BT

Typical G.C. analysis

bombycilaena erecta oil greece
#%LeftshiftComponents
220.50  arteannuic alcohol
69.10  artemisyl alcohol
1010.70  artemisyl acetate
260.30beta- bisabolol
140.70iso bornyl acetate
250.40alpha- cadinol
33.60  camphene
818.80  camphor
92.60trans- carveol
110.30cis- carveol
120.40  carvotan acetone
150.90cis- carvyl acetate
191.00beta- caryophyllene
210.20  caryophyllene oxide
1312.20(Z)- chrysanthenyl acetate
183.80isocomene
200.30gamma- curcumene
270.407- ethyl-1,4-dimethyl azulene
242.00alpha- eudesmol
230.20  guaiol
290.80  hexadecanoic acid
171.50  italicene
161.20beta- maaliene
70.20  nonanal
20.40alpha- pinene
40.10beta- pinene
280.30  tetradecanoic acid
10.90  tricyclene
514.90  yomogi alcohol
J. of Ess. Oil Res. 12, No. 3, 360, (2000)
chenopodium ambrosioides oil spain
#%LeftshiftComponents
 0.04  allyl levulinate
 0.02allo- aromadendrene
 0.22iso borneol
 0.20iso bornyl acetate
 0.02nor bornyl acetate
 0.06iso bornyl propionate
 0.08delta- cadinene
 0.84  camphor
 2.28trans- carveol
 4.91cis- carveol
 2.07  carvone
 0.16  carvone oxide
 2.09beta- caryophyllene
 0.04beta- copaene
 0.03para- cymene
 0.71  dihydrocarveol
 5.00  geranial
 0.04  geranic acid
 4.30  geraniol
 0.24alpha- guaiene
 0.02  lavandulyl acetate
 32.50  limonene
 0.07  linalool
 0.21(Z)- linalool oxide furanoid
 4.00(Z)-para-mentha-2,8-dien-1-ol
 1.64  menthol
 0.03 methyl undecanal
 0.03  myrcene
 0.41  nerol
 0.01  neryl acetate
 0.02  neryl formate
 0.15  perillyl alcohol
 0.01alpha- phellandrene
 0.09alpha- pinene
 0.06beta- pinene
 26.70trans- pinocarveol
 3.54iso pulegol
 0.08iso pulegyl acetate
 0.06(E)- sabinene hydrate
 0.83alpha- terpinene
 0.03gamma- terpinene
 0.26alpha- thujene
 0.14  undecanal
 1.21(E)- verbenol
cypress leaf oil algetian
#%LeftshiftComponents
32trace  borneol
24trace-0.13  bornyl acetate
25traceiso bornyl acetate
360.20-0.76delta-cadinene + gamma-cadinene
44tracealpha- cadinol
45tracedelta- cadinol
40trace(Z)-alpha-calacorene
40.20-0.50  camphene
20trace  camphor
719.35-21.13delta-3- carene
38trace-0.08trans-carveol + (Z)-calamenene
260.14-0.35beta- caryophyllene
41trace  caryophyllene oxide
23trace-0.19alpha- cedrene
432.03-3.92  cedrol
19trace-0.06alpha- copaene
180.07-0.15alpha- cubebene
42trace  cubenol
39tracepara- cymen-8-ol
150.21-0.24para- cymene
480.10-0.28  dehydroabietane
30.73-0.81alpha- fenchene
17trace(Z)-3- hexen-1-ol
30trace-0.23alpha- humulene
102.28-3.31  limonene
210.07-0.33  linalool
220.11-0.16  linalyl acetate
470.12-0.20  manoyl oxide
35trace-0.10alpha- muurolene
34trace-0.32gamma- muurolene
83.11-3.48 myrcene + alpha-phellandrene
28trace  myrtenal
37trace  myrtenol
13trace(E)-beta- ocimene
12trace(Z)-beta- ocimene
110.43-0.54beta-phellandrene + 1,8-cineole
247.00-52.76alpha- pinene
51.10-1.37beta- pinene
29tracetrans- pinocarveol
60.74-0.93  sabinene
460.26-0.95  sandracopimaradiene
270.35-1.01  terpinen-4-ol
90.22-0.26alpha- terpinene
140.41-0.51gamma- terpinene
16trace  terpinolene
334.10-6.47alpha- terpinyl acetate
310.42-1.03alpha- terpinyl formate
10.09-0.11  tricyclene
N. Chanegriha, A. Baaliouamer, B. Y. Melklati, J. Favre-Bonvin and S. Alamercey, Chemical composition of Algetian cypress essential oil, J, Essent, Oil, Res., 5(6), 671-674 (1993). P&F 20, No. 4, 29, (1995)
eucalyptus urophylla s.t. blake leaf oil ethiopia
#%LeftshiftComponents
131.20iso borneol
150.20iso bornyl acetate
20.50  camphene
171.10beta- caryophyllene
190.20  caryophyllene oxide
834.501,8- cineole
120.70alpha- fenchyl alcohol
200.50  globulol
59.80  limonene
110.20  linalool
76.80(Z)-beta- ocimene
40.60alpha- phellandrene
60.20beta- phellandrene
113.30alpha- pinene
39.10beta- pinene
180.50  spathulenol
90.20gamma- terpinene
145.60alpha- terpineol
100.50  terpinolene
1611.60alpha- terpinyl acetate
J. of Ess. Oil Res. 12, No. 4, 467, (2000)
rosmarinus officinalis leaf oil CO2 extract
#%LeftshiftComponents
42trace  abietatriene
340.41beta- bisabolene
1515.56  borneol
234.94iso bornyl acetate
360.35delta- cadinene
350.26gamma- cadinene
250.19alpha- cadinol
370.15  calamenene
23.11  camphene
1215.33  camphor
40.39delta-3- carene
220.26  carvone
282.22beta- caryophyllene
390.37  caryophyllene oxide
400.20 cedrane diol
1020.021,8- cineole
260.43alpha- cubebene
311.28ar- curcumene
81.81para- cymene
200.39  dihydrocarveol
380.37  farnesene
300.38beta- gurjunene
90.51  limonene
113.53  linalool
210.48  linalyl acetate
270.12  methyl eugenol
330.20alpha- muurolene
60.35  myrcene
161.17  nonanol
41trace  octadecane
50.181- octen-3-ol
130.80 pinanone
18.30alpha- pinene
70.74beta- pinene
140.39  pinocarvone
30.32  sabinene
290.41alpha- santalene
320.16alpha- selinene
171.00  terpinen-4-ol
181.95alpha- terpineol
240.69  thymol
43trace  totarol
198.36  verbenone

E. Reverchon and F. Senatore, Isolation of rosemary oil: Comparison between hydrodistillation and supercritical CO2 extraction. Flav. Fragr. J., 7, 227-230 (1992).

P&F 17, No. 6, 51, (1992)

sage oil giza egypt
Comparative percentage composition of Salvia offlcinalis oil produced from plants grown in two areas of Egypt, Giza oil
#%LeftshiftComponents
 0.10  tricyclene
 0.17alpha- thujene
 3.81alpha- pinene
 3.70beta- pinene
 3.82  camphene
 3.85  sabinene
 3.38  myrcene
 0.85ortho- cymene
 0.76para- cymene
 9.381,8- cineole
 0.10(Z)-beta- ocimene
 1.10gamma- terpinene
 1.02  linalool
 0.68  terpinolene
 17.72alpha- thujone
 2.03beta- thujone
 0.05(Z)-para- menth-2-en-1-ol
 13.29  camphor
 0.10(Z)-beta- terpineol
 0.68iso menthone
 0.43iso pinocamphone
 2.37  borneol
 1.10alpha- terpineol
 1.44  carvone
 0.08  bornyl acetate
 2.20iso bornyl acetate
 0.68  sabinene hydrate acetate
 0.68  thymol
 1.70beta- caryophyllene
 1.10 aromadendr-9-ene
 3.05alpha- humulene
 0.10allo aromadendr-9-ene
 1.44  germacrene B
 0.04gamma- cadinene
 0.60delta- cadinene
 0.85  spathulenol
 0.60  caryophyllene oxide
 3.30  globulol
 0.85 bergamotol acetate
F. M. Soliman, M. A. El-Sohly, M. M. Fathy and F. S. El-Salhawy, A comparitive study of the essential oils from Mentha and Salvia species grown in Egypt. Egypt. J. Pharm. Sci., 38, 553-564 (1997).
tagetes minuta flower oil rwanda
#%LeftshiftComponents
10.63  acetone
280.06  artemisyl ketone
33trace  bornyl acetate
34traceiso bornyl acetate
8trace  camphene
100.11delta-3- carene
160.041,8- cineole
21tracepara- cymene
221.03  dihydrotagetone
250.163,4- dimethyl octa-2,4,6-triene
70.02  ethyl 2-methyl butyrate
60.12  ethyl butyrate
150.032- hexenal
260.14(Z)-3- hexen-1-ol
141.77  limonene
320.17  linalool
230.54para- menth-4-en-3-one
20.034- methyl-2-pentanone
11trace1- methyl-3-isopropyl cyclohexane
130.11  myrcene
200.17(E)-beta- ocimene
1737.08(Z)-beta- ocimene
29trace(Z)-beta-ocimene epoxide
120.07alpha- phellandrene
360.082(10)-pinen-4-one
40.03alpha- pinene
90.28  sabinene
30.05  santene
386.31(E)- tagetenone
373.34(Z)- tagetenone
302.86(E)- tagetone
3135.40(Z)- tagetone
350.07  terpinen-4-ol
19tracegamma- terpinene
180.35  terpinolene
5tracealpha- thujene
270.022,4,6- trimethyl anisole
24trace1,7,7- trimethyl bicyclo(3.1.1)heptan-2-one

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

#%LeftshiftComponents
1trace  acetone
220.30  artemisyl ketone
27trace  bornyl acetate
28traceiso bornyl acetate
7trace  camphene
11tracedelta-3- carene
16trace1,8- cineole
190.30para- cymene
203.30  dihydrotagetone
6trace  ethyl 2-methyl butyrate
8trace  ethyl valerate
15trace2- hexenal
210.50(Z)-3- hexen-1-ol
141.30  limonene
26trace  linalool
13trace  myrcene
18trace(E)-beta- ocimene
1731.80(Z)-beta- ocimene
230.30(Z)-beta-ocimene epoxide
12tracealpha- phellandrene
3tracealpha- pinene
9tracebeta- pinene
50.50  propyl butyrate
100.30  sabinene
2trace  santene
301.80(E)- tagetenone
316.00(Z)- tagetenone
243.40(E)- tagetone
2546.00(Z)- tagetone
290.30  terpinen-4-ol
4tracealpha- thujene

J. C. Chalchat, R. Ph. Garry and A. Muhayimana, Composition chimique d’huiles essentielles de Tagetes minuta L. du Rwanda. In: Valorisation dela Biomasse Végétale par les produits naturels. Edits., F-X. Garneau and G. J. Collin, p. 295-302, CRDI, Ottawa (1995).

P&F 25, No. 6, 32, (2000)

thuja orientalis fruit oil
#%LeftshiftComponents
120.20iso bornyl acetate
32.20  camphene
162.50  cedrol
141.20  cuparene
81.40para- cymen-8-ol
101.30para- cymen-9-ol
170.50beta- eudesmol
22.30alpha- fenchene
130.30alpha- humulene
50.90  limonene
612.30beta- phellandrene
150.70beta-sesqui phellandrene
167.80alpha- pinene
110.10iso pulegyl acetate
42.00  sabinene
71.10gamma- terpinene
90.40alpha- terpineol
J. of Ess. Oil Res. 12, No. 3, 292, (2000)
thymus zygis gracillis herb oil spain
Variations in the chemical composition of the essential oils of T. sygis L. ssp. sylvestris (Hoffm. et Link) Brot. ex. Coutinho and T. sygis L. ssp. gracilis (boiss.) R. Morales from southeastern Spain were determined by Saez (1995). In this study, oils from four collections of each subspecies were examined by GC and GC/MS. A summary of the data obtained from these analyses (Table IV) shows that different chemotypes of each of the subspecies can be found. Of these, only the thymol chemotypes of T. zygis ssp. gracilis is typical of the red thyme oil in commerce. Only the chemotype thymol will be shown here:
#%LeftshiftComponents
191.63  borneol
141.17iso bornyl acetate
290.05alpha- cadinol
20.30  camphene
110.56  camphor
283.34  carvacrol
160.12beta- caryophyllene
230.07  caryophyllene oxide
71.021,8- cineole
210.08  citronellol
92.95para- cymene
250.08  elemol
220.14  geraniol
200.09  geranyl acetate
60.09  limonene
127.89  linalool
130.06  linalyl acetate
40.06  myrcene
10.04alpha- pinene
30.04beta- pinene
100.36(E)- sabinene hydrate
260.28  spathulenol
151.60  terpinen-4-ol
50.02alpha- terpinene
80.36gamma- terpinene
180.08alpha- terpineol
170.11delta- terpineol
2771.84  thymol
240.08  viridiflorol

F. Saez, Essential oil variability of Thymus zygis growing wild in southeastern Spain. Phytochemistry, 40, 819-825 (1995).

P&F 23, No. 1, 39, (1998)

thymus zygis spp. sylvestris herb oil spain
Variations in the chemical composition of the essential oils of T. sygis L. ssp. sylvestris (Hoffm. et Link) Brot. ex. Coutinho and T. sygis L. ssp. gracilis (boiss.) R. Morales from southeastern Spain were determined by Saez (1995). In this study, oils from four collections of each subspecies were examined by GC and GC/MS. A summary of the data obtained from these analyses (Table IV) shows that different chemotypes of each of the subspecies can be found. Of these, only the thymol chemotypes of T. zygis ssp. gracilis is typical of the red thyme oil in commerce. Only the chemotype thymol will be shown here:
#%LeftshiftComponents
234.06  borneol
181.04iso bornyl acetate
300.04alpha- cadinol
31.76  camphene
150.10  camphor
291.66  carvacrol
200.36beta- caryophyllene
270.63  caryophyllene oxide
91.541,8- cineole
250.06  citronellol
1227.63para- cymene
260.39  geraniol
240.24  geranyl acetate
80.13  limonene
165.10  linalool
170.40  linalyl acetate
60.09  myrcene
101.14(Z)-beta- ocimene
22.28alpha- pinene
40.29beta- pinene
50.06  sabinene
140.22(E)- sabinene hydrate
191.15  terpinen-4-ol
71.91alpha- terpinene
1110.95gamma- terpinene
220.04alpha- terpineol
210.03delta- terpineol
130.15  terpinolene
10.08alpha- thujene
2834.18  thymol

F. Saez, Essential oil variability of Thymus zygis growing wild in southeastern Spain. Phytochemistry, 40, 819-825 (1995).

P&F 23, No. 1, 39, (1998)

valeriana officinalis rhizome oil china
#%LeftshiftComponents
101.31iso borneol
1246.22  bornyl acetate
130.61iso bornyl acetate
260.72  bornyl isovalerate
323.50  camphene
90.33  camphor
141.64  carvyl acetate
220.50beta- caryophyllene alcohol
50.40para- cymene
210.32  decahydro-1,1,4,7-tetramethyl cyclopropazulen-4-ol
200.44  decahydro-2,2,4,8-tetramethyl-4,8-methanazulen-9-ol
170.331,1- dimethoxy-3,7-dimethyl-2,6-octadiene
160.171,4-dimethoxytetramethyl benzene
71.377,7- dimethyl-2-methylene bicyclo(3.1.1)heptane
281.52(2Z)-3,7- dimethyl-2,6-octadien-1-ol isovalerate
230.602,6- dimethyl-6(4-methyl-3-pentenyl)-2-cyclohexene-1-carboxaldehyde
241.934-ethyl-2,2,4-trimethyl-3-(1-methyl ethenyl) cyclohexene methanol
270.61  geranyl isovalerate
180.38beta- gurjunene
250.53  ledol
60.77  limonene
80.353-methyl 2-norbornane carboxaldehyde
25.46alpha- pinene
43.50beta- pinene
110.282-iso propyl-5-methyl anisole
10.43alpha- thujene
190.984(2,6,6- trimethyl cyclohexa-1,3-dienyl)but-2-en-4-one
150.612,2,4-trimethyl-3-cyclohexene-1-methyl acetate

Y-D. Chen and C-H. Gu, Study on the chemical composition of essential oil from Valeriana officinalis. Lincnan Huaxue Yu Gongye, 9(1), 59-64 (1989).

P&F 24, No. 3, 47, (1999)

zingiber officinale oil CO2 extract australia
In 1994, Bartley and Foley analyzed the chemical composition of a supercritical fluid extract of Australian-grown ginger. The freshly harvested roots were peeled and chopped into 2 mm cubes before grinding under liquid nitrogen. The pulp was mixed with coarse granulated Celite (diatomaceous earth) and subjected to extraction by supercritical CO2. The analysis was preformed by a combination of capillary GC (for retention indices and quantitative data) and GC/MS (for component identification confirmation). The compounds identified were:
#%LeftshiftComponents
320.20 aromadendrenol
2310.83alpha- bergamolene
242.73beta- bisabolene
290.14alpha- bisabolol
110.60  borneol
160.10iso bornyl acetate
250.14gamma- cadinene
43.71  camphene
92.991,8- cineole
213.25ar- curcumene
120.11  decanal
280.22  dodecatrienol
190.20beta- elemene
180.23delta- elemene
270.25  elemol
200.18beta- farnesene
1525.06  geranial
140.66  geraniol
170.12  geranyl acetate
10.52  hexanal
70.43  limonene
100.46  linalool
20.113- methyl hexanol
60.53  myrcene
132.87  neral
350.086- paradol
340.20 pentenyl curcumene
81.63beta- phellandrene
268.18beta-sesqui phellandrene
50.08beta- pinene
300.22(Z)-sesqui sabinene hydrate
360.316- shogaol
30.93alpha- thujene
310.15 zingerenol
2225.87  zingiberene
330.64 zongerone

J. P. Bartley and P. Foley, Supercritical fluid extraction of Australian grown ginger (Zingibar officinale), J. Sci. Food Agric., 66, 365-371 (1994).

P&F 22, No. 5, 71, (1997)

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