BT

Typical G.C. analysis

crithmum maritimum oil
#%LeftshiftComponents
53<0.10(E)-alpha- bergamotol
26<0.10  bornyl formate
5<0.10delta-3- carene
540.10  carvacrol
45<0.10trans- carveol
57<0.10 caryophylla-2(12),6(13)-dien-5a-ol
46<0.10para- cymen-8-ol
125.30para- cymene
44<0.10beta- damascenone
320.10(E)-2- decenal
41<0.10neo dihydrocarveol
58<0.10  dillapiole
16<0.10alpha-para- dimethyl styrene
550.10  elemicin
400.10(Z)-1,2-epoxyterpinen-4-ol
19<0.104,8- epoxyterpinolene
36<0.10  limonen-4-ol
824.20  limonene
17<0.10(Z)-1,2- limonene epoxide
21<0.10  linalool
240.70(E)-para- menth-2-en-1-ol
310.40(Z)-para- menth-2-en-1-ol
50<0.10(Z)-para-menth-3-en-1,2-diol
48<0.10para- mentha-1,4-dien-7-ol
33<0.10(E)-para- mentha-2,8-dien-1-ol
520.20para- methoxypropiophenone
29<0.10  methyl carvacrol
343.40  methyl chavicol
47<0.10  methyl eugenol
250.30  methyl isothymol
270.30  methyl thymol
30<0.102- methyl-6-methylene-3,7-octadien-2-ol
61.60  myrcene
56<0.10  myristicin
370.10  myrtenyl acetate
15<0.10  nonanal
200.10(E)-2- nonenal
100.30(Z)-beta- ocimene
14<0.10  octanal
23<0.10  octanol
90.30beta- phellandrene
59<0.10  phytol
10.70alpha- pinene
30.20beta- pinene
350.20(E)- piperitol
430.40(Z)- piperitol
42<0.10  piperitone
426.90  sabinene
180.90(E)- sabinene hydrate
220.60(Z)- sabinene hydrate
490.30  spathulenol
289.00  terpinen-4-ol
71.40alpha- terpinene
1119.30gamma- terpinene
380.40alpha- terpineol
130.70  terpinolene
39<0.10alpha- terpinyl acetate
20.30alpha- thujene
51<0.10  thymol
J. of Ess. Oil Res. 12, No. 4, 424, (2000)
croton eluteria bark oil
#%LeftshiftComponents
800.01  amyl benzoate
330.28allo- aromadendrene
129tracealpha- bisabolol
126tracebeta- bisabolol
1010.94  borneol
550.22  cadalene
460.42delta- cadinene
440.17gamma- cadinene
1231.00T- cadinol
470.96alpha- calacorene
490.24beta- calacorene
450.11  calamenene
40.40  camphene
630.02  camphor
100.21delta-2- carene
1130.02  carvacrol
110trace  carvenone
1080.08trans- carveol
670.03  carvone
680.21  carvotan acetone
320.25beta- caryophyllene
870.67 caryophyllene oxide + dihydro-ar-bisabolol
860.32 cascarilla epoxide
890.08 cascarilla furan
1331.34 cascarilla hydroxyketone
920.01 cascarilla hydroxyketone
930.02 cascarilla lactone
274.62  cascarilladiene
901.28 cascarilladienone
1370.74  cascarillone
1211.78beta-cedren-10-ol
281.11beta-cedrene isomer
1180.07  cedrol
430.20alpha- chamigrene
360.11beta- chamigrene
600.281,8- cineole
480.09 compound k
500.23 compound l
510.07 compound m
520.14 compound n
530.01 compound o
540.07 compound p
740.02 compound q
770.73 compound r
1270.38 compound t
1280.18 compound u
1350.06 compound v
1384.30 compound w
250.39alpha- copaene
230.04alpha- cubebene
370.21beta- cubebene
660.05  cuminaldehyde
422.45 cuparene + alpha-muurolene
1341.88 cuparophenol
350.39ar- curcumene
240.53  cyclosativene
1020.28para- cymen-8-ol
119.91para- cymene
650.062- decanone
1310.86 dictyopterol 1A
1320.43 dictyopterol 1B
1300.513,4-dihydro-6-methyl-4-isopropyl-1(2H)-naphthalenone
79trace2,5-dimethoxy-meta-cymene
200.012,5- dimethoxytoluene (fennelone)
160.16alpha-para- dimethyl styrene
1191.286,7-dimethyl undeca-5,9-dien-2-ol
340.731,11-oxido calamenene
261.63beta- elemene
410.31gamma- elemene
1140.56  elemicin
1150.51beta- elemol
1243.03beta- eudesmol
310.07(E)-beta- farnesene
970.01alpha- fenchyl alcohol
1360.35 geran-9-yl-alpha-terpineol
812.18  geranyl acetone
290.07  germacrene D
120trace  guaiol
57trace2- heptanol
560.012- heptanone
1trace2,4- hexadien-1-al
880.28 humulene epoxide isomer
1250.71  intermedeol
120.94 limonene + 1,8-cineole
965.12  linalool
940.09  linalool oxide
690.02  linalyl acetate
390.01beta- maaliene
980.04para-menth-2-en-1-ol
111tracepara- mentha-1,3-dien-7-al
640.02para- methyl acetophenone
80.02ortho- methyl anisole
820.053- methyl but-2-enyl benzoate
220.02  methyl carvacrol
760.05 methyl cascarillate
190.01  methyl chavicol
780.22  methyl eugenol
580.036- methyl heptan-2-one
210.02  methyl thymol
590.026- methyl-5-hepten-2-one
180.095-methyl-5-hexyl furan
70.64  myrcene
1050.17  myrtenol
1160.05  nerolidol
950.022- nonanol
610.182- nonanone
140.01(E)-beta- ocimene
130.01(Z)-beta- ocimene
700.05  phellandral
90.13alpha- phellandrene
32.59alpha- pinene
60.35beta- pinene
990.17  pinocarveol
1070.10  piperitol
840.03  prenyl benzoate
910.094-iso propyl-6-methyl tetral-1-one
50.09  sabinene
109trace  sabinol
380.58beta- selinene
1170.70  spathulenol
1031.70  terpinen-4-ol
73trace  terpinen-4-yl acetate
150.60gamma- terpinene
1041.10alpha- terpineol
100tracebeta- terpineol
170.07  terpinolene
750.16alpha- terpinyl acetate
22.11alpha- thujene
620.14alpha- thujone
300.23  thujopsene
112trace  thymol
1220.77  torilenol
85trace2- tridecanone
830.15(Z)-5-tridecen-2-one
710.295,8-undecadien-2-one + (Z)-5-undecen-2-one
720.312- undecanone
400.18  valencene
1060.11  verbenone

M. L. Hagedorn and S. M. Brown, The constituents of Cascarilla oil (Croton eluteria Bennett) Flav. Fragr. J., 6, 193-204 (1991).

P&F 18, No. 6, 53, (1993)

croton flavens l. (welensali) leaf oil curacao
#%LeftshiftComponents
470.30allo- aromadendrene
241.20  borneol
320.20  bornyl acetate
280.50  bornyl formate
390.30beta- bourbonene
511.20delta- cadinene
41.70  camphene
220.30  camphene hydrate
19tracealpha- campholenal
20trace  camphor
449.30iso caryophyllene
110.101,8- cineole
380.60alpha- copaene
360.20alpha- cubebene
487.90ar- curcumene
101.70para- cymene
420.50  cyperene
270.102- decanone
430.202,6- dimethoxy-para-cymene
40trace2- dodecanone
410.80beta- elemene
350.30delta- elemene
490.30  germacrene D
450.80alpha- gurjunene
461.50alpha- humulene
121.30  limonene
180.40  linalool
16trace(E)- linalool oxide furanoid
15trace(Z)- linalool oxide furanoid
370.20  longicyclene
8trace4- methyl anisole
300.10  methyl carvacrol
29trace  methyl thymol
70.60  myrcene
520.40(E)- nerolidol
130.20(Z)-beta- ocimene
91.50alpha- phellandrene
316.00alpha- pinene
60.70beta- pinene
21.020trans- pinocarveol
230.10  pinocarvone
50.20  sabinene
534.50  spathulenol
250.10  terpinen-4-ol
140.20gamma- terpinene
260.10alpha- terpineol
17trace  terpinolene
20.30alpha- thujene
34trace  thymol
10.20  tricyclene
500.302- tridecanone
330.502- undecanone
310.60trans- verbenyl acetate
J. of Ess. Oil Res. 12, No. 6, 667, (2000)
cupressus sempervirens cone oil egypt
#%LeftshiftComponents
280.3  borneol
370.4  bornyl acetate
200.2delta- cadinene
250.2alpha- cadinol
240.2T- cadinol
819.0delta-3- carene
340.3  carveol
35trace  carvone
410.2beta- caryophyllene
210.1  caryophyllene oxide
400.2alpha- cedrene
223.3  cedrol
230.16-isocedrol
39tracealpha- copaene
460.1para- cymen-8-ol
450.1ortho- cymene
100.4para-cymenel
140.6alpha-para- dimethyl styrene
31.8alpha- fenchene
160.2alpha- fenchyl alcohol
44trace  germacrene D
420.1alpha- humulene
122.5  limonene
360.2  methyl carvacrol
63.0  myrcene
300.1  myrtenal
320.1  myrtenol
7tracealpha- phellandrene
110.4beta- phellandrene
248.2alpha- pinene
51.4beta- pinene
180.1  pinocamphone
170.6trans- pinocarveol
190.3  pinocarvone
4trace  sabinene
43tracebeta- selinene
291.6  terpinen-4-ol
90.4alpha- terpinene
130.8gamma- terpinene
312.2alpha- terpineol
270.3delta- terpineol
153.9  terpinolene
382.2alpha- terpinyl acetate
470.6delta- terpinyl acetate
10.1  tricyclene
260.1  umbellulone
330.9  verbenone

F. F. Kassem, F. M. Harmz, N. A. El-Sebakhy, H. L. DePooter, N. M. Schamp and H, About-Shleib. Composition of the essential oil of Egyptian Cupressus sempervirens L. cones. Flav. Frag J., 6, 205-207 (1991).

P&F 20, No. 4, 29, (1995)

thymus vulgaris oil CO2 extract
Oszagyan et al. (1996) analyzed the composition od supercritical fluid CO2 extract of thyme (ex. T. vulgaris) and compared it to a steam-distilled oil. The quantitative data was obtained in a GD-FID, whereas the identity od each component was determined by GC/MS. A comparison between the two analyses is shown in Table VII. Note, only the CO2 extract will be shown here.
#%LeftshiftComponents
160.02  borneol
220.37  bornyl acetate
300.24gamma- cadinene
30.04  camphene
243.17  carvacrol
271.64beta- caryophyllene
100.161,8- cineole
260.22alpha- copaene
82.55para- cymene
210.04  geraniol
320.27  heptadecane
340.16  heptadecanoic acid
310.10  hexadecane
280.09alpha- humulene
90.09  limonene
131.63  linalool
200.54  methyl carvacrol
190.32  methyl thymol
50.17  myrcene
335.98  palmitic acid
60.09alpha- phellandrene
20.01alpha- pinene
40.35beta- pinene
140.02  pinocarveol
358.30  stearic acid
171.04  terpinen-4-ol
70.07alpha- terpinene
110.67gamma- terpinene
180.20alpha- terpineol
150.22beta- terpineol
120.09  terpinolene
10.03alpha- thujene
2336.59  thymol
290.01  valencene
25tracealpha- ylangene

H. J. Bestmann, J. Ederand O. Vostrowky, Extraktion von Thymian mit flusigem CO2 in Labormasstab. Zeit. Lebersmitt. Unters Forsch., 180, 491-493 (1985).

P&F 20, No. 3, 67, (1995)

trachyspermum copticum fruit oil
#%LeftshiftComponents
23trace(E)- anethole
25trace  anise ketone
3trace  camphene
6tracedelta-3- carene
270.60  carvacrol
21trace  carvone
11trace1,8- cineole
22trace  cuminaldehyde
1315.57para- cymene
92.08  limonene
18trace  methyl carvacrol
24trace  methyl eugenol
70.56  myrcene
100.18beta- phellandrene
10.32alpha- pinene
43.31beta- pinene
5trace  sabinene
150.19(E)- sabinene hydrate
160.29(Z)- sabinene hydrate
20tracebeta- selinene
171.13  terpinen-4-ol
8tracealpha- terpinene
1211.86gamma- terpinene
190.19alpha- terpineol
14trace  terpinolene
20.20alpha- thujene
2661.31  thymol

F. Chialva, F. Monguzzi, P. Manitto and A. Akgul. Essential oil constituents of Trachyspermum copticum (L.) Link Fruits. J. Essent. Oil Res., 5, 105-106 (1993).

P&F 19, No. 2, 63, (1994)

valeriana officinalis rhizome oil
#%LeftshiftComponents
360.2-0.8beta- bisabolene
580.5-1.5epi-alpha-bisabolol
160.1-0.6  borneol
15trace-0.1iso borneol
252.3-33.5  bornyl acetate
430.5-1.2  bornyl isovalerate
460.1-0.3delta- cadinene
30.1-6.4  camphene
14trace-0.1  camphor
21trace-0.1trans- carveol
200.1-0.2cis- carveol
8trace-0.21,8- cineole
31trace-0.1  citronellyl acetate
510.2-2.1  citronellyl isovalerate
33trace-0.2alpha- copaene
570.4-3.9  cryptofauronol
70trace-2.9  cryptofauronyl acetate
22trace-0.1  cuminaldehyde
400.7-2.1ar- curcumene
70.1-1.5para- cymene
340.2-1.42,6- dimethoxy-para-cymene
620.1-0.4  drimenol
350.1-0.4beta- elemene
300.2-2.9delta- elemene
420.1-0.4gamma- elemene
75trace-0.6  ethyl palmitate
380.5-7.6  eudesma-2,6,8-triene
530.6-6.9beta- eudesmol
29trace-0.1  eugenol
610.1-0.4  eugenyl isovalerate
670.1-1.1iso eugenyl isovalerate
480.4-0.6  faurinone
410.2-1.4  germacrene D
44trace-1.0beta- gurjunene
370.1-0.9alpha- humulene
390.1-0.7beta- ionone
450.2-3.8  kessane
380.1-3.5  kessanyl acetate
730.1-0.7  kessoglycyl monoacetate
630.1-12.6alpha- kessyl acetate
520.5-2.1  ledol
100.1-1.2  limonene
13trace  linalool
500.1-1.6  maaliol
240.1-0.2  methyl carvacrol
710.1-0.9  methyl palmitate
23trace-0.4  methyl thymol
650.1-0.2  methyl valerenate
6trace-0.1  myrcene
190.1-4.0  myrtenol
28trace-9.1  myrtenyl acetate
560.1-0.2 myrtenyl hexanoate
491.6-10.5  myrtenyl isovalerate
26trace-0.8  nojigiku acetate
470.5-3.2  pacifigorgiol
720.1-1.9  palmitic acid
9trace-2.4beta- phellandrene
20.1-0.2alpha- pinene
5trace-0.9beta- pinene
4trace-0.1  sabinene
170.1-0.6  terpinen-4-ol
11trace-0.2gamma- terpinene
18trace-0.1alpha- terpineol
12trace-0.1  terpinolene
270.1  thymol
1trace-0.1  tricyclene
550.5-8.2  valeranone
660.1-1.5(E)-valeren-1-yl acetate
640.2-0.8(Z)-valeren-1-yl acetate
76trace-1.6(E)-valeren-1-yl isovalerate
74trace-0.7(Z)-valeren-1-yl isovalerate
590.4-12.4  valerenal
690.3-2.8  valerenic acid
600.3-1.2(Z+E)- valerenol
541.5-14.2  valerianol
320.1-0.4alpha- ylangene

R. Bos and H. J. Woerdenbag, Analytical aspects of the essential oil, valerenic acid derivatives and valepotriates in Valeriana officinalis roots and rhizomes. In: Proceedings, International Symposium on breeding research and medicinal and aromatic plants. Edits., F. Pank, p. 355-358, Beiträge zur Zuchtungsforschung, Quedlinburg, Germany (1996).

P&F 24, No. 3, 47, (1999)

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