BT

Typical G.C. analysis

alpinia galanga oil
#%LeftshiftComponents
2410.70alpha- bergamotene
3016.20beta- bisabolene
12trace  borneol
172.50  bornyl acetate
20.50  camphene
230.90  caryophyllene
332.50  caryophyllene oxide
160.20  chavicol
191.00  chavicyl acetate
75.501,8- cineole
201.60  citronellyl acetate
220.70  copaene
281.90ar- curcumene
14tracepara- cymen-8-ol
60.80para- cymene
291.50  eugenyl acetate
2618.20(E)-beta- farnesene
215.10  geranyl acetate
250.60alpha- humulene
81.60  limonene
11trace  linalool
50.70  myrcene
311.90  pentadecane
321.60beta-sesqui phellandrene
110.20alpha- pinene
41.60beta- pinene
3trace  sabinene
270.80 santalene
130.30  terpinen-4-ol
9tracealpha- terpinene
150.20alpha- terpineol
10trace  terpinolene
18trace  tridecane

H. L. De Pooter, M. Nor Omar, B. A. Coolsaet and N. M. Schamp, The Essential Oil of Greater Galanga (Alpinia galanga) from Malaysia, Phytochem.,24, 93-96 (1985).

P&F 11, No. 1, 29, (1986)

cassia leaf oil
#%LeftshiftComponents
 0.54  benzaldehyde
 1.82  benzyl benzoate
 1.58  camphene
 2.60  camphor
 2.90delta-3- carene
 6.24beta- caryophyllene
 46.52(E)- cinnamaldehyde
 2.64(E)- cinnamyl acetate
 1.40alpha- copaene
 4.18para- cymene
 3.63  eugenol
 0.30  eugenyl acetate
 0.85alpha- humulene
 2.98  linalool
 0.79ortho- methoxycinnamaldehyde
 0.07  myrcene
 9.16beta-phellandrene + limonene
 3.47alpha- pinene
 1.02beta- pinene
 0.07alpha- terpineol

L.-F. Zhu, Y.-H. Li, B.-L. Li, B.-Y. Lu and N.-H. Xia, Aromatic Plants and Essential Constituents. South China Institute of Botany, Chinese Academy of Sciences, Hai Feng Publish. Co. distributed by Peace Book Co. Ltd., Hong Kong (1993).

P&F 19, No. 4, 33, (1994)

cinnamomum cassia bark oil china
#%LeftshiftComponents
10.54  benzaldehyde
201.82  benzyl benzoate
31.58  camphene
102.60  camphor
62.90delta-3- carene
166.24beta- caryophyllene
1246.52(E)- cinnamaldehyde
152.64(E)- cinnamyl acetate
141.40alpha- copaene
74.18para- cymene
133.63  eugenol
180.30  eugenyl acetate
170.85alpha- humulene
92.98  linalool
190.79ortho- methoxycinnamaldehyde
40.07  myrcene
89.16beta-phellandrene + limonene
23.47alpha- pinene
51.02beta- pinene
110.07alpha- terpineol

N. Bouzid, K. Toulgouate, G. Villarem and A. Gaset, Analyse quantitative des fractions d’huile essentielle pouvant co-exister lors d’hydrodistillation & plants aromatiques. Rivista Ital. EPPOS, (April), 15-25 (1997).

P&F 23, No. 1, 39, (1998)

cinnamomum tamala oil
#%LeftshiftComponents
90.20  benzaldehyde
20.10  camphene
110.70  caryophyllene
60.901,8- cineole
73.20para- cymene
1578.00  eugenol
141.20  eugenyl acetate
120.10  geraniol
50.70  limonene
80.20  linalool
130.50  methyl eugenol
40.30  myrcene
11.50alpha- pinene
30.40beta- pinene
100.30alpha- terpineol

B. C. Gulati, Essential oils of cinnamomum species in Cultivation and Utilization of Aromatic Plants. Edit. C. K. Atal and B. M. Kapur, R. R. L., Council of Scientific & Indust. Research (1982).

P&F 8, No. 4, 65, (1983)

cinnamomum zeylanicum bark oil CO2 extract
#%LeftshiftComponents
20.02-0.03  benzaldehyde
230.78-1.63  benzyl benzoate
40.02-0.10  camphene
100.71-2.221,8- cineole
1777.24-81.47  cinnamaldehyde
215.27-6.58 cinnamyl acetate + beta-caryophyllene
90.36-0.78para- cymene
201.82-2.31  eugenol
221.51-2.02  eugenyl acetate
180.00-0.12  geraniol
110.17-0.42  limonene
140.84-1.61  linalool
70.00-0.02  myrcene
30.06-0.21alpha- pinene
60.03-0.11beta- pinene
50.02-0.03  sabinene
190.00-0.02  safrole
80.04-0.23  salicylaldehyde
150.14-0.19  terpinen-4-ol
120.01-0.03gamma- terpinene
160.19-0.35alpha- terpineol
130.01-0.04  terpinolene
10.01-0.08alpha- thujene

F. Tateo and F. Chizzini, The Composition and Quality of Supercntical CO2 Extracted Cinnamon. J. Essent. Oil Res., 1, 165-168 ( 1989).

P&F 19, No. 3, 59, (1994)

cinnamomum zeylanicum leaf oil
The seasonal variation in the composition of cinnamon leaf oil produced from leaves harvested at different times of the year was studied by Kaul et al. (1996). They found that oil produced from leaves harvested either in the summer or in the winter possessed comparable chemical compositions, whereas an oil produced from leaves harvested in the rainy season had a reduced level of eugenol and an increased level of eugenyl acetate (Table VIII). Note: this page will only include the summer harvest.
#%LeftshiftComponents
220.43  benzyl benzoate
200.06delta- cadinene
30.12  camphene
170.48beta- caryophyllene
210.26  caryophyllene oxide
130.17(E)- cinnamaldehyde
160.19(E)- cinnamyl acetate
90.07  citronellal
60.36para- cymene
150.34beta- elemene
1493.94  eugenol
191.07  eugenyl acetate
180.12alpha- humulene
70.31 limonene + 1,8-cineole
80.86  linalool
50.23alpha- phellandrene
20.33alpha- pinene
40.16beta- pinene
120.07  piperitone
100.09  terpinen-4-ol
110.10alpha- terpineol
10.03alpha- thujene

P. N. Kaul, A. K. Battacharya and B. R. Rajeswara Rae, Seasonal variation in the composition of the essential oil of cinnamon (Cinnamomum zeylanicum Blume) leaves. Indian Perfum., 40(2), 36-38 (1996).

P&F 22, No. 5, 71, (1997)

cinnamon bark oil ceylon
Using GC (retention indices) Bouzid et al. (1997) analyzed an oil of cinnamon bark. The compounds identified were as follows:
#%LeftshiftComponents
10.54  benzaldehyde
201.82  benzyl benzoate
31.58  camphene
102.60  camphor
62.90delta-3- carene
166.24beta- caryophyllene
1246.52(E)- cinnamaldehyde
152.64(E)- cinnamyl acetate
141.40alpha- copaene
74.18para- cymene
133.63  eugenol
180.30  eugenyl acetate
170.85alpha- humulene
92.98  linalool
190.79ortho- methoxycinnamaldehyde
40.07  myrcene
89.16beta-phellandrene + limonene
23.47alpha- pinene
51.02beta- pinene
110.07alpha- terpineol

N. Bouzid, K. Toulgouate, G. Villarem and A. Gaset, Analyse quantitative des fractions d'huile essentielle pouvant co-exister lors d'hydrodistillation de plants aromatiques. Rivista Ital. EPPOS, (April), 15-25 (1997).

P&F 23, No. 1, 39, (1998)

clove bud oil india
#%LeftshiftComponents
261.08  asarone
90.07  benzaldehyde
160.52  benzyl alcohol
180.54delta- cadinene
170.34gamma- cadinene
146.18beta- caryophyllene
190.14 caryophyllene isomer
130.84alpha-copaene + alpha-terpineol
120.66alpha- cubebene
60.07para- cymene
2077.13  eugenol
211.08iso eugenol
225.04  eugenyl acetate
241.08(E,E)- farnesol
230.77(Z,E)- farnesol
70.032- heptanol
40.052-heptanone + 1,8-cineole
30.052- hexanone
151.06alpha- humulene
80.052- nonanol
10.02alpha- pinene
20.03beta- pinene
110.02  terpinen-4-ol
50.02alpha-terpinene + limonene
100.07(E)-beta- terpineol
250.92  vanillin

M. Copalakrishnan, C. S. Narayman and A. G. Mathew, Chemical composition of Indian clove bud, stem and leaf oils. Indian Perfum., 32(3), 229-235 (1988).

P&F 19, No. 5, 83, (1994)

clove leaf oil
#%LeftshiftComponents
220.45  asarone
80.07  benzaldehyde
141.39  benzyl alcohol
16tracedelta- cadinene
150.55gamma- cadinene
126.42beta- caryophyllene
110.37alpha-copaene + alpha-terpineol
100.08alpha- cubebene
60.05para- cymene
1780.97  eugenol
18traceiso eugenol
19trace  eugenyl acetate
210.61(E,E)- farnesol
200.61(Z,E)- farnesol
40.062-heptanone + 1,8-cineole
30.032- hexanone
131.39alpha- humulene
70.032- nonanol
10.03alpha- pinene
20.03beta- pinene
50.01alpha-terpinene + limonene
90.13(E)-beta- terpineol

M. Copalakrishnan, C. S. Narayman and A. G. Mathew, Chemical composition of Indian clove bud, stem and leaf oils. Indian Perfum., 32(3), 229-235 (1988).

P&F 19, No. 5, 83, (1994)

clove stem oil india
#%LeftshiftComponents
240.50  asarone
90.03  benzaldehyde
151.53  benzyl alcohol
170.63delta- cadinene
160.35gamma- cadinene
136.57beta- caryophyllene
120.77alpha-copaene + alpha-terpineol
110.49alpha- cubebene
60.05para- cymene
1880.19  eugenol
190.42iso eugenol
200.44  eugenyl acetate
220.69(E,E)- farnesol
210.47(Z,E)- farnesol
70.012- heptanol
40.042-heptanone + 1,8-cineole
30.052- hexanone
141.53alpha- humulene
80.062- nonanol
10.03alpha- pinene
20.06beta- pinene
50.02alpha-terpinene + limonene
100.12(E)-beta- terpineol
230.73  vanillin

M. Copalakrishnan, C. S. Narayman and A. G. Mathew, Chemical composition of Indian clove bud, stem and leaf oils. Indian Perfum., 32(3), 229-235 (1988).

P&F 19, No. 5, 83, (1994)

ferula cupularis leaf oil
Chemical composition and antibacterial activity of the essential oils from flower, leaf and stem of Ferula cupularis growing wild in Iran
#%LeftshiftComponents
1630.37  bicyclogermacrene
1536.55  bornyl angelate
1640.31delta- cadinene
1062.69  camphene
1002.90delta-2- carene
1600.17  caryophyllene oxide
1512.63  citronellyl butyrate
1082.37  decane
1305.02  dihydrolinalool acetate
1340.13trans-dimethoxycitral
1701.66beta- eudesmol
1571.87  eugenyl acetate
1610.11  geranyl butyrate
1680.21  guaiol
1155.78trans-isolimonene
1390.20para- menth-1-en-9-yl acetate
1134.05para- mentha-1,5,8-triene
9930.22beta- myrcene
1230.14  neral
1166.08allo- ocimene
1049.05beta- ocimene
1172.68neo-allo-ocimene
1361.65  octadecanal
1310.773- octen-1-yl acetate
2140.72  osthol
1092.36alpha- phellandrene
1104.18beta- phellandrene
10713.87beta- pinene
1220.62(Z)- sabinene hydrate acetate
1651.13  spathulenol
1203.45  terpinen-4-ol
1111.25alpha- terpinene
1463.70alpha- terpinyl isobutyrate
1190.363-thujenol
1411.39neo-iso- verbenyl acetate
Ziba Alipour, Poroshat Taheri, and Nasrin Samadi Department of Biology, Faculty of Science, Roudehen Islamic Azad University, Tehran, Iran, 2Department of Chemistry, School of Art & Science, Case Western Reserve University, Cleveland, OH, United State, and 3Department of Drug and Food Control, Faculty of Pharmacy and Biotechnology Research Center, Tehran University of Medical Sciences, Tehran, Iran
herniaria incana lam. oil greece
#%LeftshiftComponents
490.20  abietatriene
40.40  benzaldehyde
241.00delta- cadinene
100.20  camphor
280.60  caryophyllene oxide
130.40beta- cyclocitral
172.30(E)-beta- damascenone
160.40(E,E)-2,4- decadienal
120.40  decanal
140.30(Z)-2- decenal
601.3010- demethyl squalene
530.20  docosane
180.40  dodecanal
480.30  eicosane
250.50  eugenyl acetate
200.30(E)-beta- farnesene
350.80(E,Z)- farnesol
340.30(Z,Z)- farnesol
441.90(E,E)- farnesyl acetone
191.50  geranyl acetone
220.30(Z)-beta- guaiene
511.10  heneicosane
581.10  heptacosane
330.40  heptadecane
420.602- heptadecanone
50.20(E,E)-2- heptadienal
570.30  hexacosane
290.30  hexadecane
474.00  hexadecanoic acid
10.40  hexanal
22.20(E)-2- hexenal
270.70(Z)-3- hexen-1-yl benzoate
211.60(Z)-beta- ionone
450.30  methyl hexadecanoate
460.30 methyl octadecane
310.90T- muurolol
611.10  nonacosane
430.10  nonadecane
410.40(E)-nonadecene
91.90  nonanal
591.70  octacosane
360.30  octadecane
500.20  octadecanol
80.30  octanol
561.60  pentacosane
400.30  pentadecanoic acid
60.20  phenyl acetaldehyde
372.20neo phytadiene
522.60(E)- phytol
3tracealpha- pinene
260.30  selina-3,7(11)-diene
11trace  terpinen-4-ol
7tracegamma- terpinene
550.20  tetracosane
300.30  tetradecanal
320.40  tetradecanol
620.90  triacontane
540.80  tricosane
235.80  tridecanal
392.506,10,14- trimethyl pentadecan-2-ol
3837.606,10,14- trimethyl-2-pentadecanone
150.90  undecanal
J. of Ess. Oil Res. 12, No. 4, 435, (2000)
pimenta racemosa leaf oil
In 1991, Tucker et al. analyzed the chemical composition of two commercial samples of the leaf oil of Pimenta racemosa (Miller) J. Moore var. racemosa using both GC and GC/MS. The components that were identified were as follows:
#%LeftshiftComponents
370.00-0.39alpha- amorphene
380.00-0.09  aromadendrene
400.00-0.28allo- aromadendrene
410.00-<0.01beta- cadinene
490.28-1.03delta- cadinene
470.05-0.15gamma- cadinene
550.00-0.30alpha- cadinol
530.00-<0.01gamma- cadinol
48<0.01-0.07(Z)- calamenene
30.00-0.14  camphene
210.00-<0.01  camphor
360.64-7.24beta- caryophyllene
420.00-0.17beta- chamigrene
26<0.01-15.51  chavicol
141.38-1.391,8- cineole
270.00-0.11(E)- cinnamaldehyde
320.32-0.41alpha- copaene
300.00-<0.01alpha- cubebene
230.00-<0.01para- cymen-8-ol
19<0.01-0.97para- cymene
120.00-0.30alpha-para- dimethyl styrene
330.00-0.20beta- elemene
3144.41-68.93  eugenol
500.00-0.51  eugenyl acetate
460.00-0.59alpha- farnesene
290.00-0.22  geranial
280.00-0.12  geraniol
520.00-0.36  globulol
350.00-0.13alpha- gurjunene
390.15-1.31alpha- humulene
132.07-3.90  limonene
200.13-3.63  linalool
250.03-0.05  methyl chavicol
340-11.88  methyl eugenol
450.00-0.05alpha- muurolene
540.00-<0.01gamma-muurolol
80.10-16.17  myrcene
160.08-1.42(E)-beta- ocimene
150.08-0.10(Z)-beta- ocimene
90.00-0.843- octanol
70.00-1.103- octanone
50.00-1.741- octen-3-ol
100.07-0.45alpha- phellandrene
20.46-0.47alpha- pinene
60.00-0.09beta- pinene
40.00-<0.1  sabinene
440.00-0.63alpha- selinene
430.00-0.33beta- selinene
510.00-0.12  spathulenol
220.05-0.90  terpinen-4-ol
110.02-0.19alpha- terpinene
17<0.01-0.16gamma- terpinene
240.14-0.52alpha- terpineol
180.09-0.24  terpinolene
10.0-<0.1alpha- thujene

A. Tucker, M. J. Macirarello, R. P. Adams, L. R. Landrum and T. A. Zanoni, Volatile leaf oils of Caribbean Myrtaceae 1. Three varieties of Pimenta racemosa (Miller) J. Moore of the Dominican Republic and the commerciai bay oil. J. Essent. Oil Res., 3, 323-329 (1991).

P&F 22, No. 6, 45, (1997)

tagetes minuta flower oil CO2 extract
#%LeftshiftComponents
543.56 alchenenotriol
309.98(E)- anethole
272.10para- anisaldehyde
410.33  aromadendrene
470.08beta- bisabolene
480.12gamma- cadinene
140.11  camphor
240.23cis- carveol
403.44beta- caryophyllene
230.61  citronellol
21.12para- cymene
311.51 dehydroelshotzia ketone
200.12(Z)- dihydrocarvone
65.19  dihydrotagetone
90.22alpha-para- dimethyl styrene
333.00delta- elemene
500.11gamma-elemene (furanoid)
210.15  elsholtzia ketone
490.15  eugenyl acetate
370.28  geranyl acetate
530.28  guaiol
422.14alpha- humulene
510.29  ledol
315.14  limonene
111.03  linalool
80.43(Z)- linalool oxide furanoid
280.47  linalyl acetate
100.12(E)-para- menth-2-en-1-ol
290.39  methyl citronellate
390.24  methyl eugenol
430.226-methyl-gamma-ionone
450.29alpha- muurolene
10.24  myrcene
340.19  neryl acetate
50.30(E)-beta- ocimene
419.33(Z)-beta- ocimene
360.10beta- patchoulene
460.13  pentadecane
170.30(Z)- pinanone
133.68(Z)- sabinene hydrate
350.32(E)-iso safrole
522.42  spathulenol
260.65(E)- tagetenone
2513.26(Z)- tagetenone
152.81(E)- tagetone
160.34(Z)- tagetone
180.46  terpinen-4-ol
70.26gamma- terpinene
190.50alpha- terpineol
380.16  tetradecane
120.24alpha- thujone
320.12  tridecane
440.57  valencene
220.05  verbenone

J. Daghero, M. Mattea, E. Reverchon, G. Della Porta and F. Senatore, Isolation of Tagetes minuta L. oil using supercritical CO2 extraction. In: Proceedings WOCMAP-2. Edits., V. Martino, A. Bandoni, G. Bleak and N. Capelle, Acta Hort., 503, 21-25 (1999).

P&F 25, No. 6, 32, (2000)

valeriana officinalis rhizome oil CO2 extract china
#%LeftshiftComponents
10.37  acetic acid
170.01  benzoic acid
410.72(E)-alpha- bergamotol
420.34(Z)-alpha-bergamotol
180.47  borneol
2336.07  bornyl acetate
360.24delta- cadinene
100.02iso camphane
52.81  camphene
110.03delta-3- carene
250.02trans-carvone oxide
240.14cis- carvone oxide
310.65beta- caryophyllene
130.021,8- cineole
210.19  cumic acid
80.02para- cymene
290.07beta- elemene
270.08delta- elemene
370.53  elemol
120.013- ethyl-2,5-dimethyl-1,3-hexadiene
442.45  eugenyl acetate
350.66 germacrene
402.24  globulol
340.23  guaiene
320.21beta- gurjunene
330.31alpha- humulene
90.26  limonene
150.02  linalool
220.12  methyl chavocol
200.02  myrtenol
4326.56  nootkatone
40.60alpha- pinene
70.59beta- pinene
60.03  sabinene
160.01  sabinene hydrate
263.03  sabinyl acetate
380.73 sabinyl valerate
391.84  spathulenol
190.13  terpinen-4-ol
140.02  terpinolene
280.62alpha- terpinyl acetate
300.42 thymohydroquinone dimethyl ether
30.03  tricyclene
20.21iso valeric acid

J-J. Xian, G. Yuan, Y-X. Zhang, J-M. Yuan and X-W. Luo, The chemical constituents of the essential oil from the roots of Valeriana officinalis. Yunnan Zhiwu Yanjiu, 17, 479-481 (1995).

P&F 24, No. 3, 47, (1999)

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