BT

Typical G.C. analysis

cistus oil
#%LeftshiftComponents
60.1  acetophenone
1410.26- acetoxy-11-nor-drim-7-en-9-one
720.27- acetyl-2,2,6-trimethyl bicyclo(4.2.0)octane
1190.16-acetyl-5,8,8-trimethyl bicyclo(3.2.1)octan-2,3-dione
1490.213-nor- ambreinolide
1480.18-epi-13-nor- ambreinolide
780.2alpha- ambrinol
1371.4  ambrox
1440.16-oxo-isoambrox
810.9  aromadendr-1-ene
1350.3  aromadendr-1(10)-en-9-one
911.41,5-(Z)-aromadendr-9-ene
1320.11,10-seco- aromadendran-1,10-dione
1300.15-epi-1,10-seco- aromadendran-1,10-dione
861.5allo- aromadendrene
b30.4  benzoic acid
272.0  borneol
551.7  bornyl acetate
b210.93-iso butenyl-5-methyl-5-vinyl butyrolactone
1260.5  cadalene
980.4delta- cadinene
1250.6alpha- cadinol
1000.6alpha- calacorene
990.6(E)- calamenene
900.5(Z)- calamenene
b91.4gamma-campholenic acid
150.3alpha- campholenic aldehyde
100.3gamma- campholenic aldehyde
b70.3alpha-campholytic acid
b40.2gamma-campholytic acid
b52.4 camphonanic acid
b122.1alpha-camphoneic acid
180.1  camphor
600.8  carvacrol
480.2  carvenone
410.2trans- carveol
430.1cis- carveol
460.5  carvone
1380.1sesqui chamaenol
1171.8  copaborneol
1270.6  copabornyl acetate
741.1alpha- copaene
820.7  cubeb-11-ene
1134.1  cubeban-11-ol
1210.41-epi- cubenol
440.1  cuminaldehyde
b111.0beta- cyclogeranic acid
b80.9gamma-cyclogeranic acid
530.3para- cymen-7-ol
30.4para- cymene
b130.7 davanic acid
390.2  decanal
b203.8  decanoic acid
1060.21,2- dehydroglobulol
1180.33,4- dehydroglobulol
1100.21-epi-3,4- dehydroviridiflorol
1041.41,2- dehydroviridiflorol
1460.214,15- di-nor-8,13-epoxylabd-12-ene
790.1  dihydro-beta-ionene
940.2  dihydroactinidiolide
370.5neo dihydrocarveol
b156.5  dihydrocinnamic acid
b241.7 dimethyl (Z)-2-hexyl-3-methyl butendioic acid
490.22,4- dimethyl acetophenone
91.0alpha-para- dimethyl styrene
970.24,7- dimethyl tetral-1-one
b141.22,6- dimethyl-5-oxoheptanoic acid
770.2  dodecanal
700.111-nor- drim-7-ene
1390.1  drim-8-en-7-one
690.211-nor- drim-8-ene
1010.311-nor- driman-8-ol
1020.2beta- elemol
351.3  elsholtzia ketone
1360.25,11- epoxycadin-1(10)-en-9-ol
1080.85,11-epoxycadin-1(10)-ene
80.86,8- epoxymenth-1-ene
640.1  ethyl dihydrocinnamate
1240.4beta- eudesmol
1220.2gamma- eudesmol
651.6  eugenol
450.2alpha- fenchyl acetate
760.11-( fur-2-yl methyl)-2-formyl pyrrole
b192.4  geranic acid
510.2  geraniol
800.1  geranyl acetone
1090.5  gleenol
1110.2  globulol
b20.5  heptanoic acid
b10.7  hexanoic acid
1330.1(Z)-3-hexen-1-yl dihydrocinnamate
1340.3  hexyl dihydrocinnamate
590.1(2E,4E)-6-hydroxy-2,6-dimethyl hepta-2,4-dienal
32trace2- hydroxy-3-methyl benzaldehyde
660.22- hydroxy-4-isopropenyl toluene
680.2(E)-5-hydroxy-para-mentha-1(6),8-dien-2-one
710.3(Z)-5-hydroxy-para-mentha-1(6),8-dien-2-one
1400.110- hydroxycalamene-8,9-epoxide
1310.19- hydroxyladanifer-10-one(9(10(1))-abeo-9-hydroxyaromadendran-10-one)
500.42- hydroxypinan-3-one
870.2(E)-beta- ionone
1420.615-nor-labd-1(17)-ene
1530.4  labd-7-en-15-ol
1450.515-nor- labd-7-ene
b316.3 labd-7-enoic acid
1540.3  labd-8-en-15-ol
1430.515-nor-labd-8-ene
b324.0 labd-8-enoic acid
1520.4  labd-8(17)-en-15-ol
b305.1 labd-8(17)-enoic acid
1470.715-nor-labdan-8-ol
b232.5  lauric acid
929.3  ledene
730.2iso ledene
1161.3  ledol
120.2  linalool
70.4(E)- linalool oxide furanoid
110.2(Z)- linalool oxide furanoid
b281.0  linoleic acid
1500.3  manoyl oxide
1510.313-epi- manoyl oxide
850.1  massoia lactone
400.3(Z)-para- menth-4(8)-en-2-ol
620.12- methoxy-6-methyl acetophenone
290.3para- methyl acetophenone
521.0  methyl dihydrocinnamate
750.4  methyl eugenol
10.25- methyl furfural
20.16- methyl-5-hepten-2-one
1200.3  muurola-4,10(14)-dien-1-ol
1230.3alpha- muurolol
b252.7  myristic acid
330.9  myrtenal
b186.0  myrtenic acid
361.5  myrtenol
581.1  naginata ketone
220.2  nerol oxide
1030.2(E)- nerolidol
130.1  nonanal
b101.6  nonanoic acid
170.7(E)-3- nonen-2-one
b63.7  octanoic acid
b271.2  oleic acid
1150.1beta- oplopenone
b265.1  palmitic acid
1051.2  palustrol
1290.1  pentadecanal
420.13- phenyl propanol
231.5  pinocamphone
280.7iso pinocamphone
191.8trans- pinocarveol
240.3  pinocarvone
630.4trans- pinocarvyl acetate
470.8  piperitone
250.1  propiophenone
1280.24-iso propyl-6-methyl tetral-1-one
160.1(E)- rose oxide
140.2(Z)- rose oxide
200.1(E)- sabinol
b290.8  stearic acid
210.2(E)- tagetone
260.2(Z)- tagetone
310.8  terpinen-4-ol
340.5alpha- terpineol
1140.1  tetradecanal
890.61,1,5,6- tetramethyl-1,2-dihydronaphthalene
950.21,1,5,6- tetramethyl-1,2,3,4-tetrahydronaphthalene
540.2  thymol
1070.26-para-tolyl heptan-2-one
880.1  tridecanal
b160.71,5,5-trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid A
b171.91,5,5-trimethyl bicyclo(4.1.0)heptan-7-carboxylic acid B
50.32,2,6- trimethyl cyclohex-2-enone
41.32,2,6- trimethyl cyclohexanone
930.21-(1,2,2- trimethyl cyclopent-1-yl) pentan-1,4-dione
960.26,6,10-trimethyl decan-2-one
300.52,2,5- trimethyl oxepan-4-one
670.21,1,6- trimethyl-1,2-dihydronaphthalene
830.14,4,7a- trimethyl-1,4,5,6,7,7a-hexahydro-2H-inden-2-one
840.1  tuberolactone
610.2  undecanal
b220.3  undecanoic acid
380.3  verbenone
1124.3  viridiflorol
560.2  vitispirane A
570.1  vitispirane B

P. Weyerstahl, H. Marschall, M. Weirauch, K. Thefeld and H. Surburg, Constituents of commercial labdanum oil. Flav. Fragr. J., 13, 295-318 (1998).

P&F 24, No. 4, 31, (1999)

tagetes minuta flower oil CO2 extract
#%LeftshiftComponents
543.56 alchenenotriol
309.98(E)- anethole
272.10para- anisaldehyde
410.33  aromadendrene
470.08beta- bisabolene
480.12gamma- cadinene
140.11  camphor
240.23cis- carveol
403.44beta- caryophyllene
230.61  citronellol
21.12para- cymene
311.51 dehydroelshotzia ketone
200.12(Z)- dihydrocarvone
65.19  dihydrotagetone
90.22alpha-para- dimethyl styrene
333.00delta- elemene
500.11gamma-elemene (furanoid)
210.15  elsholtzia ketone
490.15  eugenyl acetate
370.28  geranyl acetate
530.28  guaiol
422.14alpha- humulene
510.29  ledol
315.14  limonene
111.03  linalool
80.43(Z)- linalool oxide furanoid
280.47  linalyl acetate
100.12(E)-para- menth-2-en-1-ol
290.39  methyl citronellate
390.24  methyl eugenol
430.226-methyl-gamma-ionone
450.29alpha- muurolene
10.24  myrcene
340.19  neryl acetate
50.30(E)-beta- ocimene
419.33(Z)-beta- ocimene
360.10beta- patchoulene
460.13  pentadecane
170.30(Z)- pinanone
133.68(Z)- sabinene hydrate
350.32(E)-iso safrole
522.42  spathulenol
260.65(E)- tagetenone
2513.26(Z)- tagetenone
152.81(E)- tagetone
160.34(Z)- tagetone
180.46  terpinen-4-ol
70.26gamma- terpinene
190.50alpha- terpineol
380.16  tetradecane
120.24alpha- thujone
320.12  tridecane
440.57  valencene
220.05  verbenone

J. Daghero, M. Mattea, E. Reverchon, G. Della Porta and F. Senatore, Isolation of Tagetes minuta L. oil using supercritical CO2 extraction. In: Proceedings WOCMAP-2. Edits., V. Martino, A. Bandoni, G. Bleak and N. Capelle, Acta Hort., 503, 21-25 (1999).

P&F 25, No. 6, 32, (2000)

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