BT

Typical G.C. analysis

apium graveolens leaf oil
#%LeftshiftComponents
226.20  butyl phthalide
210.90  butylidene phthalide
3trace  camphene
110.50para- cymene
243.203a,4-dehydroisobutylidene phthalide
171.40beta-elemene + caryophyllene
18tracealpha- humulene
230.20  ligustilide
826.30  limonene
10.103- methyl-4-ethyl hexane
633.60  myrcene
914.10(Z)-beta- ocimene
140.30allo- ocimene
15trace  pentyl benzene
131.00 pentyl cyclohexadiene
20.20alpha- pinene
40.10beta- pinene
5trace  sabinene
203.70beta- selinene
160.10  terpinen-4-ol
7tracealpha- terpinene
102.20gamma-terpinene + (E)-beta-ocimene
190.30alpha- terpineol
120.20  terpinolene

D. Fehr, Untersuchung uber Aromastoffe von Sellerie (Apium graoeolens L.). Pharmazie, 36, 374-376 (1979).

P&F 10, No. 5, 93, (1985)

apium graveolens seed oil CO2 extract
#%LeftshiftComponents
225.49  butyl phthalide
100.03trans- carveol
110.02cis- carveol
120.02  carvone
140.03cis- carvyl acetate
170.21beta- caryophyllene
210.21  caryophyllene oxide
80.02  dihydrocarvone
270.07 diterpene hc
160.04beta- elemene
180.03alpha- humulene
314.88  limonene
60.01  limonene oxide
50.02  linalool
291.04  linoleic acid
90.01para- mentha-6,8-dien-2-ol
20.97  myrcene
70.33  naphthalene
40.02  ocimene
302.38 octadecenoic acid
280.65  palmitic acid
150.02  phenyl pentanone
10.19beta- pinene
130.02(E)- sabinyl acetate
2628.84  sedanolide (3-butyl-3a,4,5,6-tetrahydrophthalide)
201.82alpha- selinene
1917.59beta- selinene
2522.39  sendanenolide (butyl-4,5-dihydrophthalide)
310.07  stearic acid
230.08 unknown phthalate 1
240.03 unknown phthalate 2

P-J, Fan, Z-D. Guo, J-C. Zhang, J-Q. Zheng and L-M. Liu, A study of the composition of supercritical CO2 fluid extract of celery seed. Tianran Chanwa Yanjiu Yu Kaifa, 7(2), 89-93 (1995).

P&F 23, No. 4, 37, (1998)

apium graveolens seed oil india
#%LeftshiftComponents
232.68  butyl phthalide
110.13trans- carveol
120.06cis- carveol
130.06  carvone
150.07cis- carvyl acetate
180.27beta- caryophyllene
220.25  caryophyllene oxide
90.07  dihydrocarvone
170.07beta- elemene
190.05alpha- humulene
451.95  limonene
70.08  limonene oxide
60.06  linalool
100.06para- mentha-6,8-dien-2-ol
34.38  myrcene
80.79  naphthalene
50.07  ocimene
160.12  phenyl pentanone
10.05alpha- pinene
21.16beta- pinene
140.09(E)- sabinyl acetate
272.50  sedanolide (3-butyl-3a,4,5,6-tetrahydrophthalide)
212.17alpha- selinene
2020.76beta- selinene
269.89  sendanenolide (butyl-4,5-dihydrophthalide)
240.06 unknown phthalate 1
250.07 unknown phthalate 2

P-J. Fan, Z-D. Guo, J-C. Zhang, J-Q. Zheng and L-M. Liu, A study of the composition of supercritical CO2 fluid extract of celery seed. Tianran Chanwa Yanjiu Yu Kaifa, 7(2), 89-93 (1995).

P&F 23, No. 4, 37, (1998)

carrot seed oil
#%LeftshiftComponents
360.08(E)- anethole
210.73(E)-alpha- bergamotene
201.08(Z)-alpha- bergamotene
380.23beta- bisabolene
430.21alpha- bisabolol
420.273- butyl phthalide
20.44  camphene
395.68  carotol
350.23  carvomenthone
153.56beta- caryophyllene
371.09  caryophyllene oxide
400.29 cedrene oxide
140.17alpha- copaene
100.41para- cymene
130.39  daucene
410.14  daucol
180.42alpha- farnesene
230.60beta- farnesene
310.89  geranial
3234.17  geranyl acetate
301.13alpha- humulene
70.48  limonene
120.11  linalool
191.24  longifolene
250.18para- mentha-1,3-dien-7-ol
51.87  myrcene
290.53  neral
331.01  nerol
81.92(E)-alpha- ocimene
19.09alpha- pinene
34.49beta- pinene
49.44  sabinene
340.14  sabinene hydrate
170.40alpha- santalene
220.67beta- santalene
440.13  sedanenolide
450.40  sedanolide (3-butyl-3a,4,5,6-tetrahydrophthalide)
280.44alpha- selinene
270.23beta- selinene
160.31  terpinen-4-ol
60.96alpha- terpinene
90.36gamma- terpinene
241.65alpha- terpineol
110.28  terpinolene
262.34  verbenol

F. Perineau, L. Ganou and A. Gaset, Etude de la production d’huile essentielle de fruit de carotte. Ind. Aliment. Agric., 108, 357-366 (1991).

P&F 17, No. 3, 61, (1992)

carum graveolens seed oil egypt
#%LeftshiftComponents
110.61  anethole
180.12alpha- bisabolene
190.123- butyl hexahydrophthalide
200.38  butyl phthalide
100.40  carvone
131.54beta- caryophyllene
150.18beta- farnesene
140.13alpha- humulene
458.53  limonene
60.10  linalool
90.48para- methoxyacetophenone
33.12  myrcene
73.27 pentyl cyclohexadiene
50.10alpha- phellandrene
10.14alpha- pinene
21.29beta- pinene
2117.28  sedanolide (3-butyl-3a,4,5,6-tetrahydrophthalide)
171.37alpha- selinene
168.10beta- selinene
80.28alpha- terpineol
120.15  umbellulone

A. F. Halim, M. M. Mashaly, O. salama, A. F. Ali and P. Sandra, Analysis of celery fruit oil and investigation on the effect of storage, Egypt. J. Pharm. Sci., 31, 107-113 (1990).

P&F 20, No. 1, 47, (1995)

petroselinum crispum leaf oil
#%LeftshiftComponents
3927.96 apiole
250.02alpha- bergamotene
480.04  bergapten
300.41beta- bisabolene
190.02  bornyl acetate
370.783- butyl phthalide
380.63(E)- butylidene phthalide
40trace(Z)- butylidene phthalide
350.01  carotol
240.02beta- caryophyllene
220.02alpha- copaene
71.46para- cymene
120.04para- cymenene
18trace(E)-2- decenal
170.77(Z)-2- decenal
291.672,6- dimethoxy-4-(2-propenyl) phenol
231.59beta- elemene
330.71  elemicin
521.79  falcarindiol
4915.00  falcarinol
260.01(E)-beta- farnesene
270.17  germacrene D
550.37  heraclenol
460.37  hexadecanoic acid
540.04  imperatorin
422.79(E)- ligustilide
440.01(Z)- ligustilide
130.15  linalool
510.01  linoleic acid
140.49para- menthatriene
500.06  methyl linoleate
51.94  myrcene
318.70  myristicin
360.06iso myristicin
150.05  myrtenal
340.02  nerolidol
90.02(E)-beta- ocimene
60.39alpha- phellandrene
81.72beta- phellandrene
328.51beta-sesqui phellandrene
531.06iso pimpinellin
20.25alpha- pinene
42.00beta- pinene
451.24  psoralen
30.01  sabinene
412.29  sedanenolide
430.05(E)-sedanolide
100.09gamma- terpinene
112.50  terpinolene
21tracealpha- terpinyl acetate
10.14alpha- thujene
160.20  undecatriene
200.424- vinyl guaiacol
470.24  xanthotoxin
280.05  zingiberene

M. Spraul, Strukteraufklarung Wertgebender Inhaltsstoffe aus Petersilienblatten, - Wurzeln and -samen sowie aus Dillbluten. Ph.D. thesis Technische Universtat, Munchen (1991).

P&F 21, No. 4, 57, (1996)

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