BT

Typical G.C. analysis

artemisia absinthium herb oil italy
Mucciarelli et al. (1995) performed GC/MS analysis on oils obtained from a number of Artemisia species growing in northwest Italy. In this study, they determined that an oil of A. absinthum contained:
#%LeftshiftComponents
17trace  artemisyl alcohol
46trace  artemisyl ketone
31trace  ascaridole
55trace(E)-alpha- bergamotol
54tracealpha- bisabolol
58trace bisabolol oxide
36trace  borneol
42trace  bornyl acetate
56tracealpha- cadinol
4trace  camphene
47trace  camphenilone
210.4  camphor
590.3  carvacrol
39tracetrans- carveol
25trace  carvone
500.5beta- caryophyllene
570.4  caryophyllene oxide
41trace(E)- chrysanthenyl acetate
40trace(Z)- chrysanthenyl acetate
282.01,8- cineole
480.2alpha- copaene
52traceepi- cubenol
450.2  cuminaldehyde
121.0para- cymene
26trace  damascenone
27trace2,3- dihydro-1,8-cineole
29trace(Z)- epoxyocimene
3tracealpha- fenchene
100.1  limonene
18trace  linalool
300.1  linalool oxide
7trace  myrcene
440.1  myrtenal
380.1  myrtenol
51trace(E)- nerolidol
37trace  nojiku alcohol
8tracealpha- phellandrene
10.3alpha- pinene
50.7beta- pinene
22traceiso pinocamphone
33trace  pinocarveol
230.2  pinocarvone
61.6  sabinene
140.2(E)- sabinene hydrate
431.6  sabinyl acetate
490.6gamma- selinene
530.1  spathulenol
321.3  terpinen-4-ol
90.3alpha- terpinene
110.6gamma- terpinene
35tracealpha- terpineol
130.1  terpinolene
160.4(Z)-thuj-2-en-4-ol
20.3alpha- thujene
1967.5alpha- thujone
2018.2beta- thujone
34trace(E)- verbenol
24trace  verbenone
15trace  yomogi alcohol

M. Mucciarelli, R. Caramiello, M. Maffei and F. Chialva, Essential oils from some Artemisia species growing spontaneously in Northwest Italy. Flav. Fragr. J., 10, 25-32 (1995).

P&F 23, No. 1, 39, (1998)

crithmum maritimum oil
#%LeftshiftComponents
53<0.10(E)-alpha- bergamotol
26<0.10  bornyl formate
5<0.10delta-3- carene
540.10  carvacrol
45<0.10trans- carveol
57<0.10 caryophylla-2(12),6(13)-dien-5a-ol
46<0.10para- cymen-8-ol
125.30para- cymene
44<0.10beta- damascenone
320.10(E)-2- decenal
41<0.10neo dihydrocarveol
58<0.10  dillapiole
16<0.10alpha-para- dimethyl styrene
550.10  elemicin
400.10(Z)-1,2-epoxyterpinen-4-ol
19<0.104,8- epoxyterpinolene
36<0.10  limonen-4-ol
824.20  limonene
17<0.10(Z)-1,2- limonene epoxide
21<0.10  linalool
240.70(E)-para- menth-2-en-1-ol
310.40(Z)-para- menth-2-en-1-ol
50<0.10(Z)-para-menth-3-en-1,2-diol
48<0.10para- mentha-1,4-dien-7-ol
33<0.10(E)-para- mentha-2,8-dien-1-ol
520.20para- methoxypropiophenone
29<0.10  methyl carvacrol
343.40  methyl chavicol
47<0.10  methyl eugenol
250.30  methyl isothymol
270.30  methyl thymol
30<0.102- methyl-6-methylene-3,7-octadien-2-ol
61.60  myrcene
56<0.10  myristicin
370.10  myrtenyl acetate
15<0.10  nonanal
200.10(E)-2- nonenal
100.30(Z)-beta- ocimene
14<0.10  octanal
23<0.10  octanol
90.30beta- phellandrene
59<0.10  phytol
10.70alpha- pinene
30.20beta- pinene
350.20(E)- piperitol
430.40(Z)- piperitol
42<0.10  piperitone
426.90  sabinene
180.90(E)- sabinene hydrate
220.60(Z)- sabinene hydrate
490.30  spathulenol
289.00  terpinen-4-ol
71.40alpha- terpinene
1119.30gamma- terpinene
380.40alpha- terpineol
130.70  terpinolene
39<0.10alpha- terpinyl acetate
20.30alpha- thujene
51<0.10  thymol
J. of Ess. Oil Res. 12, No. 4, 424, (2000)
mentha pulegium oil cuba
#%LeftshiftComponents
270.10beta- bourbonene
300.18delta- cadinene
250.09alpha- calacorene
282.49beta- caryophyllene
311.04  caryophyllene oxide
60.08para- cymene
260.39beta- damascenone
336.78  hexadecanoic acid
290.27alpha- humulene
71.13  limonene
90.77  linalool
150.16  menthol
160.30iso menthol
131.86neo menthol
1420.68neoiso menthol
106.29  menthone
119.73iso menthone
200.14iso menthyl acetate
230.28neo menthyl acetate
226.24neoiso menthyl acetate
50.06  myrcene
80.11(Z)-beta- ocimene
40.413- octanol
10.35alpha- pinene
30.38beta- pinene
242.39  piperitenone
191.02  piperitone
1825.14  pulegone
20.11  sabinene
170.29alpha- terpineol
320.56  tetradecanoic acid
213.03  thymol
120.74  umbellulone

J. Pino, A. R.sado and V. Fluentes, Chemical composition of the essential oil of Mentha puiegium L. from Cuba. J. Essent. Oil. Res., 8, 295-296 (1996).

P&F 23, No. 3, 63, (1998)

salvia officinalis seed oil tunisia
GC Analyses of Salvia Seeds as Valuable Essential Oil Source Mouna Ben Taârit, Kamel Msaada, Karim Hosni, and Brahim Marzouk1 1Laboratoire des Substances Bioactives, Centre de Biotechnologie, Technopôle de Borj-Cédria, BP 901, 2050 Hammam-Lif, Tunisia 2Laboratoire des Substances Naturelles, Institut National de Recherche et d’Analyse Physico-Chimique (INRAP), Sidi Thabet, 2020 Ariana, Tunisia
#%LeftshiftComponents
1470.47alpha- amorphene
1461.43allo- aromadendrene
1620.18  aromadendrene
1751.29  bicyclogermacrene
1740.72beta- bisabolene
1163.54  borneol
1590.16  bornyl acetate
1510.08gamma- cadinene
1510.53delta- cadinene
2180.15T- cadinol
 0.41alpha- cadinol
15313.08  camphor
1150.03delta-3- carene
1290.83  carvacrol
1610.19beta- caryophyllene
1570.16  caryophyllene oxide
1036.661,8- cineole
1490.01alpha- copaene
1490.34epi- cubebol
1180.17para- cymen-8-ol
1021.52para- cymene
1380.06beta- damascenone
1380.16beta- elemene
1330.07delta- elemene
 0.47beta- eudesmol
1350.83  eugenol
1500.24(E,E)-alpha- farnesene
1141.01 geigerene
1850.33  geraniol
1850.08  germacrene B
1721.18  germacrene D
8781.29  hexanol
1453.71alpha- humulene
1600.25  humulene oxide II
1550.68  linalool
1070.13(Z)- linalool oxide
1230.08  linalyl acetate
 2.2213-epi- manool
1400.18  methyl eugenol
1190.28  myrtanol
1190.55  myrtenal
1561.41(E)- nerolidol
1380.14(Z)-allo-ocimene
9391.26alpha- pinene
1060.19(Z)- sabinene hydrate
1210.18(Z)- sabinol
1570.08  spathulenol
1170.09  terpinen-4-ol
1700.91alpha- terpineol
1182.42delta- terpineol
1701.81alpha- terpinyl acetate
1033.08alpha- thujene
11014.77alpha- thujone
1114.30beta- thujone
1290.37  thymol
1010.23  tricyclene
1100.48  undecane
1592.66  viridiflorol
1490.04alpha- ylangene
Overall, it emerges that tricyclene and camphor were biochemical markers of the essential oil of S. verbenaca seeds. Being rich in camphor, seeds could be used as antimicrobial agent. Another point that should be highlighted is that S. officinalis seeds had the same a-thujone chemotype as leaves, whereas these two organs showed some quantitative differences leading to the safe use of seeds essential oil in food industry. From a qualitative standpoint, seeds of S. sclarea seemed to have the same enzymatic trend as flowers characterized by the prevalence of linalool. It is noteworthy to mention that linalool-producing seeds as S. sclarea were suitable for flavouring purposes and constitute potential anti-inflammatory agents.
salvia sclarea oil greece
#%LeftshiftComponents
320.10  aromadendrene
57trace  benzyl tiglate
29trace  bornyl acetate
250.15beta- bourbonene
43tracedelta- cadinene
2trace  camphene
62trace  carvacrol
301.20beta- caryophyllene
501.50  caryophyllene oxide
6trace1,8- cineole
230.50alpha- copaene
260.10beta- cubebene
480.15para- cymen-8-ol
460.10beta- damascenone
691.25 deutenyl curcumene furanoid
45trace dihydro-para-cymen-8-ol
580.10  dodecahydro-3a-,6,6,9a-tetramethyl(2,1beta)furan
550.15  elemol
610.158,13- epoxy-15,16-dinorlabd-12-ene
56trace  eudesmol
54trace10-epi-gamma- eudesmol
630.20alpha- eudesmol
641.50beta- eudesmol
24trace formic acid + benzaldehyde
412.15  geranial
496.50  geraniol
447.50  geranyl acetate
401.25  geranyl formate
140.10  hexanol
170.102- hexanol
150.153- hexanol
70.152- hexenal
12trace hexen-1-yl acetate furanoid
350.10alpha- humulene
51trace  hydroxycitronellal
670.10endo-8-hydroxycycloisolongifolene furanoid
521.20 hydroxylinalool furanoid
370.10 lavandulol + beta-farnesene
50.15  limonene
2717.20  linalool
221.10(E)- linalool oxide furanoid
190.15(Z)- linalool oxide furanoid
2814.30  linalyl acetate
31trace  linalyl formate
712.50  manool
680.10  manoyl oxide
700.1513-epi- manoyl oxide
34trace  methyl chavicol
9trace2-methyl-2-vinyl-4-isopropenyl tetrahydrofuran
13trace6- methyl-5-hepten-2-one
38trace  muurolene
66trace muurolol
40.25  myrcene
361.50  neral
475.50  nerol
21trace  nerol oxide
53trace  nerolidol
425.20  neryl acetate
16trace  nonanal
100.15(E)-beta- ocimene
80.10(Z)-beta- ocimene
180.10  perillene
10.10alpha- pinene
30.10beta- pinene
725.20  sclareol
590.20  spathulenol
330.20  terpinen-4-ol
3915.10alpha- terpineol
11trace  terpinolene
65trace  thymol
600.10  valerianol
200.10alpha-ylangene + 1-octen-3-ol

Ch. Souleles and N. Argyriadou, Constituents of the essential oil of Salvia sclarea growing wild in Greece. Internat. J. Pharmacog., 35, 218-220 (1997).

P&F 25, No. 4, 55, (2000)

salvia sclarea oil spain
#%LeftshiftComponents
6trace  amyl butyrate
390.52  bicyclogermacrene
150.12  borneol
241.11  bornyl acetate
300.27beta- bourbonene
350.14alpha- cadinene
420.22gamma- cadinene
511.10alpha- cadinol
45tracebeta- calacorene
440.77(Z)-calamenene + germacrene B
2trace  camphene
334.80beta- caryophyllene
470.99  caryophyllene oxide
320.14alpha- cedrene
70.831,8-cineole + limonene
260.36alpha- cubebene
480.16  cubenol
280.27beta- damascenone
180.11  dihydrocarveol
310.43beta- elemene
25tracedelta- elemene
500.73beta- eudesmol
410.27(E,E)-alpha- farnesene
360.14(Z)-beta- farnesene
220.93  geranial
201.12  geraniol
291.62  geranyl acetate
230.25  geranyl formate
377.57  germacrene D
340.14beta- gurjunene
1432.97  linalool
12trace(E)- linalool oxide furanoid
11trace(Z)- linalool oxide furanoid
2116.85  linalyl acetate
540.55  manool
52trace  manoyl oxide
531.1413-epi- manoyl oxide
400.40alpha- muurolene
490.42alpha- muurolol
51.61  myrcene
190.72  nerol
43trace(Z)- nerolidol
271.17  neryl acetate
90.94(E)-beta- ocimene
80.58(Z)-beta- ocimene
10.30alpha- pinene
40.41beta- pinene
3trace  sabinene
550.45  sclareol
460.12  spathulenol
16trace  terpinen-4-ol
10tracegamma- terpinene
175.63alpha- terpineol
130.37  terpinolene
382.84  valencene

M. E. Torres, A. Velasco-Negueruela, M. J. Perez-Alonso and M. G. Pinilla, Volatile constituents of two Salvia species grown wild in Spain. J. Essent. Oil Res., 9, 27-33 (1997).

P&F 25, No. 4, 55, (2000)

valeriana officinalis rhizome oil china
#%LeftshiftComponents
101.31iso borneol
1246.22  bornyl acetate
130.61iso bornyl acetate
260.72  bornyl isovalerate
323.50  camphene
90.33  camphor
141.64  carvyl acetate
220.50beta- caryophyllene alcohol
50.40para- cymene
210.32  decahydro-1,1,4,7-tetramethyl cyclopropazulen-4-ol
200.44  decahydro-2,2,4,8-tetramethyl-4,8-methanazulen-9-ol
170.331,1- dimethoxy-3,7-dimethyl-2,6-octadiene
160.171,4-dimethoxytetramethyl benzene
71.377,7- dimethyl-2-methylene bicyclo(3.1.1)heptane
281.52(2Z)-3,7- dimethyl-2,6-octadien-1-ol isovalerate
230.602,6- dimethyl-6(4-methyl-3-pentenyl)-2-cyclohexene-1-carboxaldehyde
241.934-ethyl-2,2,4-trimethyl-3-(1-methyl ethenyl) cyclohexene methanol
270.61  geranyl isovalerate
180.38beta- gurjunene
250.53  ledol
60.77  limonene
80.353-methyl 2-norbornane carboxaldehyde
25.46alpha- pinene
43.50beta- pinene
110.282-iso propyl-5-methyl anisole
10.43alpha- thujene
190.984(2,6,6- trimethyl cyclohexa-1,3-dienyl)but-2-en-4-one
150.612,2,4-trimethyl-3-cyclohexene-1-methyl acetate

Y-D. Chen and C-H. Gu, Study on the chemical composition of essential oil from Valeriana officinalis. Lincnan Huaxue Yu Gongye, 9(1), 59-64 (1989).

P&F 24, No. 3, 47, (1999)

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