BT

Typical G.C. analysis

boronia megastigma nees absolute
#%LeftshiftComponents
380.102-acetoxylinalool A + tridecane + methyl 2-methoxybenzoate
580.02 acetvanillone + (E)-beta-farnesene
320.45(E)-anethole + safrol + nonanoic acid
87trace apiole
48.015 benzyl 3-methyl butyrate + (Z)-retro-gamma-ionone
40.01  benzyl alcohol
970.06  benzyl benzoate
880.20beta-bisabolol + tetradecanol
340.10isobornyl acetate + menthyl acetate
400.02trans-carvyl acetate + (E)-linalool
540.04beta- caryophyllene
730.09  caryophyllene oxide
120.01  chrysanthenone
651.20sesqui cineole
86trace  coniferyl methyl ether
410.07 cyclic beta-ionone
470.03 decanoic acid + benzyl 2-methyl butyrate + (Z)-retro-gamma-ionone
220.012- decanol
310.06 decanol + 5-hydroxylinalool B + methyl 2-isobutyroxy-3-methyl valerate
210.602-decanone + 7-hydroxyhotrienol
570.657,8-dihydro-beta-ionol + (Z)-retro-alpha-ionone
551.307,8- dihydro-beta-ionone
630.06 dihydroactinodiolide + undecyl acetate
230.01 dodecane + lilac alcohol
500.042- dodecanol
763.80 dodecyl acetate + 8-hydroxylinalyl isobutyrate
108trace  eicosane
420.01delta- elemene
700.097,11-epoxymegastigm-5(6)-en-9-one
490.01  ethyl decanoate
950.08(E,E)- farnesol
28trace  geraniol
460.70 geranyl acetate + vanillin
56trace  geranyl acetone
1114.30(E)-4-(geranyl oxy) cinnamic acid
1061.90(Z)-4-(geranyl oxy) cinnamic acid
90.02  guaiacol
940.70  heptadecane
770.04  hexadecane
590.03alpha- humulene
750.03  humulene oxide I
850.303- hydroxy-beta-ionone
430.208- hydroxylinalool
910.108-hydroxylinalyl 2-methyl butyrate
1132.208-hydroxylinalyl decanoate
1160.308-hydroxylinalyl dodecanoate
1050.308-hydroxylinalyl heptanoate
1091.808-hydroxylinalyl heptanoate
920.108-hydroxylinalyl isovalerate
1120.708-hydroxylinalyl nonanoate
690.208-hydroxylinalyl propionate
990.308-hydroxylinalyl tiglate
1181.408-hydroxylinalyl tridecanoate
980.098-hydroxylinalyl valerate
802.40(E)-3-hydroxymegastigm-7-en-9-one
680.03(Z)-3-hydroxymegastigm-7-en-9-one
1070.09N-(2-(4-hydroxyphenyl)ethyl) 2-methyl butyramide
1100.20N-(2-(4-hydroxyphenyl)ethyl) tiglamide
1159.30N-(2-(4-hydroxyphenyl)ethyl) tiglamide + methyl (Z)-4-(geranyl oxy) cinnamate
840.154-oxo-beta- ionol
520.30beta-ionol + 4,5-epoxy-gamma-homocyclocitral
710.64(E,E)-pseudo- ionone
450.05(Z)-alpha-ionone + (Z)-carvyl acetate
530.04(E)-alpha-ionone + 2,6-dimethyl-4-methyl phenol
6114.90(E)-beta-ionone + alpha-curcumene + 5,6-epoxy-beta-ionone
670.02  italicene ether
820.35delta-jasmonic acid lactone (syn) + 4-hydroxy-beta-ionone
890.70delta-jasmonic acid lactone )anti) + methyl curcubate
50.45  limonene
290.20 linalyl acetate + 5-hydroxylinalool A
740.30(E)-megastigm-7-en-3,9-dione
140.15para-mentha-1,3,8-triene + camphor
30.06para- mentha-1,5,8-triene
1176.70 methyl (E)-4-(geranyl oxy) cinnamate
960.50  methyl (E)-4-hydroxycinnamate
830.70  methyl (Z)-epi-jasmonate
791.20 methyl (Z)-jasmonate + (E)-3-hydroxymegastigm-7-en-9-one
10.10 methyl 1-hydroxy-3-methyl valerate + beta-pinene
440.20 methyl 2-(2-methyl butyoxy)-3-methyl valerate + neryl acetate
150.06 methyl 2-acetoxy-3-methyl valerate
810.70 methyl 2,3-di-epi-curcubate + 4-oxo-beta-ionone
9014.60 methyl 3-epi-curcubate + (Z)-8-heptadecene
18tracepara- methyl acetophenone
240.01  methyl nonanoate
130.01  methyl octanoate
1040.02  methyl palmitate
20.40 myrcene + octanal
250.20 nerol + (E)-tagetenone
1030.08  nonadecane
100.75 nonanal + linalool + hotrienol + 2-phenethyl alcohol
19trace  nonanol
110.082- nonanol
70.07(E)-beta- ocimene
60.02(Z)-beta- ocimene
1010.03  octadecane
200.07  octanoic acid
80.03  octanol
640.16 pentadecane + isoitalicene ether
102trace  pentadecyl acetate
620.05endoperoxide of cyclic beta-ionone
660.02beta-sesqui phellandrene
30traceisopiperitenone + geranial
270.01  piperitone
720.55 spathulenol + (E)-9-hydroxymegastigm-7-en-3-one
780.09 syringl methyl ether + zingerone
260.30(Z)-tagetenone + anisaldehyde
160.02(E)- tagetone
170.03(Z)- tagetone
35trace  terpinen-4-yl acetate
510.02  tetradecane
1000.50  tetradecyl acetate
370.03 theaspirane A + 2-undecanol
392.40 theaspirane B + 2-acetoxylinalool B + methyl decanoate
1140.03  tricosane
930.15  tridecyl acetate
360.05  undecanal
601.00 undecanoic acid + 8-hydroxyl linalyl acetate + dodecanol + 2-phenethyl isovalerate + benzyl tiglate
330.052-undecanone + bornyl acetate

P. Weyerstahl, H. Marschall, W-R. Bork, R. Rilk, S. Schneider and H-C. Wahlburg, Constituents of the absolute of Boronia megastigma Nees from Tasmania. Flav. Fragr. J., 10, 297-311 (1995).

P&F 24, No. 1, 53, (1999)

cistus oil
#%LeftshiftComponents
60.1  acetophenone
1410.26- acetoxy-11-nor-drim-7-en-9-one
720.27- acetyl-2,2,6-trimethyl bicyclo(4.2.0)octane
1190.16-acetyl-5,8,8-trimethyl bicyclo(3.2.1)octan-2,3-dione
1490.213-nor- ambreinolide
1480.18-epi-13-nor- ambreinolide
780.2alpha- ambrinol
1371.4  ambrox
1440.16-oxo-isoambrox
810.9  aromadendr-1-ene
1350.3  aromadendr-1(10)-en-9-one
911.41,5-(Z)-aromadendr-9-ene
1320.11,10-seco- aromadendran-1,10-dione
1300.15-epi-1,10-seco- aromadendran-1,10-dione
861.5allo- aromadendrene
b30.4  benzoic acid
272.0  borneol
551.7  bornyl acetate
b210.93-iso butenyl-5-methyl-5-vinyl butyrolactone
1260.5  cadalene
980.4delta- cadinene
1250.6alpha- cadinol
1000.6alpha- calacorene
990.6(E)- calamenene
900.5(Z)- calamenene
b91.4gamma-campholenic acid
150.3alpha- campholenic aldehyde
100.3gamma- campholenic aldehyde
b70.3alpha-campholytic acid
b40.2gamma-campholytic acid
b52.4 camphonanic acid
b122.1alpha-camphoneic acid
180.1  camphor
600.8  carvacrol
480.2  carvenone
410.2trans- carveol
430.1cis- carveol
460.5  carvone
1380.1sesqui chamaenol
1171.8  copaborneol
1270.6  copabornyl acetate
741.1alpha- copaene
820.7  cubeb-11-ene
1134.1  cubeban-11-ol
1210.41-epi- cubenol
440.1  cuminaldehyde
b111.0beta- cyclogeranic acid
b80.9gamma-cyclogeranic acid
530.3para- cymen-7-ol
30.4para- cymene
b130.7 davanic acid
390.2  decanal
b203.8  decanoic acid
1060.21,2- dehydroglobulol
1180.33,4- dehydroglobulol
1100.21-epi-3,4- dehydroviridiflorol
1041.41,2- dehydroviridiflorol
1460.214,15- di-nor-8,13-epoxylabd-12-ene
790.1  dihydro-beta-ionene
940.2  dihydroactinidiolide
370.5neo dihydrocarveol
b156.5  dihydrocinnamic acid
b241.7 dimethyl (Z)-2-hexyl-3-methyl butendioic acid
490.22,4- dimethyl acetophenone
91.0alpha-para- dimethyl styrene
970.24,7- dimethyl tetral-1-one
b141.22,6- dimethyl-5-oxoheptanoic acid
770.2  dodecanal
700.111-nor- drim-7-ene
1390.1  drim-8-en-7-one
690.211-nor- drim-8-ene
1010.311-nor- driman-8-ol
1020.2beta- elemol
351.3  elsholtzia ketone
1360.25,11- epoxycadin-1(10)-en-9-ol
1080.85,11-epoxycadin-1(10)-ene
80.86,8- epoxymenth-1-ene
640.1  ethyl dihydrocinnamate
1240.4beta- eudesmol
1220.2gamma- eudesmol
651.6  eugenol
450.2alpha- fenchyl acetate
760.11-( fur-2-yl methyl)-2-formyl pyrrole
b192.4  geranic acid
510.2  geraniol
800.1  geranyl acetone
1090.5  gleenol
1110.2  globulol
b20.5  heptanoic acid
b10.7  hexanoic acid
1330.1(Z)-3-hexen-1-yl dihydrocinnamate
1340.3  hexyl dihydrocinnamate
590.1(2E,4E)-6-hydroxy-2,6-dimethyl hepta-2,4-dienal
32trace2- hydroxy-3-methyl benzaldehyde
660.22- hydroxy-4-isopropenyl toluene
680.2(E)-5-hydroxy-para-mentha-1(6),8-dien-2-one
710.3(Z)-5-hydroxy-para-mentha-1(6),8-dien-2-one
1400.110- hydroxycalamene-8,9-epoxide
1310.19- hydroxyladanifer-10-one(9(10(1))-abeo-9-hydroxyaromadendran-10-one)
500.42- hydroxypinan-3-one
870.2(E)-beta- ionone
1420.615-nor-labd-1(17)-ene
1530.4  labd-7-en-15-ol
1450.515-nor- labd-7-ene
b316.3 labd-7-enoic acid
1540.3  labd-8-en-15-ol
1430.515-nor-labd-8-ene
b324.0 labd-8-enoic acid
1520.4  labd-8(17)-en-15-ol
b305.1 labd-8(17)-enoic acid
1470.715-nor-labdan-8-ol
b232.5  lauric acid
929.3  ledene
730.2iso ledene
1161.3  ledol
120.2  linalool
70.4(E)- linalool oxide furanoid
110.2(Z)- linalool oxide furanoid
b281.0  linoleic acid
1500.3  manoyl oxide
1510.313-epi- manoyl oxide
850.1  massoia lactone
400.3(Z)-para- menth-4(8)-en-2-ol
620.12- methoxy-6-methyl acetophenone
290.3para- methyl acetophenone
521.0  methyl dihydrocinnamate
750.4  methyl eugenol
10.25- methyl furfural
20.16- methyl-5-hepten-2-one
1200.3  muurola-4,10(14)-dien-1-ol
1230.3alpha- muurolol
b252.7  myristic acid
330.9  myrtenal
b186.0  myrtenic acid
361.5  myrtenol
581.1  naginata ketone
220.2  nerol oxide
1030.2(E)- nerolidol
130.1  nonanal
b101.6  nonanoic acid
170.7(E)-3- nonen-2-one
b63.7  octanoic acid
b271.2  oleic acid
1150.1beta- oplopenone
b265.1  palmitic acid
1051.2  palustrol
1290.1  pentadecanal
420.13- phenyl propanol
231.5  pinocamphone
280.7iso pinocamphone
191.8trans- pinocarveol
240.3  pinocarvone
630.4trans- pinocarvyl acetate
470.8  piperitone
250.1  propiophenone
1280.24-iso propyl-6-methyl tetral-1-one
160.1(E)- rose oxide
140.2(Z)- rose oxide
200.1(E)- sabinol
b290.8  stearic acid
210.2(E)- tagetone
260.2(Z)- tagetone
310.8  terpinen-4-ol
340.5alpha- terpineol
1140.1  tetradecanal
890.61,1,5,6- tetramethyl-1,2-dihydronaphthalene
950.21,1,5,6- tetramethyl-1,2,3,4-tetrahydronaphthalene
540.2  thymol
1070.26-para-tolyl heptan-2-one
880.1  tridecanal
b160.71,5,5-trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid A
b171.91,5,5-trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid B
50.32,2,6- trimethyl cyclohex-2-enone
41.32,2,6- trimethyl cyclohexanone
930.21-(1,2,2- trimethyl cyclopent-1-yl) pentan-1,4-dione
960.26,6,10-trimethyl decan-2-one
300.52,2,5- trimethyl oxepan-4-one
670.21,1,6- trimethyl-1,2-dihydronaphthalene
830.14,4,7a- trimethyl-1,4,5,6,7,7a-hexahydro-2H-inden-2-one
840.1  tuberolactone
610.2  undecanal
b220.3  undecanoic acid
380.3  verbenone
1124.3  viridiflorol
560.2  vitispirane A
570.1  vitispirane B

P. Weyerstahl, H. Marschall, M. Weirauch, K. Thefeld and H. Surburg, Constituents of commercial labdanum oil. Flav. Fragr. J., 13, 295-318 (1998).

P&F 24, No. 4, 31, (1999)

tagetes minuta flower oil
#%LeftshiftComponents
150.71beta- caryophyllene
200.27  caryophyllene oxide
647.05  dihydrotagetone
180.37gamma- elemene
210.21gamma- eudesmol
130.17  eugenol
120.18  geraniol
170.10  germacrene D
160.35alpha- humulene
45.00  limonene
30.10  myrcene
521.10(E)-beta- ocimene
140.37beta- patchoulene
190.142- phenethyl tiglate
10.12alpha- pinene
20.86  sabinene
111.13(E)- tagetenone
101.42(Z)- tagetenone
87.49(E)- tagetone
70.95(Z)- tagetone
90.17  terpinen-4-ol

B. Benveniste and N. Azzo,Tagette oil, Technical Bulletin & Newsletter, Vol. IV, Kato Worldwide Ltd., N.Y, (October 1, 1992).

P&F 21, No. 5, 57, (1996)

tagetes minuta flower oil CO2 extract
#%LeftshiftComponents
543.56 alchenenotriol
309.98(E)- anethole
272.10para- anisaldehyde
410.33  aromadendrene
470.08beta- bisabolene
480.12gamma- cadinene
140.11  camphor
240.23cis- carveol
403.44beta- caryophyllene
230.61  citronellol
21.12para- cymene
311.51 dehydroelshotzia ketone
200.12(Z)- dihydrocarvone
65.19  dihydrotagetone
90.22alpha-para- dimethyl styrene
333.00delta- elemene
500.11gamma-elemene (furanoid)
210.15  elsholtzia ketone
490.15  eugenyl acetate
370.28  geranyl acetate
530.28  guaiol
422.14alpha- humulene
510.29  ledol
315.14  limonene
111.03  linalool
80.43(Z)- linalool oxide furanoid
280.47  linalyl acetate
100.12(E)-para- menth-2-en-1-ol
290.39  methyl citronellate
390.24  methyl eugenol
430.226-methyl-gamma-ionone
450.29alpha- muurolene
10.24  myrcene
340.19  neryl acetate
50.30(E)-beta- ocimene
419.33(Z)-beta- ocimene
360.10beta- patchoulene
460.13  pentadecane
170.30(Z)- pinanone
133.68(Z)- sabinene hydrate
350.32(E)-iso safrole
522.42  spathulenol
260.65(E)- tagetenone
2513.26(Z)- tagetenone
152.81(E)- tagetone
160.34(Z)- tagetone
180.46  terpinen-4-ol
70.26gamma- terpinene
190.50alpha- terpineol
380.16  tetradecane
120.24alpha- thujone
320.12  tridecane
440.57  valencene
220.05  verbenone

J. Daghero, M. Mattea, E. Reverchon, G. Della Porta and F. Senatore, Isolation of Tagetes minuta L. oil using supercritical CO2 extraction. In: Proceedings WOCMAP-2. Edits., V. Martino, A. Bandoni, G. Bleak and N. Capelle, Acta Hort., 503, 21-25 (1999).

P&F 25, No. 6, 32, (2000)

tagetes minuta flower oil rwanda
#%LeftshiftComponents
10.63  acetone
280.06  artemisyl ketone
33trace  bornyl acetate
34traceiso bornyl acetate
8trace  camphene
100.11delta-3- carene
160.041,8- cineole
21tracepara- cymene
221.03  dihydrotagetone
250.163,4- dimethyl octa-2,4,6-triene
70.02  ethyl 2-methyl butyrate
60.12  ethyl butyrate
150.032- hexenal
260.14(Z)-3- hexen-1-ol
141.77  limonene
320.17  linalool
230.54para- menth-4-en-3-one
20.034- methyl-2-pentanone
11trace1- methyl-3-isopropyl cyclohexane
130.11  myrcene
200.17(E)-beta- ocimene
1737.08(Z)-beta- ocimene
29trace(Z)-beta-ocimene epoxide
120.07alpha- phellandrene
360.082(10)-pinen-4-one
40.03alpha- pinene
90.28  sabinene
30.05  santene
386.31(E)- tagetenone
373.34(Z)- tagetenone
302.86(E)- tagetone
3135.40(Z)- tagetone
350.07  terpinen-4-ol
19tracegamma- terpinene
180.35  terpinolene
5tracealpha- thujene
270.022,4,6- trimethyl anisole
24trace1,7,7- trimethyl bicyclo(3.1.1)heptan-2-one

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

#%LeftshiftComponents
1trace  acetone
220.30  artemisyl ketone
27trace  bornyl acetate
28traceiso bornyl acetate
7trace  camphene
11tracedelta-3- carene
16trace1,8- cineole
190.30para- cymene
203.30  dihydrotagetone
6trace  ethyl 2-methyl butyrate
8trace  ethyl valerate
15trace2- hexenal
210.50(Z)-3- hexen-1-ol
141.30  limonene
26trace  linalool
13trace  myrcene
18trace(E)-beta- ocimene
1731.80(Z)-beta- ocimene
230.30(Z)-beta-ocimene epoxide
12tracealpha- phellandrene
3tracealpha- pinene
9tracebeta- pinene
50.50  propyl butyrate
100.30  sabinene
2trace  santene
301.80(E)- tagetenone
316.00(Z)- tagetenone
243.40(E)- tagetone
2546.00(Z)- tagetone
290.30  terpinen-4-ol
4tracealpha- thujene

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

tagetes minuta flower oil turkey
#%LeftshiftComponents
210.10  bicyclogermacrene
180.47beta- caryophyllene
160.12  decanal
1330.30  dihydrotagetone
20.08  ethyl 2-methyl butyrate
90.06(E)-2- hexenal
77.24  limonene
40.10  myrcene
120.39(E)-beta- ocimene
1028.49(Z)-beta- ocimene
140.32allo- ocimene
50.09alpha- phellandrene
80.07beta- phellandrene
10.06alpha- pinene
220.26iso piperitenone
30.96  sabinene
2015.35(E)- tagetenone
191.87(Z)- tagetenone
174.80(E)- tagetone
150.25(Z)- tagetone
60.02alpha- terpinene
110.05gamma- terpinene

K. H. C. Baser and H. Malyer, Essential oil of Tagetes minuta L. from Turkey. J. Essent. Oil Res., 8, 337-338 (1996).

P&F 25, No. 6, 32, (2000)

tagetes minuta flower oil zambia
#%LeftshiftComponents
100.80cis- carvyl acetate
82.20iso caryophyllene
430.00  dihydrotagetone
90.50  germacrene B
18.30  limonene
70.50  linalool
30.40(E)-beta- ocimene
223.60(Z)-beta- ocimene
56.30(E)- tagetone
614.10(Z)- tagetone

E. H. Chisowa, D. R. Hall and D. L. Farman, Chemical composition of the essential oil of Tagetes minuta L. from Zambia. J. Essent. Oil Res., 10, 183-184 (1998).

P&F 25, No. 6, 32, (2000)

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