace apiole
48.015 benzyl 3-methyl butyrate + (Z)-retro-gamma-ionone
40.01  benzyl alcohol
970.06  benzyl benzoate
880.20beta-bisabolol + tetradecanol
340.10isobornyl acetate + menthyl acetate
400.02trans-carvyl acetate + (E)-linalool
540.04beta- caryophyllene
730.09  caryophyllene oxide
120.01  chrysanthenone
651.20sesqui cineole
86trace  coniferyl methyl ether
410.07 cyclic beta-ionone
470.03 decanoic acid + benzyl 2-methyl butyrate + (Z)-retro-gamma-ionone
220.012- decanol
310.06 decanol + 5-hydroxylinalool B + methyl 2-isobutyroxy-3-methyl valerate
210.602-decanone + 7-hydroxyhotrienol
570.657,8-dihydro-beta-ionol + (Z)-retro-alpha-ionone
551.307,8- dihydro-beta-ionone
630.06 dihydroactinodiolide + undecyl acetate
230.01 dodecane + lilac alcohol
500.042- dodecanol
763.80 dodecyl acetate + 8-hydroxylinalyl isobutyrate
108trace  eicosane
420.01delta- elemene
700.097,11-epoxymegastigm-5(6)-en-9-one
490.01  ethyl decanoate
950.08(E,E)- farnesol
28trace  geraniol
460.70 geranyl acetate + vanillin
56trace  geranyl acetone
1114.30(E)-4-(geranyl oxy) cinnamic acid
1061.90(Z)-4-(geranyl oxy) cinnamic acid
90.02  guaiacol
940.70  heptadecane
770.04  hexadecane
590.03alpha- humulene
750.03  humulene oxide I
850.303- hydroxy-beta-ionone
430.208- hydroxylinalool
910.108-hydroxylinalyl 2-methyl butyrate
1132.208-hydroxylinalyl decanoate
1160.308-hydroxylinalyl dodecanoate
1050.308-hydroxylinalyl heptanoate
1091.808-hydroxylinalyl heptanoate
920.108-hydroxylinalyl isovalerate
1120.708-hydroxylinalyl nonanoate
690.208-hydroxylinalyl propionate
990.308-hydroxylinalyl tiglate
1181.408-hydroxylinalyl tridecanoate
980.098-hydroxylinalyl valerate
802.40(E)-3-hydroxymegastigm-7-en-9-one
680.03(Z)-3-hydroxymegastigm-7-en-9-one
1070.09N-(2-(4-hydroxyphenyl)ethyl) 2-methyl butyramide
1100.20N-(2-(4-hydroxyphenyl)ethyl) tiglamide
1159.30N-(2-(4-hydroxyphenyl)ethyl) tiglamide + methyl (Z)-4-(geranyl oxy) cinnamate
840.154-oxo-beta- ionol
520.30beta-ionol + 4,5-epoxy-gamma-homocyclocitral
710.64(E,E)-pseudo- ionone
450.05(Z)-alpha-ionone + (Z)-carvyl acetate
530.04(E)-alpha-ionone + 2,6-dimethyl-4-methyl phenol
6114.90(E)-beta-ionone + alpha-curcumene + 5,6-epoxy-beta-ionone
670.02  italicene ether
820.35delta-jasmonic acid lactone (syn) + 4-hydroxy-beta-ionone
890.70delta-jasmonic acid lactone )anti) + methyl curcubate
50.45  limonene
290.20 linalyl acetate + 5-hydroxylinalool A
740.30(E)-megastigm-7-en-3,9-dione
140.15para-mentha-1,3,8-triene + camphor
30.06para- mentha-1,5,8-triene
1176.70 methyl (E)-4-(geranyl oxy) cinnamate
960.50  methyl (E)-4-hydroxycinnamate
830.70  methyl (Z)-epi-jasmonate
791.20 methyl (Z)-jasmonate + (E)-3-hydroxymegastigm-7-en-9-one
10.10 methyl 1-hydroxy-3-methyl valerate + beta-pinene
440.20 methyl 2-(2-methyl butyoxy)-3-methyl valerate + neryl acetate
150.06 methyl 2-acetoxy-3-methyl valerate
810.70 methyl 2,3-di-epi-curcubate + 4-oxo-beta-ionone
9014.60 methyl 3-epi-curcubate + (Z)-8-heptadecene
18tracepara- methyl acetophenone
240.01  methyl nonanoate
130.01  methyl octanoate
1040.02  methyl palmitate
20.40 myrcene + octanal
250.20 nerol + (E)-tagetenone
1030.08  nonadecane
100.75 nonanal + linalool + hotrienol + 2-phenethyl alcohol
19trace  nonanol
110.082- nonanol
70.07(E)-beta- ocimene
60.02(Z)-beta- ocimene
1010.03  octadecane
200.07  octanoic acid
80.03  octanol
640.16 pentadecane + isoitalicene ether
102trace  pentadecyl acetate
620.05endoperoxide of cyclic beta-ionone
660.02beta-sesqui phellandrene
30traceisopiperitenone + geranial
270.01  piperitone
720.55 spathulenol + (E)-9-hydroxymegastigm-7-en-3-one
780.09 syringl methyl ether + zingerone
260.30(Z)-tagetenone + anisaldehyde
160.02(E)- tagetone
170.03(Z)- tagetone
35trace  terpinen-4-yl acetate
510.02  tetradecane
1000.50  tetradecyl acetate
370.03 theaspirane A + 2-undecanol
392.40 theaspirane B + 2-acetoxylinalool B + methyl decanoate
1140.03  tricosane
930.15  tridecyl acetate
360.05  undecanal
601.00 undecanoic acid + 8-hydroxyl linalyl acetate + dodecanol + 2-phenethyl isovalerate + benzyl tiglate
330.052-undecanone + bornyl acetate

P. Weyerstahl, H. Marschall, W-R. Bork, R. Rilk, S. Schneider and H-C. Wahlburg, Constituents of the absolute of Boronia megastigma Nees from Tasmania. Flav. Fragr. J., 10, 297-311 (1995).

P&F 24, No. 1, 53, (1999)

cajuput leaf oil vietnam
#%LeftshiftComponents
49trace  bulnesol
370.4  cadina-1,4-diene
35tracedelta- cadinene
34tracegamma- cadinene
47tracealpha- cadinol
44traceT- cadinol
38trace  calamenene
2trace  camphene
5tracedelta-3- carene
232.5beta- caryophyllene
410.3  caryophyllene oxide
1041.11,8- cineole
20tracealpha- copaene
270.5gamma- curcumene
156.8para- cymene
170.2para- cymenene
220.3beta- elemene
18tracedelta- elemene
25tracegamma- elemene
42trace  elemol
480.7beta- eudesmol
450.6gamma- eudesmol
310.3alpha- farnesene
390.4  geraniol
290.3beta- guaiene
431.2  guaiol
281.6alpha- humulene
94.1  limonene
213.6  linalool
40tracealpha- maaliene
46tracealpha- muurolol
60.1  myrcene
14trace(E)-beta- ocimene
12trace(Z)-beta- ocimene
70.5alpha- phellandrene
110.2beta- phellandrene
36tracebeta-sesqui phellandrene
13.2alpha- pinene
30.8beta- pinene
4trace  sabinene
331.5alpha- selinene
321.5beta- selinene
241.5  terpinen-4-ol
80.6alpha- terpinene
134.6gamma- terpinene
308.7alpha- terpineol
165.9  terpinolene
26trace  thujopsene
190.3alpha- ylangene

O. Motl, J. Hodacova and K. Ubik, Composition of Vietnamese cajuput essential oil. Flav. Fragr. J., 5, 39-42 (1990).

P&F 25, No. 1, 33, (2000)

citrus x latifolia oil expressed
#%LeftshiftComponents
330.8alpha- bergamotene
52trace(E)-alpha- bisabolene
480.8beta- bisabolene
68tracealpha- bisabolol
25trace  borneol
32trace  bornyl acetate
690.1alpha- cadinol
30.1  camphene
6tracedelta-3- carene
350.3beta- caryophyllene
73trace  cinnamic alcohol
220.1  citronellal
40trace  citronellyl acetate
19tracealpha- cubebene
27tracebeta- cubebene
150.1para- cymene
240.1  decanal
72trace  decanoic acid
61trace(E)-2- dodecen-1-ol
340.1beta- elemene
210.1delta- elemene
37tracegamma- elemene
67tracegamma- eudesmol
500.2(E,E)-alpha- farnesene
410.1(E)-beta- farnesene
71trace(E,E)- farnesyl acetate
492.3  geranial
58trace  geraniol
511.0  geranyl acetate
45trace  geranyl formate
560.1  germacrene B
460.1  germacrene D
70trace  heptadecanal
650.1  hexadecanal
42tracealpha- humulene
1052.2  limonene
260.2  linalool
30trace  linalyl acetate
59tracepara- mentha-1,8-dien-10-yl acetate
38trace(E)-para- mentha-2,8-dien-1-ol
71.3  myrcene
431.2  neral
62trace(E)- nerolidol
471.4  neryl acetate
18trace  nonanal
310.1  nonyl acetate
14trace(E)-beta- ocimene
12trace(Z)-beta- ocimene
74trace  octadecanal
17trace  octanal
29trace  octanol
23trace  pentadecane
54trace  perillaldehyde
60trace  perillyl acetate
8tracealpha- phellandrene
11tracebeta- phellandrene
53tracebeta-sesqui phellandrene
23.2alpha- pinene
413.0beta- pinene
57traceiso piperitenone
52.0  sabinene
200.1(E)- sabinene hydrate
280.1(Z)- sabinene hydrate
39tracebeta- santalene
64trace  spathulenol
90.3alpha- terpinene
1317.0gamma- terpinene
440.4alpha- terpineol
160.7  terpinolene
55trace  tetradecanal
1tracealpha- thujene
66trace  thymol
36trace  undecanal
75trace  undecanoic acid
63trace  viridiflorol

S. M. Njoroge, H. Ueda, H. Kusunose and M. Sawamura, Japanese sour citrus fruits Part IV. Volatile compounds of Naaoshichi and Tahiti lime essential oils. Flav. Fragr. J., 11, 25-29 (1996).

P&F 24, No. 2, 35, (1999)

curcuma longa root oil CO2 extract
#%LeftshiftComponents
81.40alpha- bergamotene
91.08  borneol
25.50  camphene
132.12  carvone
71.63beta- caryophyllene
54.05  citronellal
202.94  citronellyl valerate
32.16 cubebene
174.23ar- curcumene
41.15para- cymene
151.02  germacrene D
141.01  linalool
61.99  menthofuran
181.53  nerol
163.17beta-sesqui phellandrene
191.84  phellandrol
11.25alpha- pinene
120.96alpha- terpineol
1116.12 turmerone
1042.00ar- turmerone
211.14  xanthorrhizol

B. Gopalan, M. Goto, A. Kodama and T. Hirose, Supercritical carbon dioxide extraction of Turmeric (Curcuma longa). J. Agric. Food Chem., 48, 2189-2192 (2000).

P&F 25, No. 6, 32, (2000)

curcuma longa root oil vietnam
#%LeftshiftComponents
100.20beta- bisabolene
70.90beta- caryophyllene
20.101,8- cineole
121.50ar- curcumene
171.00  curzerenone
30.05para- cymene
60.05beta- elemene
80.50alpha- humulene
10.05  limonene
113.00beta-sesqui phellandrene
50.05  terpinen-4-ol
40.90  terpinolene
130.15alpha,alpha,para- trimethyl benzyl alcohol
1430.00alpha- turmerone
1610.00ar- turmerone
1510.00beta- turmerone
91.50  zingiberene

T. S. Phan, N. H. Van, X. D. Nguyen and S. B. Luong, Chemical composition of the essential oil from rhizome Curcuma longa Linn. of Vietnam. Tap Chi Hoa Hoc, 25(1), 18-21 (1987).

P&F 25, No. 6, 32, (2000)

daucus carota ssp. maximus (desf.) ball seed oil
#%LeftshiftComponents
1517.65beta- asarone
80.28alpha- bergamotene
163.00alpha- bisabolene
1334.70beta- bisabolene
170.39preiso calamendiol
71.48beta- caryophyllene
4tracepara- cymene
100.43(E)-beta- farnesene
90.31alpha- humulene
5trace  limonene
61.97  methyl eugenol
1137.22(E)- methyl isoeugenol
140.25beta-sesqui phellandrene
1tracealpha- pinene
3tracebeta- pinene
2trace  sabinene
120.65  shyobunone

H. E. A. Saad, S. H. El-Sharkawy and A. F. Halim, Essential oils of Daucus carota ssp. maximus. Pharm. Acta Helv. 70, 79-84 (1995).

P&F 24, No. 6, 45, (1999)

petroselinum crispum leaf oil
#%LeftshiftComponents
3927.96 apiole
250.02alpha- bergamotene
480.04  bergapten
300.41beta- bisabolene
190.02  bornyl acetate
370.783- butyl phthalide
380.63(E)- butylidene phthalide
40trace(Z)- butylidene phthalide
350.01  carotol
240.02beta- caryophyllene
220.02alpha- copaene
71.46para- cymene
120.04para- cymenene
18trace(E)-2- decenal
170.77(Z)-2- decenal
291.672,6- dimethoxy-4-(2-propenyl) phenol
231.59beta- elemene
330.71  elemicin
521.79  falcarindiol
4915.00  falcarinol
260.01(E)-beta- farnesene
270.17  germacrene D
550.37  heraclenol
460.37  hexadecanoic acid
540.04  imperatorin
422.79(E)- ligustilide
440.01(Z)- ligustilide
130.15  linalool
510.01  linoleic acid
140.49para- menthatriene
500.06  methyl linoleate
51.94  myrcene
318.70  myristicin
360.06iso myristicin
150.05  myrtenal
340.02  nerolidol
90.02(E)-beta- ocimene
60.39alpha- phellandrene
81.72beta- phellandrene
328.51beta-sesqui phellandrene
531.06iso pimpinellin
20.25alpha- pinene
42.00beta- pinene
451.24  psoralen
30.01  sabinene
412.29  sedanenolide
430.05(E)-sedanolide
100.09gamma- terpinene
112.50  terpinolene
21tracealpha- terpinyl acetate
10.14alpha- thujene
160.20  undecatriene
200.424- vinyl guaiacol
470.24  xanthotoxin
280.05  zingiberene

M. Spraul, Strukteraufklarung Wertgebender Inhaltsstoffe aus Petersilienblatten, - Wurzeln and -samen sowie aus Dillbluten. Ph.D. thesis Technische Universtat, Munchen (1991).

P&F 21, No. 4, 57, (1996)

petroselinum crispum leaf oil cuba
In 1997, Pino et al. analyLed a parsley leaf oil that was produced from plants grown in Cuba. Using CC/MS as the method of analysis the oil was determined to contain the following constituents:
#%LeftshiftComponents
240.02alpha- amorphene
3414.40 apiole
110.02  benzyl alcohol
210.02(E)-beta- bergamotene
321.42  carotol
190.24beta- caryophyllene
140.03  citronellal
160.09para- cymen-8-ol
50.03para- cymene
90.28alpha-para- dimethyl styrene
180.61beta- elemene
200.21gamma- elemene
281.70  elemicin
290.02iso elemicin
300.02  elemol
230.11(Z)-beta- farnesene
251.09  germacrene D
330.28  guaiol
220.03alpha- humulene
70.06  limonene
123.90para- mentha-1,3,8-triene
130.05para- mentha-1,4,8-triene
150.03para- menthatriene
30.84  myrcene
2663.90  myristicin
310.03  nerolidol
40.09alpha- phellandrene
61.60beta- phellandrene
271.04beta-sesqui phellandrene
10.03alpha- pinene
20.01beta- pinene
80.03gamma- terpinene
100.72  terpinolene
170.02  thymol

J. A. Pino, A. Rosado and V. Fuentes, Herb oil of parsley (Petroselinum crispum Mill.) from Cuba. J. Essent. Oil Res., 9, 241-242 (1997).

P&F 26, No. 2, 22, (2001)

thuja orientalis fruit oil
#%LeftshiftComponents
120.20iso bornyl acetate
32.20  camphene
162.50  cedrol
141.20  cuparene
81.40para- cymen-8-ol
101.30para- cymen-9-ol
170.50beta- eudesmol
22.30alpha- fenchene
130.30alpha- humulene
50.90  limonene
612.30beta- phellandrene
150.70beta-sesqui phellandrene
167.80alpha- pinene
110.10iso pulegyl acetate
42.00  sabinene
71.10gamma- terpinene
90.40alpha- terpineol
J. of Ess. Oil Res. 12, No. 3, 292, (2000)
thymus richardii pers. subsp. nitidus (guss.) jalas oil italy
#%LeftshiftComponents
270.70allo- aromadendrene
3032.30beta- bisabolene
14trace  borneol
250.60beta- bourbonene
311.00delta- cadinene
344.00T- cadinol
13trace  camphor
2213.10  carvacrol
24trace  carvacryl acetate
180.50trans- carveol
200.70  carvone
263.40beta- caryophyllene
333.10  caryophyllene oxide
80.751,8- cineole
52.10para- cymene
161.00(Z)- dihydrocarvone
175.00(E)- dihydrocarvone
291.90  germacrene D
61.00  limonene
121.60  linalool
1912.40  methyl thymol
280.40gamma- muurolene
4trace  myrcene
70.50beta- phellandrene
320.70beta-sesqui phellandrene
10.70alpha- pinene
3tracebeta- pinene
2trace  sabinene
101.50(Z)- sabinene hydrate
150.60  terpinen-4-ol
9tracegamma- terpinene
11tracebeta- thujone
211.30  thymol
23trace  thymyl acetate
J. of Ess. Oil Res. 13, No. 1, 8, (2001)
wulffia stenoglossa dc. flower oil brazil
#%LeftshiftComponents
190.20(E)-alpha- bergamotene
225.10  bicyclogermacrene
242.70beta- bisabolene
370.70epi-alpha-bisabolol
260.30delta- cadinene
250.10gamma- cadinene
360.40alpha- cadinol
178.80beta- caryophyllene
321.00  caryophyllene oxide
140.10alpha- copaene
152.40beta- copaene
120.60  decanal
310.50  dendrolasin
430.10  docosane
110.10  dodecane
130.30delta- elemene
180.10gamma- elemene
410.10  ethyl hexadecanoate
233.30  germacrene A
290.10  germacrene B
2113.00  germacrene D
330.10  globulol
420.10  heneicosane
470.10  heptacosane
460.10  hexacosane
202.10alpha- humulene
340.10  humulene oxide II
513.60  limonene
70.50  linalool
390.10  methyl hexadecanoate
350.40alpha- muurolol
411.80  myrcene
380.70  myristic acid
300.90(E)- nerolidol
80.20  nonanal
10.20  nonane
617.30(E)-beta- ocimene
404.00  palmitic acid
450.30  pentacosane
270.10beta-sesqui phellandrene
22.10alpha- pinene
31.00  sabinene
280.10(Z)-sesqui sabinene hydrate
90.10  terpinen-4-ol
100.10alpha- terpineol
160.10  tetradecane
440.20  tricosane
J. of Ess. Oil Res. 12, No. 4, 415, (2000)
zingiber officinale oil CO2 extract
#%LeftshiftComponents
113.53beta- bisabolene
201.82 bisabolyl acetate
30.60  borneol
70.31beta- caryophyllene
1trace1,8- cineole
910.87ar- curcumene
181.31  eudesmol
60.83  eugenol
1314.17beta- farnesene
160.88(E,E)- farnesol
15trace(Z,Z)- farnesol
226.02  gingerol
172.26  gingerone
210.54 lanceolyl acetate
2trace  linalool
50.80  linalyl acetate
192.21  nerolidyl acetate
80.64  neryl acetate
126.81beta-sesqui phellandrene
14tracebeta- selinene
2312.226- shogaol
42.51alpha- terpineol
1024.70  zingiberene

M. D’Alpaos, P. Traldi, G. Tassinato and P. Pallado, Extraction of essential oils and flavors with classic and supercritical techniques: a comparison. Rivista Ital. EPPOS (Numero Speciale – Agosto), 200-207 (1997).

P&F 25, No. 2, 46, (2000)

zingiber officinale oil CO2 extract australia
In 1994, Bartley and Foley analyzed the chemical composition of a supercritical fluid extract of Australian-grown ginger. The freshly harvested roots were peeled and chopped into 2 mm cubes before grinding under liquid nitrogen. The pulp was mixed with coarse granulated Celite (diatomaceous earth) and subjected to extraction by supercritical CO2. The analysis was preformed by a combination of capillary GC (for retention indices and quantitative data) and GC/MS (for component identification confirmation). The compounds identified were:
#%LeftshiftComponents
320.20 aromadendrenol
2310.83alpha- bergamolene
242.73beta- bisabolene
290.14alpha- bisabolol
110.60  borneol
160.10iso bornyl acetate
250.14gamma- cadinene
43.71  camphene
92.991,8- cineole
213.25ar- curcumene
120.11  decanal
280.22  dodecatrienol
190.20beta- elemene
180.23delta- elemene
270.25  elemol
200.18beta- farnesene
1525.06  geranial
140.66  geraniol
170.12  geranyl acetate
10.52  hexanal
70.43  limonene
100.46  linalool
20.113- methyl hexanol
60.53  myrcene
132.87  neral
350.086- paradol
340.20 pentenyl curcumene
81.63beta- phellandrene
268.18beta-sesqui phellandrene
50.08beta- pinene
300.22(Z)-sesqui sabinene hydrate
360.316- shogaol
30.93alpha- thujene
310.15 zingerenol
2225.87  zingiberene
330.64 zongerone

J. P. Bartley and P. Foley, Supercritical fluid extraction of Australian grown ginger (Zingibar officinale), J. Sci. Food Agric., 66, 365-371 (1994).

P&F 22, No. 5, 71, (1997)

zingiber officinale var. gigante root oil brazil
#%LeftshiftComponents
220.50  aromadendrene
254.70beta- bisabolene
150.70  borneol
35.70  camphene
140.30  citronellal
171.00  citronellol
190.50alpha- copaene
237.90ar- curcumene
80.20para- cymene
210.90beta- elemene
267.40alpha- farnesene
189.60 geraniol + geranial
200.50  geranyl acetate
10.402- heptanol
101.60  limonene
120.70  linalool
50.506- methyl-5-hepten-2-one
61.30  myrcene
165.40  neral
130.302- nonanol
70.60alpha- phellandrene
277.00beta-sesqui phellandrene
98.40beta-phellandrene + 1,8-cineole
22.30alpha- pinene
40.40beta- pinene
110.50  terpinolene
2419.00  zingiberene

P&F 25, No. 2, 46, (2000)

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