BT

Typical G.C. analysis

acorus calamus leaf oil
#%LeftshiftComponents
301.61  acolamone
363.62iso acolamone
284.09  acoragermacrone
396.57(1,10)- aristolen-2-one
340.21beta- bisabolene
100.11  borneol
140.25  bornyl acetate
170.05beta- bourbonene
294.07delta- cadinene
310.30alpha- calacorene
420.58iso calamendiol
410.10  calamenene
400.72  calamusenone
90.08  camphor
204.13beta- caryophyllene
160.04alpha- copaene
230.32beta- cubebene
351.81isoepi-cubenol
40.04para- cymene
430.40  dibutyl phthalate
180.79beta- elemene
150.21delta- elemene
320.73  elemol
270.80beta- guaiene
240.96beta- gurjurene
210.07alpha- humulene
52.61  limonene
83.10  linalool
130.11  linalyl acetate
470.02  linoleic acid
30.07para- mentha-2,4(8)-diene
480.04  methyl 9,12,15-octadecatrienoate
190.86  methyl eugenol
263.37(E)- methyl isoeugenol
2236.40(Z)- methyl isoeugenol
372.60alpha- muurolol
383.17epi-alpha- muurolol
20.09  myrcene
450.041- octadecene
440.06  palmitic acid
460.11  phytol
10.21  sabinene
253.19  shyobunone
330.64iso shyobunone
110.21  terpinen-4-ol
70.04alpha- terpinene
60.05gamma- terpinene
120.31alpha- terpineol
490.10  tricosane

M. X. Li and Z-B. Jiang, The volatile constituents of the essential oil and their distribution in Acorus calamus L. Zhongcaoyo, 24, 459-461 (1993).

P&F 22, No. 2, 59, (1997)

acorus calamus rhizome oil
#%LeftshiftComponents
193.09  acolamone
253.25iso acolamone
177.38  acoragermacrone
330.24  acorenone
262.85beta- asarone
30.11  borneol
352.46  cadala-1,4,9-triene
183.72delta- cadinene
201.30alpha- calacorene
230.30beta- calacorene
370.86  calamendiol
368.37iso calamendiol
3114.70  calamenene
380.60  calamenone
300.73  calamusenone
20.24  camphor
90.33beta- caryophyllene
60.07alpha- copaene
120.14beta- cubebene
320.231,4- dihydro-1,1,4,4-tetramethyl-2,3-naphthalene dione
70.48beta- elemene
210.60  elemol
160.90beta- guaiene
130.12beta- gurjunene
100.31beta- gurjurene
292.488-hydroxy-delta-cadinene
340.808-hydroxy-gamma-cadinene
10.21  linalool
80.58  methyl eugenol
150.29(E)- methyl isoeugenol
1117.70(Z)- methyl isoeugenol
271.18alpha- muurolol
281.70epi-alpha- muurolol
145.03  shyobunone
240.82epi- shyobunone
220.08iso shyobunone
40.22  terpinen-4-ol
50.14alpha- terpineol

M. X. Li and Z-B. Jiang, The volatile constituents of the essential oil and their distribution in Acorus calamus L. Zhongcaoyo, 24, 459-461 (1993).

P&F 22, No. 2, 59, (1997)

acorus calamus root oil
#%LeftshiftComponents
260.33  acolamone
190.35  acoradiene
240.50  acoragermacrone
361.09  acorenone
301.68beta- asarone
30.04  borneol
60.04  bornyl acetate
370.64  cadala-1,4,9-triene
251.57beta- cadinene
120.44delta- cadinene
132.11gamma- cadinene
270.68alpha- calacorene
290.91preiso calamendiol
343.15  calamenene
399.62  calamenone
20.03  camphor
141.43  cascarilladiene
100.61alpha- cedrene
90.05alpha- copaene
200.74ar- curcumene
420.097-desmethyl-2-methoxycadalene
400.15  dibutyl phthalate
350.591,4- dihydro-1,1,4,4-tetramethyl-2,3-naphthalene dione
330.451,6- dimethyl-4-isopropyl naphthalene
110.29beta- elemene
220.30(E,E)-alpha- farnesene
161.12(E)-beta- farnesene
210.11beta- guaiene
157.66beta- gurjurene
10.24  linalool
172.85(Z)- methyl isoeugenol
230.96alpha- muurolene
310.69alpha- muurolol
320.24epi-alpha- muurolol
410.05  palmitic acid
380.352-isoproponyl-6-isopropyl methyl-3-vinyl cyclohexanol
80.01alpha-sabinene
2818.70epi- shyobunone
40.08  terpinen-4-ol
50.05alpha- terpineol
70.133,3,7,9-tetramethyl tricyclo(5.4.0.0)undecene
180.162,6,10,10-tetramethyl tricyclo(7.2.0.0)undecene

M. X. Li and Z-B. Jiang, The volatile constituents of the essential oil and their distribution in Acorus calamus L. Zhongcaoyo, 24, 459-461 (1993).

P&F 22, No. 2, 59, (1997)

artemisia campestris spp. glutinosa flower oil italy
#%LeftshiftComponents
21trace  aromadendrene
2714.50  bicyclogermacrene
330.90 bisabolene endoperoxide
397.00alpha- bisabolol
421.70alpha-bisabolol oxide
220.10iso borneol
30tracedelta- cadinene
440.50alpha- cadinol
320.20  calamenene
2trace  camphene
18trace  camphor
430.90  carvacrol
340.30  caryophyllene oxide
371.00  cedrol
70.201,8- cineole
170.40alpha- copaene
310.20ar- curcumene
110.10para- cymene
285.00(E,E)-alpha- farnesene
241.50(E)-beta- farnesene
290.10  geranyl acetate
268.00  germacrene D
401.00  globulol
230.40beta- guaiene
140.20(Z)-3- hexen-1-yl isovalerate
251.40alpha- humulene
63.00  limonene
353.70  methyl eugenol
450.40T- muurolol
511.20  myrcene
200.40  myrtenal
360.80(E)- nerolidol
82.40(Z)-beta- ocimene
130.10allo- ocimene
105.40(E)-beta- ocimene
12.60alpha- pinene
319.00beta- pinene
40.30  sabinene
410.90  spathulenol
190.90  terpinen-4-ol
90.40gamma- terpinene
12trace  terpinolene
15tracealpha- thujone
16tracebeta- thujone
380.90  viridiflorol
J. of Ess. Oil Res. 13, No. 2, 91, (2001)
artemisia variabilis flower oil italy
#%LeftshiftComponents
380.40  acenaphthalene
240.70  bicyclogermacrene
331.00alpha- bisabolol
26tracedelta- cadinene
370.90alpha- cadinol
2trace  camphene
16trace  camphor
80.101,8- cineole
27tracear- curcumene
300.101H-cyclobutano(de)naphthalene
120.40para- cymene
3977.301,2-dihydroacenaphthlene
280.501,4- dimethyl naphthalene
250.10  geranyl acetate
230.30  germacrene D
340.20  globulol
20tracebeta- guaiene
15trace(Z)-3- hexen-1-yl isovalerate
210.10alpha- humulene
400.102- hydroxy-4,6-dimethoxyacetophenone
71.00  limonene
17trace  linalool
29trace  methyl eugenol
50.20  myrcene
19trace  myrtenal
310.30(E)- nerolidol
95.50(Z)-beta- ocimene
14traceallo- ocimene
111.30(E)-beta- ocimene
10.80alpha- pinene
33.60beta- pinene
40.10  sabinene
351.00  spathulenol
180.10  terpinen-4-ol
60.10alpha- terpinene
103.20gamma- terpinene
220.20alpha- terpineol
13trace  terpinolene
360.80  thymol
320.20  viridiflorol
J. of Ess. Oil Res. 13, No. 2, 91, (2001)
cajuput leaf oil vietnam
#%LeftshiftComponents
49trace  bulnesol
370.4  cadina-1,4-diene
35tracedelta- cadinene
34tracegamma- cadinene
47tracealpha- cadinol
44traceT- cadinol
38trace  calamenene
2trace  camphene
5tracedelta-3- carene
232.5beta- caryophyllene
410.3  caryophyllene oxide
1041.11,8- cineole
20tracealpha- copaene
270.5gamma- curcumene
156.8para- cymene
170.2para- cymenene
220.3beta- elemene
18tracedelta- elemene
25tracegamma- elemene
42trace  elemol
480.7beta- eudesmol
450.6gamma- eudesmol
310.3alpha- farnesene
390.4  geraniol
290.3beta- guaiene
431.2  guaiol
281.6alpha- humulene
94.1  limonene
213.6  linalool
40tracealpha- maaliene
46tracealpha- muurolol
60.1  myrcene
14trace(E)-beta- ocimene
12trace(Z)-beta- ocimene
70.5alpha- phellandrene
110.2beta- phellandrene
36tracebeta-sesqui phellandrene
13.2alpha- pinene
30.8beta- pinene
4trace  sabinene
331.5alpha- selinene
321.5beta- selinene
241.5  terpinen-4-ol
80.6alpha- terpinene
134.6gamma- terpinene
308.7alpha- terpineol
165.9  terpinolene
26trace  thujopsene
190.3alpha- ylangene

O. Motl, J. Hodacova and K. Ubik, Composition of Vietnamese cajuput essential oil. Flav. Fragr. J., 5, 39-42 (1990).

P&F 25, No. 1, 33, (2000)

chamaecyparis obtusa leaf oil
#%LeftshiftComponents
131.23  borneol
177.15  bornyl acetate
361.70 cadin-10(15)-4-ol
272.76delta- cadinene
280.53gamma- cadinene
204.71beta-cadrene
300.41  calamenene
20.23  camphene
380.65  caryophylla-3,8(13)-dien-5alpha-ol
181.65(Z)- caryophyllene
190.28beta- caryophyllene
320.93  cedrol
250.48beta- cubebene
90.82para- cymene
211.47alpha- elemene
290.39gamma- elemene
3114.78  elemol
345.39alpha- eudesmol
356.54beta- eudesmol
338.28gamma- eudesmol
102.09alpha- fenchol
240.30beta- guaiene
63.05  limonene
120.41  longicyclene
370.73 longicyclenyl aclohol
150.72  longifolene
110.37alpha- longipinene
263.81alpha- muurolene
225.71gamma- muurolene
11.01alpha- pinene
42.77beta- pinene
31.61  sabinene
51.11alpha- terpinene
71.77gamma- terpinene
141.11alpha- terpineol
81.00  terpinolene
239.09alpha- terpinyl acetate
160.89  verbenone

B. Shieh, Y. Lizuka and Y. Matsubara, Monoterpenoid and sesquiterpenoid constituents of the essential oil of Hinoki (Chamaecyparis obtusa (Sieb. et Zucc. ) Endl.). Agric. Biol. Chem. (Japan), 45, 1497-1499 (1981).

P&F 8, No. 1, 61, (1983)

cinnamomum zeylanicum fruit oil india
In 1997, Jayaprakasha et al. analyzed two oils of the fruit of C. zeylanicum by GC and GC/MS. Although the oils were produced from fruit harvested in two different locations in India, Karnataka and Kerala, the oil compositions were similar as can be seen from the following analytical results:
#%LeftshiftComponents
322.7-2.8  benzyl benzoate
80.3-0.4  borneol
212.3-3.0delta- cadinene
201.2-1.6gamma- cadinene
311.0-1.5alpha- cadinol
302.7-3.4T- cadinol
159.2-13.7beta- caryophyllene
240.9-1.1  caryophyllene oxide
100.6-4.3(E)- cinnamaldehyde
70.2-0.3(Z)- cinnamaldehyde
1642.4-54.2(E)- cinnamyl acetate
112.0-2.2(E)- cinnamyl alcohol
141.8-3.1alpha- copaene
290.5-0.8  cubenol
270.4-0.510-epi-gamma- eudesmol
120.2-0.3  eugenol
191.7-2.0  germacrene B
180.7-0.8  germacrene D
260.3  germacrene D-4-ol
250.5-0.6  globulol
220.4beta- guaiene
172.8-3.1alpha- humulene
340.0-0.3  methyl oleate
330.0-0.3  methyl palmitate
280.3alpha- muurolol
30.0-0.2  myrcene
230.2-0.4  nerolidol
60.2-0.5(E)-beta- ocimene
40.1-0.7alpha- phellandrene
50.4-1.6beta- phellandrene
132.9-4.33- phenyl propyl acetate
10.1-1.6alpha- pinene
20.1-0.6beta- pinene
90.3alpha- terpineol

G. K. Jayaprakasha, L. Jaganmohan Rao and K. K. Sakariah, Chemical composition of the folatile oil from the fruits of Cinnamomum zeylanicum Blume. Flav. Fragr. J., 12, 331-333 (1997)

P&F 23, No. 1, 39, (1998)

schinus molle leaf oil
#%LeftshiftComponents
211.71delta- cadinene
31tracealpha- cadinol
274.70T- cadinol
230.93  calamenene
2trace  camphene
160.47beta- caryophyllene
140.02alpha- copaene
130.01alpha- cubebene
100.59para- cymene
150.01beta- elemene
18tracegamma- elemene
2413.25  elemol
30tracealpha- eudesmol
263.24gamma- eudesmol
205.21  germacrene D
22tracebeta- guaiene
190.39alpha- humulene
89.27  limonene
12trace  methyl octanoate
29tracealpha- muurolol
28traceT- muurolol
5trace  myrcene
252.94  neryl hexanoate
630.24alpha- phellandrene
99.63beta- phellandrene
11.46alpha- pinene
30.10beta- pinene
40.67  sabinene
170.03  terpinen-4-ol
70.02alpha- terpinene
110.20  terpinolene

M. Maffei and F. Chialva, Essential oils from Schinus molle berries and leaves. Flav. Fragr. J., 5, 49 -52 (1990).

P&F 22, No. 5, 71, (1997)

schinus molle seed oil
Bernhard et al. (1983) analyzed an oil of S. molle fruit produced by the Likens-Nickerson apparatus using GC/MS. They found that the oil contained the following components:
#%LeftshiftComponents
129.11delta- cadinene
326.64 cadinol
271.39T- cadinol
230.26alpha- calacorene
160.15gamma- calacorene
140.28  calamenene
82.02beta- caryophyllene
210.12alpha- copaene
200.13alpha- cubebene
172.93para- cymene
70.52beta- elemene
241.32  elemol
300.90alpha- eudesmol
311.01beta- eudesmol
261.04gamma- eudesmol
150.34  geranyl butyrate
130.22beta- guaiene
220.71alpha- gurjunene
90.58alpha- humulene
57.23  limonene
190.95  methyl octanoate
111.48alpha- muurolene
100.48gamma- muurolene
290.69alpha- muurolol
282.32T- muurolol
320.41  myrcene
250.28  neryl hexanoate
417.34alpha- phellandrene
66.21beta- phellandrene
12.66alpha- pinene
20.17beta- pinene
180.10  terpinolene

R. A. Bernhard, T. Shibamoto, K. Yamaguchi and E. White, The volatile constituents of Schinus molle L. J. Agric. Food Chem., 31, 463-466 (1983).

P&F 22, No. 5, 71, (1997)

valeriana officinalis rhizome oil CO2 extract china
#%LeftshiftComponents
10.37  acetic acid
170.01  benzoic acid
410.72(E)-alpha- bergamotol
420.34(Z)-alpha-bergamotol
180.47  borneol
2336.07  bornyl acetate
360.24delta- cadinene
100.02iso camphane
52.81  camphene
110.03delta-3- carene
250.02trans-carvone oxide
240.14cis- carvone oxide
310.65beta- caryophyllene
130.021,8- cineole
210.19  cumic acid
80.02para- cymene
290.07beta- elemene
270.08delta- elemene
370.53  elemol
120.013- ethyl-2,5-dimethyl-1,3-hexadiene
442.45  eugenyl acetate
350.66 germacrene
402.24  globulol
340.23  guaiene
320.21beta- gurjunene
330.31alpha- humulene
90.26  limonene
150.02  linalool
220.12  methyl chavocol
200.02  myrtenol
4326.56  nootkatone
40.60alpha- pinene
70.59beta- pinene
60.03  sabinene
160.01  sabinene hydrate
263.03  sabinyl acetate
380.73 sabinyl valerate
391.84  spathulenol
190.13  terpinen-4-ol
140.02  terpinolene
280.62alpha- terpinyl acetate
300.42 thymohydroquinone dimethyl ether
30.03  tricyclene
20.21iso valeric acid

J-J. Xian, G. Yuan, Y-X. Zhang, J-M. Yuan and X-W. Luo, The chemical constituents of the essential oil from the roots of Valeriana officinalis. Yunnan Zhiwu Yanjiu, 17, 479-481 (1995).

P&F 24, No. 3, 47, (1999)

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