BT

Typical G.C. analysis

chenopodium ambrosioides oil spain
#%LeftshiftComponents
 0.04  allyl levulinate
 0.02allo- aromadendrene
 0.22iso borneol
 0.20iso bornyl acetate
 0.02nor bornyl acetate
 0.06iso bornyl propionate
 0.08delta- cadinene
 0.84  camphor
 2.28trans- carveol
 4.91cis- carveol
 2.07  carvone
 0.16  carvone oxide
 2.09beta- caryophyllene
 0.04beta- copaene
 0.03para- cymene
 0.71  dihydrocarveol
 5.00  geranial
 0.04  geranic acid
 4.30  geraniol
 0.24alpha- guaiene
 0.02  lavandulyl acetate
 32.50  limonene
 0.07  linalool
 0.21(Z)- linalool oxide furanoid
 4.00(Z)-para-mentha-2,8-dien-1-ol
 1.64  menthol
 0.03 methyl undecanal
 0.03  myrcene
 0.41  nerol
 0.01  neryl acetate
 0.02  neryl formate
 0.15  perillyl alcohol
 0.01alpha- phellandrene
 0.09alpha- pinene
 0.06beta- pinene
 26.70trans- pinocarveol
 3.54iso pulegol
 0.08iso pulegyl acetate
 0.06(E)- sabinene hydrate
 0.83alpha- terpinene
 0.03gamma- terpinene
 0.26alpha- thujene
 0.14  undecanal
 1.21(E)- verbenol
coriandrum sativum fruit oil CO2 extract
#%LeftshiftComponents
120.07  borneol
11.20  camphene
90.30beta- caryophyllene
40.301,8- cineole
71.20  decanal
140.40  geraniol
34.70  limonene
860.10 linalool + camphor
100.70  menthol
61.00  menthone
130.06  nerol
21.10beta- pinene
520.05gamma-terpinene + alpha-terpinene
110.23alpha- terpineol

A. S. Reis Machado, E. Gomes de Azevedo, M. Nunes da Ponte and R. M. A. Sardinha, High pressure carbon dioxide extraction from coriander plants. Headspace analysis. J. Essent. Oil Res., 5, 645-649 (1993).

P&F 22, No. 1, 49, (1997)

foeniculum vulgare mill. var. dulce d.c. oil italy
#%LeftshiftComponents
1987.08(E)- anethole
183.47(Z)- anethole
2trace  camphene
140.04  camphor
90.371,8- cineole
70.12para- cymene
122.12  fenchone
84.70  limonene
13trace  linalool
16trace  menthol
15trace  menthone
50.17  myrcene
11trace(E)-beta- ocimene
10trace(Z)-beta- ocimene
6tracealpha- phellandrene
10.25alpha- pinene
4tracebeta- pinene
3trace  sabinene
17trace  terpinen-4-ol

R. Piccaglia and M. Marotti, Characterization of several aromatic plants grown in Northern Italy. Flav. Fragr. J., 8, 115-122 (1993).

P&F 19, No. 1, 31, (1994)

heracleum candolleanum rhizome oil india
#%LeftshiftComponents
218.60  bornylene
150.20trans- carveol
121.20  citronellyl acetate
160.40para- cymen-8-ol
49.00para- cymene
63.00  decanal
133.20  dodecanal
147.90  heptyl hexanoate
70.30  heptyl isobutyrate
100.40  hexyl hexanoate
80.70  linalool
110.70  menthol
94.40  octanol
511.90  octyl acetate
118.90alpha- pinene
34.60gamma- terpinene
J. of Ess. Oil Res. 13, No. 2, 80, (2001)
melissa officinalis var. citra oil slovak republic
#%LeftshiftComponents
240.06beta- bourbonene
294.20beta- caryophyllene
388.35  caryophyllene oxide
80.141,8- cineole
2211.31  citronellal
230.67alpha- copaene
200.26alpha- cubebene
20.082,5- diethyl tetrahydrofuran
3433.60  geranial
391.05  geranic acid
375.89  geranyl acetate
42trace  heptacosane
30.05 hexenal
310.13alpha- humulene
70.11  limonene
250.08  linalool
170.24  linalool oxide
300.12  menthol
180.60  menthone
210.42iso menthone
280.27  menthyl acetate
330.36  methyl geranate
130.316- methyl-5-hepten-2-one
360.14alpha- muurolene
350.26gamma- muurolene
60.12  myrcene
400.80  myristic acid
3222.18  neral
100.26  ocimene
12trace2,3- octane dione
160.123- octanol
90.123- octanone
4trace1,3,5- octatriene
190.251- octen-3-ol
110.184- octen-3-one
411.01  palmitic acid
10.15alpha- pinene
50.14beta- pinene
260.07isopulegol 1
270.06isopulegol 2
140.12 rose oxide 1
150.07 rose oxide 2

M. Holla, E. Svajdlenka, J. Tekel, S. Vaverkova and E. Havranek, Composition of the essential oil from Melissa officinalis L. cultivated in Slovak Republic. J. Essent. Oil Res., 9, 481-484 (1997).

P&F 24, No. 3, 47, (1999)

mentha arvensis leaf oil india
#%LeftshiftComponents
10.02  acetic acid
400.05  carvone
490.29  caryophyllene oxide
160.251,8- cineole
350.10  citronellol
290.03para- cymen-8-ol
140.02para- cymene
420.03  decanol
40.03(Z)-3- hexen-1-ol
360.28(Z)-3- hexen-1-yl 3-methyl butyrate
110.04(Z)-3- hexen-1-yl acetate
370.03  hexyl 3-methyl butyrate
150.39  limonene
200.03  linalool
460.03para- menth-8-ene-1,2-diol
2774.51  menthol
280.05iso menthol
300.12neo menthol
248.30  menthone
264.59iso menthone
446.11  menthyl acetate
380.23iso menthyl acetate
450.12neo menthyl acetate
430.16neoiso menthyl acetate
20.083- methyl butanol
210.033- methyl butyl 3-methyl butyrate
6trace3- methyl cyclohexanol
7trace3- methyl cyclohexanone
130.02  methyl octyl ether
30.023- methyl-2-cyclopenten-1-one
330.04 myrtenal + myrtenol
480.02  nerolidol
250.09  nonanol
190.043- nonanol
170.06  octanol
100.963- octanol
320.11  octyl acetate
220.043- octyl acetate
120.02alpha- phellandrene
50.15alpha- pinene
90.24beta-pinene + 3-octanone
410.45  piperitone
390.13  pulegone
80.06  sabinene
180.02  sabinene hydrate
470.06 terpin hydrate
310.07alpha- terpineol
230.01beta- terpineol
340.03  verbenone

M. H. Boelens, Chemical characterization of cornmint oil, Perf. & Flav., 18(5), 27-32 (1993).

P&F 19, No. 6, 57, (1994)

mentha longifolia oil
#%LeftshiftComponents
17traceiso amyl isovalerate
360.30delta- cadinene
35tracegamma- cadinene
300.20beta- caryophyllene
110.601,8- cineole
230.10  cuminaldehyde
210.50para- cymen-8-ol
15tracepara- cymenene
320.10beta- farnesene
330.10  geranyl propionate
340.30  germacrene D
4trace  hexanol
10.20(E)-2- hexenal
20.20(Z)-3- hexen-1-ol
3trace2- hexen-1-ol
310.10alpha- humulene
260.204- hydroxypiperitone
101.00  limonene
16trace  linalool
18trace  menthol
80.20  myrcene
90.103- octanol
13trace2- octen-1-ol
70.10beta- pinene
270.20  piperitenone
250.50iso piperitenone
2883.70  piperitenone oxide
291.00isopiperitenone oxide
248.10  piperitone oxide
60.10  sabinene
14trace(Z)- sabinene hydrate
20trace  terpinen-4-ol
120.10gamma- terpinene
221.10alpha- terpineol
190.20delta- terpineol
50.10  tricyclene
J. of Ess. Oil Res. 12, No. 5, 530, (2000)
mentha pulegium oil cuba
#%LeftshiftComponents
270.10beta- bourbonene
300.18delta- cadinene
250.09alpha- calacorene
282.49beta- caryophyllene
311.04  caryophyllene oxide
60.08para- cymene
260.39beta- damascenone
336.78  hexadecanoic acid
290.27alpha- humulene
71.13  limonene
90.77  linalool
150.16  menthol
160.30iso menthol
131.86neo menthol
1420.68neoiso menthol
106.29  menthone
119.73iso menthone
200.14iso menthyl acetate
230.28neo menthyl acetate
226.24neoiso menthyl acetate
50.06  myrcene
80.11(Z)-beta- ocimene
40.413- octanol
10.35alpha- pinene
30.38beta- pinene
242.39  piperitenone
191.02  piperitone
1825.14  pulegone
20.11  sabinene
170.29alpha- terpineol
320.56  tetradecanoic acid
213.03  thymol
120.74  umbellulone

J. Pino, A. R.sado and V. Fluentes, Chemical composition of the essential oil of Mentha puiegium L. from Cuba. J. Essent. Oil. Res., 8, 295-296 (1996).

P&F 23, No. 3, 63, (1998)

mentha pulegium oil uruguay
#%LeftshiftComponents
130.20-2.20  carvone
100.90-1.40beta- caryophyllene
5trace-0.101,8- cineole
40.20  limonene
110.50-3.60  menthol
91.60-4.20neo menthol
74.20-5.60  menthone
835.60-40.60iso menthone
60.20-1.503- octanol
3tracealpha- phellandrene
1trace-0.40alpha- pinene
2tracebeta- pinene
1226.8-41.10  pulegone

M. B. de Grosso and P. Moyna. Cmposicion quimica de las esencias de Mentha del Uruguayrmias de Ment. An. Real. Acad. Farm., 51, 333-338 (1985).

P&F 23, No. 3, 63, (1998)

mentha x piperita herb oil idaho
Kubeczka (1993) compared the chemical compositions of peppermint oil produced from two different regions in the United States with the composition of an oil noted as Mitcham oil (origin unknown). His results are shown in Table VI. Note: Only the Peppermint Oil from Michigan analysis will be shown here:
#%LeftshiftComponents
20.01  camphene
222.24beta- caryophyllene
87.021,8-cineole + beta-phellandrene
120.24para- cymene
271.27  germacrene D
72.44  limonene
190.31  linalool
172.48  menthofuran
2438.01  menthol
213.25neo menthol
1623.14  menthone
183.08iso menthone
203.69  menthyl acetate
50.33  myrcene
90.41(Z)-beta- ocimene
110.11(Z)-beta- ocimene
140.303- octanol
11.34alpha- pinene
31.65beta- pinene
280.46  piperitone
230.78iso(iso) pulegol
251.38  pulegone
40.77  sabinene
151.14(E)- sabinene hydrate
60.43alpha- terpinene
100.68gamma- terpinene
260.15alpha- terpineol
130.18  terpinolene
290.15  viridiflorol

K. H. Kubeczka, Moglichkeiten und grenzen der qualitatsbeurteilung arzneilich verwendeter atherischer Ole. In: Atherische Ole-anspruch und wirklichkeit. Edit., R. Carle, pp. 85-102, Wissenschaft, Verlag. mbh Stuttgart (1993).

P&F 22, No. 4, 57, (1997)

mentha x piperita oil CO2 extract
Reverchon et al. (1994) compared the composition of a supercritical CO2 extract (SFE) of peppermint under two separate sets of conditions with a sample of peppermint oil produced by hydrodistillation. The results of the GC/MS analyses of the volatile concentrates of peppermint oil and peppermint produced by SFE can be seen in Table VIII. Note: Only the SFE-2 (T:40C, P:120 bar) will be shown as follows:
#%LeftshiftComponents
180.20  bornyl acetate
220.70beta- bourbonene
295.00gamma- cadinene
330.60T- cadinol
310.40(E)- calamenene
244.30beta- caryophyllene
320.20  caryophyllene oxide
63.601,8- cineole
21tracealpha- cubebene
50.10  decane
130.20  dihydrocarveol
230.90beta- elemene
300.40gamma- elemene
270.60beta- farnesene
250.20beta- gurjunene
26tracealpha- humulene
160.60  linalyl acetate
80.40para-menth-2-en-1-ol
1123.80  menthol
120.20iso menthol
936.10  menthone
107.50iso menthone
1911.70  menthyl acetate
200.20iso menthyl acetate
170.20neo menthyl acetate
28tracegamma- muurolene
30.20  myrcene
70.20(Z)-beta- ocimene
40.103- octanol
10.20alpha- pinene
20.50beta- pinene
150.60  piperitone
140.30  pulegone

E. Reverchon, A. Ambruosi and F. Senatore, Isolation of peppermint oil using ssupercritical CO2 extraction. Flav. Fragr. J., 9, 19-23 (1994).

P&F 22, No. 4, 57, (1997)

mentha x piperita oil mongolia
#%LeftshiftComponents
290.05  borneol
160.31beta-bourbonene + benzaldehyde
330.16delta- cadinene
170.42  camphor
320.16  carvone
32.471,8- cineole
40.22para- cymene
340.05  geraniol
300.05  germacrene D
130.06(Z)-3- hexen-1-yl isovalerate
270.18alpha- humulene
350.04(Z)- jasmone
20.38  limonene
180.28  linalool
10trace(Z)- linalool oxide furanoid
140.07  menthofuran
2535.07  menthol
213.74neo menthol
240.39neoiso menthol
1132.22  menthone
155.43iso menthone
209.39  menthyl acetate
50.072- methyl butyl 2-methyl butyrate
60.082- methyl butyl isovalerate
360.06(Z)- nerolidol
80.213- octanol
90.301- octen-3-ol
70.073- octyl acetate
10.04beta- pinene
311.32  piperitone
260.22  pulegone
230.05  rosefuran oxide
12trace(E)- sabinene hydrate
190.24(Z)- sabinene hydrate
220.07  terpinen-4-ol
280.06alpha- terpineol
370.09  viridiflorol

D. Karasawa, S. Shatar, A. Erdenechimeg, Y. Okamoto, H. Tateha and S, Shimizu, A study on Mongolian mints. A new chemotype from Mentha asiatia Borriss and constituents of M. arvensis L. and M. piperita L. J. Essent. Oil. Res., 7, 255-260 (1995).

P&F 22, No. 4, 57, (1997)

mentha x piperita oil russia
#%LeftshiftComponents
40.171,8- cineole
30.68  limonene
1044.46  menthol
92.00neo menthol
616.77  menthone
723.45iso menthone
83.75  menthyl acetate
10.80alpha- pinene
20.69beta- pinene
121.08 piperitone + piperitenone
110.99  pulegone
52.29(E)- sabinene hydrate

E. B. Kirichenko, L-D. Ky and V. A. Mel’nikov, Essential oil composition of some Vietnanese mint varieties. Byull. GI, Bot. sada, 154, 56-69 (1989).

P&F 22, No. 4, 57, (1997)

michelia alba flower absolute
Headspace
#%LeftshiftComponents
10.50  methyl isobutyrate
29.71  methyl butyrate
343.59  methyl valerate
40.133-methoxy-3-methyl-2-butanone
50.13  methyl 2-methyl butyrate
60.02  ethyl benzene
70.052- methyl pentanol
80.55  methyl 4-methyl valerate
90.01alpha- thujene
100.17alpha- pinene
110.05  camphene
120.02  benzaldehyde
130.05  sabinene
140.17beta- pinene
150.02para- menth-3-ene
160.58  myrcene
170.34alpha- phellandrene
180.01gamma- terpinene
191.49para- cymene
200.87  limonene
210.091,8- cineole
220.13  terpinolene
230.67delta-3- carene
240.11  methyl benzoate
250.05  linalool
260.392- phenethyl alcohol
270.02  menthol
280.07  nerol
290.018-vvvvvmethyl-5-ethyl-6,8-nonadien-2-one
300.02  indole
310.14  benzofuran
320.01beta- caryophyllene
330.012- phenethyl isovalerate
340.22beta- cubebene
ocimum basilicum herb oil poland
#%LeftshiftComponents
212.18alpha- bergamolene
310.13  bicyclogermacrene
200.67  bornyl acetate
180.70beta- bourbonene
390.52delta- cadinol
2trace  camphene
50.11delta-3- carene
251.42beta- caryophyllene
90.721,8- cineole
350.11  citronellol
170.37alpha- copaene
340.04ar- curcumene
120.02para- cymene
220.86beta- elemene
380.62  eugenol
360.02  geraniol
330.05  geranyl acetate
305.07  germacrene D
270.78alpha- humulene
80.11  limonene
1954.06  linalool
230.06  linalyl acetate
150.30para-menthene
261.44  menthol
160.32iso menthone
288.68  methyl chavicol
371.02  methyl eugenol
60.08  myrcene
100.02(Z)-beta- ocimene
140.11allo- ocimene
10.83alpha- pinene
30.08beta- pinene
40.09  sabinene
240.40  terpinen-4-ol
70.06alpha- terpinene
110.15gamma- terpinene
290.91alpha- terpineol
130.03  terpinolene
320.85alpha- terpinyl acetate

E. Kostrzewa and K. Karwowska, Chemical composition of the essential oil from sweet basil grown in Poland. Prace Inst. Lab. Bad. Przem Spoz., 44, 97-107(1991).

P&F 20, No. 4, 29, (1995)

pimenta dioica leaf oil
#%LeftshiftComponents
182.77alpha- amorphene
172.13allo- aromadendrene
220.49  cadina-1,4-diene
215.49delta- cadinene
284.94alpha- cadinol
276.64T- cadinol
231.23alpha- calacorene
2011.12 calamenene + gamma-cadinene
131.00  carvacrol
110.10  carvone
151.00beta- caryophyllene
242.69  caryophyllene oxide
514.501,8- cineole
41.87para- cymene
250.52alpha- eudesmol
260.82beta- eudesmol
1428.04  eugenol
1610.12alpha- humulene
60.10  limonene
90.56  menthol
100.09  methyl chavocol
191.76alpha- muurolene
20.19  myrcene
31.12alpha- phellandrene
10.56alpha- pinene
70.56gamma- terpinene
81.38  terpinolene
121.00  thymol

J. A. Pino, J. Garcia and M. A. Martinez, Solvent extraction and supercritical carbon dioxide extraction of Pimenta dioica Merrill leaf. J. Essent. Oil Res., 9, 689-691 (1997).

P&F 24, No. 2, 35, (1999)

spearmint oil america
#%LeftshiftComponents
190.91-1.24beta- bourbonene
20.05-0.08  camphene
310.11-0.17trans- carveol
320.31-0.54cis- carveol
2965.79-71.62  carvone
300.03-0.12cis- carvyl acetate
71.40-1.571,8- cineole
12trace-0.04para- cymene
250.12-0.43(E)- dihydrocarvone
240.92-2.20(Z)- dihydrocarvone
270.35-0.43  dihydrocarvyl acetate
220.06-0.23beta- elemene
280.09-0.30  germacrene D
613.65-17.27  limonene
200.10-0.51  linalool
260.08-0.11  menthol
180.08-0.26  menthone
50.82-1.13  myrcene
9trace-0.07(E)-beta- ocimene
80.06-0.14(Z)-beta- ocimene
152.09-2.663- octanol
11trace-0.073- octanone
160.05-0.121- octen-3-yl acetate
140.13-0.233- octyl acetate
10.51-0.72alpha- pinene
30.58-0.76beta- pinene
40.43-0.56  sabinene
170.95-1.43(E)- sabinene hydrate
210.06-0.08(Z)- sabinene hydrate
230.33-0.45  terpinen-4-ol
100.07-0.14gamma- terpinene
130.04-0.07  terpinolene

B. M. Lawrence, unpublished information.

P&F 18, No. 3, 61, (1993)

tanacetum vulgare oil
#%LeftshiftComponents
161.60  artemisyl alcohol
1223.50  artemisyl ketone
180.10beta- bourbonene
31tracedelta- cadinene
30.60  camphene
196.00  camphor
296.60  carvone
230.30beta- caryophyllene
80.701,8- cineole
170.10alpha- copaene
200.10beta- copaene
100.80para- cymene
281.50  germacrene D
70.20  limonene
260.20  menthol
240.10neo menthol
10.10(E)-2-methyl-3-methylene hept-5-ene
60.10alpha- phellandrene
20.20alpha- pinene
40.10beta- pinene
51.50  sabinene
270.20  sabinol
301.20  sabinyl 2-methyl butyrate
210.70  terpinen-4-ol
90.30gamma- terpinene
11trace  terpinolene
140.90alpha- thujone
1549.50beta- thujone
250.40isothujyl alcohol
320.20  viridiflorol
220.10beta- ylangene
131.10  yomogi alcohol

B. M. Lawrence, unpublished data (1976).

P&F 25, No. 1, 33, (2000)

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